Development of saw palmetto (Serenoa repens) fruit and extract standard reference materials
As part of a collaboration with the National Institutes of Health's Office of Dietary Supplements and the Food and Drug Administration's Center for Drug Evaluation and Research, the National Institute of Standards and Technology has developed two standard reference materials (SRMs) represe...
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2008-10, Vol.392 (3), p.427-438 |
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| creator | Schantz, Michele M Bedner, Mary Long, Stephen E Molloy, John L Murphy, Karen E Porter, Barbara J Putzbach, Karsten Rimmer, Catherine A Sander, Lane C Sharpless, Katherine E Thomas, Jeanice B Wise, Stephen A Wood, Laura J Yen, James H Yarita, Takashi NguyenPho, Agnes Sorenson, Wendy R Betz, Joseph M |
| description | As part of a collaboration with the National Institutes of Health's Office of Dietary Supplements and the Food and Drug Administration's Center for Drug Evaluation and Research, the National Institute of Standards and Technology has developed two standard reference materials (SRMs) representing different forms of saw palmetto (Serenoa repens), SRM 3250 Serenoa repens fruit and SRM 3251 Serenoa repens extract. Both of these SRMs have been characterized for their fatty acid and phytosterol content. The fatty acid concentration values are based on results from gas chromatography with flame ionization detection (GC-FID) and mass spectrometry (GC/MS) analysis while the sterol concentration values are based on results from GC-FID and liquid chromatography with mass spectrometry analysis. In addition, SRM 3250 has been characterized for lead content, and SRM 3251 has been characterized for the content of β-carotene and tocopherols. SRM 3250 (fruit) has certified concentration values for three phytosterols, 14 fatty acids as triglycerides, and lead along with reference concentration values for four fatty acids as triglycerides and 16 free fatty acids. SRM 3251 (extract) has certified concentration values for three phytosterols, 17 fatty acids as triglycerides, β-carotene, and γ-tocopherol along with reference concentration values for three fatty acids as triglycerides, 17 fatty acids as free fatty acids, β-carotene isomers, and δ-tocopherol and information values for two phytosterols. These SRMs will complement other reference materials currently available with concentrations for similar analytes and are part of a series of SRMs being developed for dietary supplements. |
| doi_str_mv | 10.1007/s00216-008-2297-0 |
| format | Article |
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Both of these SRMs have been characterized for their fatty acid and phytosterol content. The fatty acid concentration values are based on results from gas chromatography with flame ionization detection (GC-FID) and mass spectrometry (GC/MS) analysis while the sterol concentration values are based on results from GC-FID and liquid chromatography with mass spectrometry analysis. In addition, SRM 3250 has been characterized for lead content, and SRM 3251 has been characterized for the content of β-carotene and tocopherols. SRM 3250 (fruit) has certified concentration values for three phytosterols, 14 fatty acids as triglycerides, and lead along with reference concentration values for four fatty acids as triglycerides and 16 free fatty acids. SRM 3251 (extract) has certified concentration values for three phytosterols, 17 fatty acids as triglycerides, β-carotene, and γ-tocopherol along with reference concentration values for three fatty acids as triglycerides, 17 fatty acids as free fatty acids, β-carotene isomers, and δ-tocopherol and information values for two phytosterols. These SRMs will complement other reference materials currently available with concentrations for similar analytes and are part of a series of SRMs being developed for dietary supplements.</description><identifier>ISSN: 1618-2642</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-008-2297-0</identifier><identifier>PMID: 18677464</identifier><language>eng</language><publisher>Berlin/Heidelberg: Berlin/Heidelberg : Springer-Verlag</publisher><subject>Analytical Chemistry ; beta Carotene - analysis ; Biochemistry ; Certified reference material ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; fatty acids ; Fatty Acids - analysis ; Food Science ; Fruit - chemistry ; Laboratory Medicine ; Monitoring/Environmental Analysis ; Original Paper ; phytosterols ; Plant Extracts - analysis ; Plant Extracts - chemistry ; Reference Standards ; Serenoa - chemistry ; Serenoa repens ; Standard reference material ; Sterols - analysis ; Tocopherols - chemistry</subject><ispartof>Analytical and bioanalytical chemistry, 2008-10, Vol.392 (3), p.427-438</ispartof><rights>Springer-Verlag 