SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples

Continuous wave irradiation has limited bandwidth for heteronuclear 1H decoupling at high fields and for 13C decoupling in 1H/ 13C/ 15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of 1H and 13C heteronuclear decoupling on single crystals of peptides and on m...

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Veröffentlicht in:	Journal of magnetic resonance (1997) 2005-12, Vol.177 (2), p.197-202
Hauptverfasser:	Sinha, Neeraj, Grant, Christopher V., Wu, Chin H., De Angelis, Anna A., Howell, Stanley C., Opella, Stanley J.
Format:	Artikel
Sprache:	eng
Schlagworte:	900 MHz Aligned samples Bacteriophages - chemistry Carbon Isotopes Decoupling Glycine - analogs & derivatives Glycine - chemistry Hydrogen Bonding Nitrogen Isotopes Nuclear Magnetic Resonance, Biomolecular - methods Peptides - chemistry Single crystals SPINAL
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