Characterisation of hydrolysable tannins from leaves of Betula pubescens by high-performance liquid chromatography–mass spectrometry
A high-performance liquid chromatography–electrospray ionisation mass spectrometry (HPLC–ESI-MS) method, assisted by diode array detection, for the characterisation of individual hydrolysable tannins in birch leaves was developed. With the method, it was found that birch ( Betula pubescens) leaves c...
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| Veröffentlicht in: | Journal of Chromatography A 1999-12, Vol.864 (2), p.283-291 |
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| container_end_page | 291 |
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| container_issue | 2 |
| container_start_page | 283 |
| container_title | Journal of Chromatography A |
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| creator | Salminen, J.-P Ossipov, V Loponen, J Haukioja, E Pihlaja, K |
| description | A high-performance liquid chromatography–electrospray ionisation mass spectrometry (HPLC–ESI-MS) method, assisted by diode array detection, for the characterisation of individual hydrolysable tannins in birch leaves was developed. With the method, it was found that birch (
Betula pubescens) leaves contained an exceptionally complex mixture of hydrolysable tannins; 14 gallotannins and 20 ellagitannins were identified. The developed HPLC–ESI-MS method allows the qualitative and quantitative determination of individual gallotannins and ellagitannins directly from crude birch leaf extract. This is important in studying ecological functions of these phenolic compounds, especially their role in the resistance of birch leaves against insects. |
| doi_str_mv | 10.1016/S0021-9673(99)01036-5 |
| format | Article |
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Betula pubescens) leaves contained an exceptionally complex mixture of hydrolysable tannins; 14 gallotannins and 20 ellagitannins were identified. The developed HPLC–ESI-MS method allows the qualitative and quantitative determination of individual gallotannins and ellagitannins directly from crude birch leaf extract. This is important in studying ecological functions of these phenolic compounds, especially their role in the resistance of birch leaves against insects.</description><identifier>ISSN: 0021-9673</identifier><identifier>DOI: 10.1016/S0021-9673(99)01036-5</identifier><identifier>PMID: 10669296</identifier><identifier>CODEN: JOCRAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Biological and medical sciences ; Chemical constitution ; Chromatography, High Pressure Liquid ; Ellagitannins ; Fundamental and applied biological sciences. Psychology ; Gallotannins ; Gas Chromatography-Mass Spectrometry ; Hydrolysable tannins ; Hydrolysis ; Indicators and Reagents ; Mass Spectrometry ; Plant Extracts - chemistry ; Plant Leaves - chemistry ; Plant physiology and development ; Reference Standards ; Solvents ; Spectrophotometry, Ultraviolet ; Tannins - analysis</subject><ispartof>Journal of Chromatography A, 1999-12, Vol.864 (2), p.283-291</ispartof><rights>1999 Elsevier Science B.V.</rights><rights>2000 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c442t-42efb832486b20f7ae5af40ceebf22bd084e125a2ad1fe762c41fe8c041136fd3</citedby><cites>FETCH-LOGICAL-c442t-42efb832486b20f7ae5af40ceebf22bd084e125a2ad1fe762c41fe8c041136fd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S0021-9673(99)01036-5$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1265648$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/10669296$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Salminen, J.-P</creatorcontrib><creatorcontrib>Ossipov, V</creatorcontrib><creatorcontrib>Loponen, J</creatorcontrib><creatorcontrib>Haukioja, E</creatorcontrib><creatorcontrib>Pihlaja, K</creatorcontrib><title>Characterisation of hydrolysable tannins from leaves of Betula pubescens by high-performance liquid chromatography–mass spectrometry</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>A high-performance liquid chromatography–electrospray ionisation mass spectrometry (HPLC–ESI-MS) method, assisted by diode array detection, for the characterisation of individual hydrolysable tannins in birch leaves was developed. With the method, it was found that birch (
