Quantitative determination of anti-tumor agent bis(4-fluorobenzyl)trisulfide, fluorapacin and its pharmaceutical preparation by high-performance liquid chromatography

A simple isocratic and stability-indicating HPLC method was developed and validated for the quantitative determination of anti-tumor agent fluorapacin and its pharmaceutical preparation. A Spherisorb ODS II C 18 (250 mm × 4.6 mm, 5 μm) column was eluted with a mobile phase consisting of acetonitrile...

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Veröffentlicht in:	Journal of pharmaceutical and biomedical analysis 2008-01, Vol.46 (1), p.206-210
Hauptverfasser:	Bao, Yimei, He, Yuyu, Xu, Xiaoying, Mo, Xiaopeng, Xu, Xiao, Wang, Xiaobo, An, Haoyun
Format:	Artikel
Sprache:	eng
Schlagworte:	alpha-Tocopherol - analysis alpha-Tocopherol - chemistry Analysis Analytical method Analytical, structural and metabolic biochemistry Antineoplastic Agents - analysis Antineoplastic Agents - chemistry Biological and medical sciences Calibration Chromatography, High Pressure Liquid - methods Drug Stability Ethanol - analysis Ethanol - chemistry Fluorapacin Fluorobenzenes - analysis Fluorobenzenes - chemistry Fundamental and applied biological sciences. Psychology General pharmacology Glycerol - analogs & derivatives Glycerol - analysis Glycerol - chemistry HPLC Isocratic Medical sciences Molecular Structure Pharmaceutical preparation Pharmaceutical Preparations - analysis Pharmaceutical Preparations - chemistry Pharmacology. Drug treatments Quality Control Quantitative determination Reproducibility of Results Sulfides - analysis Sulfides - chemistry Technology, Pharmaceutical - methods
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