Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals
The quintessence of the hot‐injection method, a synthesis route for monodisperse, highly luminescent semiconductor nanocrystals, is reviewed. The separate stages of nucleation and growth of the nanocrystals are discussed in the framework of classical nucleation theory and an equilibrium model propos...
Gespeichert in:
| Veröffentlicht in: | Small (Weinheim an der Bergstrasse, Germany) Germany), 2005-12, Vol.1 (12), p.1152-1162 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 1162 |
|---|---|
| container_issue | 12 |
| container_start_page | 1152 |
| container_title | Small (Weinheim an der Bergstrasse, Germany) |
| container_volume | 1 |
| creator | de Mello Donegá, Celso Liljeroth, Peter Vanmaekelbergh, Daniel |
| description | The quintessence of the hot‐injection method, a synthesis route for monodisperse, highly luminescent semiconductor nanocrystals, is reviewed. The separate stages of nucleation and growth of the nanocrystals are discussed in the framework of classical nucleation theory and an equilibrium model proposed by Debye. We also review the numerous adaptations of the original synthesis that currently provide colloidal nanocrystals with well‐defined, size‐dependent optical, electrical, and magnetic properties. The availability of these remarkable materials is one of the most promising developments in nanoscience and nanotechnology.
Suspensions of monodisperse, highly luminescent nanocrystals are currently prepared by a hot‐injection method. Due to their size‐dependent optoelectronic properties, such nanocrystals are of enormous interest. In this Review, we examine whether we can understand the results of this method at the atomic level. We also review adaptations to this method that have been proposed to prepare a variety of semiconductor and magnetic nanocrystals. |
| doi_str_mv | 10.1002/smll.200500239 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_70182273</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>70182273</sourcerecordid><originalsourceid>FETCH-LOGICAL-c4879-318cebe2ad00d4a6298376f1103660c8a26ab487887ed5c468a4d5acb0a411a23</originalsourceid><addsrcrecordid>eNqFkE1v1DAQhq0K1JbSK0fkE6dm8UfWdo6o6peULVULVOrFmnUmrEsSb-0EyL8nZVcLt55mxn7e5_AS8o6zGWdMfExt08wEY_PpkMUeOeSKy0wZUbza7ZwdkDcpPTImucj1PjngmhcyZ8Uh-X6zGpN3wa2w9Q4aevYTmgF6HzoaatqvkF6GPrvqHtH9fVxgvwrVCQV6N3bTd_KJ3oahR1qHSBehC5VPa4wJ6TV0wcUx9dCkt-R1PQ083s4j8vX87MvpZVZ-vrg6_VRmLje6yCQ3DpcooGKsykGJwkitas6ZVIo5A0LBciKN0VjNXa4M5NUc3JJBzjkIeUQ-bLzrGJ4GTL1tfXLYNNBhGJLVjBshtJzA2QZ0MaQUsbbr6FuIo-XMPldrn6u1u2qnwPuteVi2WP3Dt11OQLEBfvkGxxd09m5Rlv_Ls03Wpx5_77IQf1ilpZ7b--sLe1_ePuTf9OSTfwB8V5Xk</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>70182273</pqid></control><display><type>article</type><title>Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals</title><source>MEDLINE</source><source>Wiley Online Library All Journals</source><creator>de Mello Donegá, Celso ; Liljeroth, Peter ; Vanmaekelbergh, Daniel</creator><creatorcontrib>de Mello Donegá, Celso ; Liljeroth, Peter ; Vanmaekelbergh, Daniel</creatorcontrib><description>The quintessence of the hot‐injection method, a synthesis route for monodisperse, highly luminescent semiconductor nanocrystals, is reviewed. The separate stages of nucleation and growth of the nanocrystals are discussed in the framework of classical nucleation theory and an equilibrium model proposed by Debye. We also review the numerous adaptations of the original synthesis that currently provide colloidal nanocrystals with well‐defined, size‐dependent optical, electrical, and magnetic properties. The availability of these remarkable materials is one of the most promising developments in nanoscience and nanotechnology.