2008</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c397t-9f55ad7aa4555135f31910fe9c60b311eaf47289d12c7c2dbc99269b01ad247a3</citedby><cites>FETCH-LOGICAL-c397t-9f55ad7aa4555135f31910fe9c60b311eaf47289d12c7c2dbc99269b01ad247a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00216-008-2297-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00216-008-2297-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/18677464$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Schantz, Michele M</creatorcontrib><creatorcontrib>Bedner, Mary</creatorcontrib><creatorcontrib>Long, Stephen E</creatorcontrib><creatorcontrib>Molloy, John L</creatorcontrib><creatorcontrib>Murphy, Karen E</creatorcontrib><creatorcontrib>Porter, Barbara J</creatorcontrib><creatorcontrib>Putzbach, Karsten</creatorcontrib><creatorcontrib>Rimmer, Catherine A</creatorcontrib><creatorcontrib>Sander, Lane C</creatorcontrib><creatorcontrib>Sharpless, Katherine E</creatorcontrib><creatorcontrib>Thomas, Jeanice B</creatorcontrib><creatorcontrib>Wise, Stephen A</creatorcontrib><creatorcontrib>Wood, Laura J</creatorcontrib><creatorcontrib>Yen, James H</creatorcontrib><creatorcontrib>Yarita, Takashi</creatorcontrib><creatorcontrib>NguyenPho, Agnes</creatorcontrib><creatorcontrib>Sorenson, Wendy R</creatorcontrib><creatorcontrib>Betz, Joseph M</creatorcontrib><title>Development of saw palmetto (Serenoa repens) fruit and extract standard reference materials</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>As part of a collaboration with the National Institutes of Health's Office of Dietary Supplements and the Food and Drug Administration's Center for Drug Evaluation and Research, the National Institute of Standards and Technology has developed two standard reference materials (SRMs) representing different forms of saw palmetto (Serenoa repens), SRM 3250 Serenoa repens fruit and SRM 3251 Serenoa repens extract. Both of these SRMs have been characterized for their fatty acid and phytosterol content. The fatty acid concentration values are based on results from gas chromatography with flame ionization detection (GC-FID) and mass spectrometry (GC/MS) analysis while the sterol concentration values are based on results from GC-FID and liquid chromatography with mass spectrometry analysis. In addition, SRM 3250 has been characterized for lead content, and SRM 3251 has been characterized for the content of β-carotene and tocopherols. SRM 3250 (fruit) has certified concentration values for three phytosterols, 14 fatty acids as triglycerides, and lead along with reference concentration values for four fatty acids as triglycerides and 16 free fatty acids. SRM 3251 (extract) has certified concentration values for three phytosterols, 17 fatty acids as triglycerides, β-carotene, and γ-tocopherol along with reference concentration values for three fatty acids as triglycerides, 17 fatty acids as free fatty acids, β-carotene isomers, and δ-tocopherol and information values for two phytosterols. 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Both of these SRMs have been characterized for their fatty acid and phytosterol content. The fatty acid concentration values are based on results from gas chromatography with flame ionization detection (GC-FID) and mass spectrometry (GC/MS) analysis while the sterol concentration values are based on results from GC-FID and liquid chromatography with mass spectrometry analysis. In addition, SRM 3250 has been characterized for lead content, and SRM 3251 has been characterized for the content of β-carotene and tocopherols. SRM 3250 (fruit) has certified concentration values for three phytosterols, 14 fatty acids as triglycerides, and lead along with reference concentration values for four fatty acids as triglycerides and 16 free fatty acids. SRM 3251 (extract) has certified concentration values for three phytosterols, 17 fatty acids as triglycerides, β-carotene, and γ-tocopherol along with reference concentration values for three fatty acids as triglycerides, 17 fatty acids as free fatty acids, β-carotene isomers, and δ-tocopherol and information values for two phytosterols. These SRMs will complement other reference materials currently available with concentrations for similar analytes and are part of a series of SRMs being developed for dietary supplements.</abstract><cop>Berlin/Heidelberg</cop><pub>Berlin/Heidelberg : Springer-Verlag</pub><pmid>18677464</pmid><doi>10.1007/s00216-008-2297-0</doi><tpages>12</tpages></addata></record> |
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| subjects | Analytical Chemistry beta Carotene - analysis Biochemistry Certified reference material Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science fatty acids Fatty Acids - analysis Food Science Fruit - chemistry Laboratory Medicine Monitoring/Environmental Analysis Original Paper phytosterols Plant Extracts - analysis Plant Extracts - chemistry Reference Standards Serenoa - chemistry Serenoa repens Standard reference material Sterols - analysis Tocopherols - chemistry |
| title | Development of saw palmetto (Serenoa repens) fruit and extract standard reference materials |
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