Betula pubescens) leaves contained an exceptionally complex mixture of hydrolysable tannins; 14 gallotannins and 20 ellagitannins were identified. The developed HPLC–ESI-MS method allows the qualitative and quantitative determination of individual gallotannins and ellagitannins directly from crude birch leaf extract. This is important in studying ecological functions of these phenolic compounds, especially their role in the resistance of birch leaves against insects.</description><subject>Biological and medical sciences</subject><subject>Chemical constitution</subject><subject>Chromatography, High Pressure Liquid</subject><subject>Ellagitannins</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Gallotannins</subject><subject>Gas Chromatography-Mass Spectrometry</subject><subject>Hydrolysable tannins</subject><subject>Hydrolysis</subject><subject>Indicators and Reagents</subject><subject>Mass Spectrometry</subject><subject>Plant Extracts - chemistry</subject><subject>Plant Leaves - chemistry</subject><subject>Plant physiology and development</subject><subject>Reference Standards</subject><subject>Solvents</subject><subject>Spectrophotometry, Ultraviolet</subject><subject>Tannins - analysis</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1999</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkM1u1TAQRr0AtaXlEUBeIASLFNtxnGSF4Io_qRILYG1NnHFjlMSp7VTKjhUv0DfkSfDtvQJ2rEaaOd_M6BDyhLNLzrh69YUxwYtW1eWLtn3JOCtVUT0gZ3_ap-RRjN8Z4zWrxQk55UypVrTqjPzcDRDAJAwuQnJ-pt7SYeuDH7cI3Yg0wTy7OVIb_ERHhFuMe-YtpnUEuqwdRoN53m10cNdDsWCwPkwwG6Sju1ldT82Qs5D8dYBl2H79uJsgRhoXNCkPMIXtgjy0MEZ8fKzn5Nv7d193H4urzx8-7d5cFUZKkQop0HZNKWSjOsFsDViBlcwgdlaIrmeNRC4qENBzi7USRubaGCY5L5Xty3Py_LB3Cf5mxZj05PL74wgz-jVq1UrRlKrNYHUATfAxBrR6CW6CsGnO9F66vpeu93Z12-p76brKuafHA2s3Yf9P6mA8A8-OAEQDow1ZlIt_OaEqJZuMvT5gmG3cOgw6GofZae9C1qZ77_7zyW_fAqXA</recordid><startdate>19991224</startdate><enddate>19991224</enddate><creator>Salminen, J.-P</creator><creator>Ossipov, V</creator><creator>Loponen, J</creator><creator>Haukioja, E</creator><creator>Pihlaja, K</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>19991224</creationdate><title>Characterisation of hydrolysable tannins from leaves of Betula pubescens by high-performance liquid chromatography–mass spectrometry</title><author>Salminen, J.-P ; Ossipov, V ; Loponen, J ; Haukioja, E ; Pihlaja, K</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c442t-42efb832486b20f7ae5af40ceebf22bd084e125a2ad1fe762c41fe8c041136fd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1999</creationdate><topic>Biological and medical sciences</topic><topic>Chemical constitution</topic><topic>Chromatography, High Pressure Liquid</topic><topic>Ellagitannins</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Gallotannins</topic><topic>Gas Chromatography-Mass Spectrometry</topic><topic>Hydrolysable tannins</topic><topic>Hydrolysis</topic><topic>Indicators and Reagents</topic><topic>Mass Spectrometry</topic><topic>Plant Extracts - chemistry</topic><topic>Plant Leaves - chemistry</topic><topic>Plant physiology and development</topic><topic>Reference Standards</topic><topic>Solvents</topic><topic>Spectrophotometry, Ultraviolet</topic><topic>Tannins - analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Salminen, J.-P</creatorcontrib><creatorcontrib>Ossipov, V</creatorcontrib><creatorcontrib>Loponen, J</creatorcontrib><creatorcontrib>Haukioja, E</creatorcontrib><creatorcontrib>Pihlaja, K</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Salminen, J.-P</au><au>Ossipov, V</au><au>Loponen, J</au><au>Haukioja, E</au><au>Pihlaja, K</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterisation of hydrolysable tannins from leaves of Betula pubescens by high-performance liquid chromatography–mass spectrometry</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>1999-12-24</date><risdate>1999</risdate><volume>864</volume><issue>2</issue><spage>283</spage><epage>291</epage><pages>283-291</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>A high-performance liquid chromatography–electrospray ionisation mass spectrometry (HPLC–ESI-MS) method, assisted by diode array detection, for the characterisation of individual hydrolysable tannins in birch leaves was developed. With the method, it was found that birch (
Betula pubescens) leaves contained an exceptionally complex mixture of hydrolysable tannins; 14 gallotannins and 20 ellagitannins were identified. The developed HPLC–ESI-MS method allows the qualitative and quantitative determination of individual gallotannins and ellagitannins directly from crude birch leaf extract. This is important in studying ecological functions of these phenolic compounds, especially their role in the resistance of birch leaves against insects.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>10669296</pmid><doi>10.1016/S0021-9673(99)01036-5</doi><tpages>9</tpages></addata></record> |
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| subjects | Biological and medical sciences Chemical constitution Chromatography, High Pressure Liquid Ellagitannins Fundamental and applied biological sciences. Psychology Gallotannins Gas Chromatography-Mass Spectrometry Hydrolysable tannins Hydrolysis Indicators and Reagents Mass Spectrometry Plant Extracts - chemistry Plant Leaves - chemistry Plant physiology and development Reference Standards Solvents Spectrophotometry, Ultraviolet Tannins - analysis |
| title | Characterisation of hydrolysable tannins from leaves of Betula pubescens by high-performance liquid chromatography–mass spectrometry |
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