Suspensions of monodisperse, highly luminescent nanocrystals are currently prepared by a hot‐injection method. Due to their size‐dependent optoelectronic properties, such nanocrystals are of enormous interest. In this Review, we examine whether we can understand the results of this method at the atomic level. We also review adaptations to this method that have been proposed to prepare a variety of semiconductor and magnetic nanocrystals.</description><identifier>ISSN: 1613-6810</identifier><identifier>EISSN: 1613-6829</identifier><identifier>DOI: 10.1002/smll.200500239</identifier><identifier>PMID: 17193409</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>Cadmium Compounds - chemistry ; Chemistry, Physical - methods ; Electrochemistry - instrumentation ; Electrochemistry - methods ; Hot Temperature ; Kinetics ; Models, Chemical ; nanocrystals ; Nanoparticles - chemistry ; nanoscience ; Nanotechnology - instrumentation ; Nanotechnology - methods ; Quantum Dots ; Selenium Compounds - chemistry ; Semiconductors ; Surface Properties ; synthetic methods ; Temperature ; Thermodynamics ; Ultraviolet Rays</subject><ispartof>Small (Weinheim an der Bergstrasse, Germany), 2005-12, Vol.1 (12), p.1152-1162</ispartof><rights>Copyright © 2005 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4879-318cebe2ad00d4a6298376f1103660c8a26ab487887ed5c468a4d5acb0a411a23</citedby><cites>FETCH-LOGICAL-c4879-318cebe2ad00d4a6298376f1103660c8a26ab487887ed5c468a4d5acb0a411a23</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fsmll.200500239$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fsmll.200500239$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17193409$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>de Mello Donegá, Celso</creatorcontrib><creatorcontrib>Liljeroth, Peter</creatorcontrib><creatorcontrib>Vanmaekelbergh, Daniel</creatorcontrib><title>Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals</title><title>Small (Weinheim an der Bergstrasse, Germany)</title><addtitle>Small</addtitle><description>The quintessence of the hot‐injection method, a synthesis route for monodisperse, highly luminescent semiconductor nanocrystals, is reviewed. The separate stages of nucleation and growth of the nanocrystals are discussed in the framework of classical nucleation theory and an equilibrium model proposed by Debye. We also review the numerous adaptations of the original synthesis that currently provide colloidal nanocrystals with well‐defined, size‐dependent optical, electrical, and magnetic properties. The availability of these remarkable materials is one of the most promising developments in nanoscience and nanotechnology.
Suspensions of monodisperse, highly luminescent nanocrystals are currently prepared by a hot‐injection method. Due to their size‐dependent optoelectronic properties, such nanocrystals are of enormous interest. In this Review, we examine whether we can understand the results of this method at the atomic level. We also review adaptations to this method that have been proposed to prepare a variety of semiconductor and magnetic nanocrystals.</description><subject>Cadmium Compounds - chemistry</subject><subject>Chemistry, Physical - methods</subject><subject>Electrochemistry - instrumentation</subject><subject>Electrochemistry - methods</subject><subject>Hot Temperature</subject><subject>Kinetics</subject><subject>Models, Chemical</subject><subject>nanocrystals</subject><subject>Nanoparticles - chemistry</subject><subject>nanoscience</subject><subject>Nanotechnology - instrumentation</subject><subject>Nanotechnology - methods</subject><subject>Quantum Dots</subject><subject>Selenium Compounds - chemistry</subject><subject>Semiconductors</subject><subject>Surface Properties</subject><subject>synthetic methods</subject><subject>Temperature</subject><subject>Thermodynamics</subject><subject>Ultraviolet Rays</subject><issn>1613-6810</issn><issn>1613-6829</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkE1v1DAQhq0K1JbSK0fkE6dm8UfWdo6o6peULVULVOrFmnUmrEsSb-0EyL8nZVcLt55mxn7e5_AS8o6zGWdMfExt08wEY_PpkMUeOeSKy0wZUbza7ZwdkDcpPTImucj1PjngmhcyZ8Uh-X6zGpN3wa2w9Q4aevYTmgF6HzoaatqvkF6GPrvqHtH9fVxgvwrVCQV6N3bTd_KJ3oahR1qHSBehC5VPa4wJ6TV0wcUx9dCkt-R1PQ083s4j8vX87MvpZVZ-vrg6_VRmLje6yCQ3DpcooGKsykGJwkitas6ZVIo5A0LBciKN0VjNXa4M5NUc3JJBzjkIeUQ-bLzrGJ4GTL1tfXLYNNBhGJLVjBshtJzA2QZ0MaQUsbbr6FuIo-XMPldrn6u1u2qnwPuteVi2WP3Dt11OQLEBfvkGxxd09m5Rlv_Ls03Wpx5_77IQf1ilpZ7b--sLe1_ePuTf9OSTfwB8V5Xk</recordid><startdate>200512</startdate><enddate>200512</enddate><creator>de Mello Donegá, Celso</creator><creator>Liljeroth, Peter</creator><creator>Vanmaekelbergh, Daniel</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>200512</creationdate><title>Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals</title><author>de Mello Donegá, Celso ; Liljeroth, Peter ; Vanmaekelbergh, Daniel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4879-318cebe2ad00d4a6298376f1103660c8a26ab487887ed5c468a4d5acb0a411a23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Cadmium Compounds - chemistry</topic><topic>Chemistry, Physical - methods</topic><topic>Electrochemistry - instrumentation</topic><topic>Electrochemistry - methods</topic><topic>Hot Temperature</topic><topic>Kinetics</topic><topic>Models, Chemical</topic><topic>nanocrystals</topic><topic>Nanoparticles - chemistry</topic><topic>nanoscience</topic><topic>Nanotechnology - instrumentation</topic><topic>Nanotechnology - methods</topic><topic>Quantum Dots</topic><topic>Selenium Compounds - chemistry</topic><topic>Semiconductors</topic><topic>Surface Properties</topic><topic>synthetic methods</topic><topic>Temperature</topic><topic>Thermodynamics</topic><topic>Ultraviolet Rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>de Mello Donegá, Celso</creatorcontrib><creatorcontrib>Liljeroth, Peter</creatorcontrib><creatorcontrib>Vanmaekelbergh, Daniel</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Small (Weinheim an der Bergstrasse, Germany)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>de Mello Donegá, Celso</au><au>Liljeroth, Peter</au><au>Vanmaekelbergh, Daniel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals</atitle><jtitle>Small (Weinheim an der Bergstrasse, Germany)</jtitle><addtitle>Small</addtitle><date>2005-12</date><risdate>2005</risdate><volume>1</volume><issue>12</issue><spage>1152</spage><epage>1162</epage><pages>1152-1162</pages><issn>1613-6810</issn><eissn>1613-6829</eissn><abstract>The quintessence of the hot‐injection method, a synthesis route for monodisperse, highly luminescent semiconductor nanocrystals, is reviewed. The separate stages of nucleation and growth of the nanocrystals are discussed in the framework of classical nucleation theory and an equilibrium model proposed by Debye. We also review the numerous adaptations of the original synthesis that currently provide colloidal nanocrystals with well‐defined, size‐dependent optical, electrical, and magnetic properties. The availability of these remarkable materials is one of the most promising developments in nanoscience and nanotechnology.
Suspensions of monodisperse, highly luminescent nanocrystals are currently prepared by a hot‐injection method. Due to their size‐dependent optoelectronic properties, such nanocrystals are of enormous interest. In this Review, we examine whether we can understand the results of this method at the atomic level. We also review adaptations to this method that have been proposed to prepare a variety of semiconductor and magnetic nanocrystals.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><pmid>17193409</pmid><doi>10.1002/smll.200500239</doi><tpages>11</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1613-6810 |
| ispartof | Small (Weinheim an der Bergstrasse, Germany), 2005-12, Vol.1 (12), p.1152-1162 |
| issn | 1613-6810 1613-6829 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_70182273 |
| source | MEDLINE; Wiley Online Library All Journals |
| subjects | Cadmium Compounds - chemistry Chemistry, Physical - methods Electrochemistry - instrumentation Electrochemistry - methods Hot Temperature Kinetics Models, Chemical nanocrystals Nanoparticles - chemistry nanoscience Nanotechnology - instrumentation Nanotechnology - methods Quantum Dots Selenium Compounds - chemistry Semiconductors Surface Properties synthetic methods Temperature Thermodynamics Ultraviolet Rays |
| title | Physicochemical Evaluation of the Hot-Injection Method, a Synthesis Route for Monodisperse Nanocrystals |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-06T10%3A52%3A36IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Physicochemical%20Evaluation%20of%20the%20Hot-Injection%20Method,%20a%20Synthesis%20Route%20for%20Monodisperse%20Nanocrystals&rft.jtitle=Small%20(Weinheim%20an%20der%20Bergstrasse,%20Germany)&rft.au=de%E2%80%85Mello%E2%80%85Doneg%C3%A1,%20Celso&rft.date=2005-12&rft.volume=1&rft.issue=12&rft.spage=1152&rft.epage=1162&rft.pages=1152-1162&rft.issn=1613-6810&rft.eissn=1613-6829&rft_id=info:doi/10.1002/smll.200500239&rft_dat=%3Cproquest_cross%3E70182273%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=70182273&rft_id=info:pmid/17193409&rfr_iscdi=true |