SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples
Continuous wave irradiation has limited bandwidth for heteronuclear 1H decoupling at high fields and for 13C decoupling in 1H/ 13C/ 15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of 1H and 13C heteronuclear decoupling on single crystals of peptides and on m...
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| Veröffentlicht in: | Journal of magnetic resonance (1997) 2005-12, Vol.177 (2), p.197-202 |
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| container_issue | 2 |
| container_start_page | 197 |
| container_title | Journal of magnetic resonance (1997) |
| container_volume | 177 |
| creator | Sinha, Neeraj Grant, Christopher V. Wu, Chin H. De Angelis, Anna A. Howell, Stanley C. Opella, Stanley J. |
| description | Continuous wave irradiation has limited bandwidth for heteronuclear
1H decoupling at high fields and for
13C decoupling in
1H/
13C/
15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of
1H and
13C heteronuclear decoupling on single crystals of peptides and on magnetically aligned samples of membrane proteins in bicelles, which is of particular importance because aqueous samples of biomolecules are lossy at high fields, which limits the strengths of the RF fields that can be applied. |
| doi_str_mv | 10.1016/j.jmr.2005.07.008 |
| format | Article |
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1H decoupling at high fields and for
13C decoupling in
1H/
13C/
15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of
1H and
13C heteronuclear decoupling on single crystals of peptides and on magnetically aligned samples of membrane proteins in bicelles, which is of particular importance because aqueous samples of biomolecules are lossy at high fields, which limits the strengths of the RF fields that can be applied.</description><identifier>ISSN: 1090-7807</identifier><identifier>EISSN: 1096-0856</identifier><identifier>DOI: 10.1016/j.jmr.2005.07.008</identifier><identifier>PMID: 16137902</identifier><language>eng</language><publisher>United States: Elsevier Inc</publisher><subject>900 MHz ; Aligned samples ; Bacteriophages - chemistry ; Carbon Isotopes ; Decoupling ; Glycine - analogs & derivatives ; Glycine - chemistry ; Hydrogen Bonding ; Nitrogen Isotopes ; Nuclear Magnetic Resonance, Biomolecular - methods ; Peptides - chemistry ; Single crystals ; SPINAL</subject><ispartof>Journal of magnetic resonance (1997), 2005-12, Vol.177 (2), p.197-202</ispartof><rights>2005 Elsevier Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c351t-dc185d86417fbb04b3a91da7186f2c82292605fd68fbd4e0f2c3370ad48e9b243</citedby><cites>FETCH-LOGICAL-c351t-dc185d86417fbb04b3a91da7186f2c82292605fd68fbd4e0f2c3370ad48e9b243</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1090780705002351$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/16137902$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Sinha, Neeraj</creatorcontrib><creatorcontrib>Grant, Christopher V.</creatorcontrib><creatorcontrib>Wu, Chin H.</creatorcontrib><creatorcontrib>De Angelis, Anna A.</creatorcontrib><creatorcontrib>Howell, Stanley C.</creatorcontrib><creatorcontrib>Opella, Stanley J.</creatorcontrib><title>SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples</title><title>Journal of magnetic resonance (1997)</title><addtitle>J Magn Reson</addtitle><description>Continuous wave irradiation has limited bandwidth for heteronuclear
1H decoupling at high fields and for
13C decoupling in
1H/
13C/
15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of
1H and
13C heteronuclear decoupling on single crystals of peptides and on magnetically aligned samples of membrane proteins in bicelles, which is of particular importance because aqueous samples of biomolecules are lossy at high fields, which limits the strengths of the RF fields that can be applied.</description><subject>900 MHz</subject><subject>Aligned samples</subject><subject>Bacteriophages - chemistry</subject><subject>Carbon Isotopes</subject><subject>Decoupling</subject><subject>Glycine - analogs & derivatives</subject><subject>Glycine - chemistry</subject><subject>Hydrogen Bonding</subject><subject>Nitrogen Isotopes</subject><subject>Nuclear Magnetic Resonance, Biomolecular - methods</subject><subject>Peptides - chemistry</subject><subject>Single crystals</subject><subject>SPINAL</subject><issn>1090-7807</issn><issn>1096-0856</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kE1P3DAQhq0KVGDbH9BL5RO3pON82I56QgjoSsuH-nG2HHsCXiVxaicI_n297Eq9cZrRzPu-mnkI-cIgZ8D4t22-HUJeANQ5iBxAfiCnDBqegaz50VsPmZAgTshZjFsAxmoBH8kJ46wUDRSn5OXXw_ruYkMHb5dez2ipReOXqXfjI3UjfXKPT7Rz2KeFX9oeM6pHS-fgptQHjH7Uo0Eafe9sFucUQe9uf1J8mTC4Acc5Uj_S3cIlaXilUQ_JGj-R4073ET8f6or8ub76ffkj29zfrC8vNpkpazZn1jBZW8krJrq2haotdcOsFkzyrjCyKJqCQ91ZLrvWVghpWJYCtK0kNm1RlStyvs-dgv-7YJzV4KLBvtcj-iUqLmXZMNEkIdsLTfAxBuzUlB5IFysGaodbbVXCrXa4FQiVcCfP10P40g5o_zsOfJPg-16A6cVnh0FF4zABsy6gmZX17p34f2HNkcE</recordid><startdate>20051201</startdate><enddate>20051201</enddate><creator>Sinha, Neeraj</creator><creator>Grant, Christopher V.</creator><creator>Wu, Chin H.</creator><creator>De Angelis, Anna A.</creator><creator>Howell, Stanley C.</creator><creator>Opella, Stanley J.</creator><general>Elsevier Inc</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20051201</creationdate><title>SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples</title><author>Sinha, Neeraj ; Grant, Christopher V. ; Wu, Chin H. ; De Angelis, Anna A. ; Howell, Stanley C. ; Opella, Stanley J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c351t-dc185d86417fbb04b3a91da7186f2c82292605fd68fbd4e0f2c3370ad48e9b243</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>900 MHz</topic><topic>Aligned samples</topic><topic>Bacteriophages - chemistry</topic><topic>Carbon Isotopes</topic><topic>Decoupling</topic><topic>Glycine - analogs & derivatives</topic><topic>Glycine - chemistry</topic><topic>Hydrogen Bonding</topic><topic>Nitrogen Isotopes</topic><topic>Nuclear Magnetic Resonance, Biomolecular - methods</topic><topic>Peptides - chemistry</topic><topic>Single crystals</topic><topic>SPINAL</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sinha, Neeraj</creatorcontrib><creatorcontrib>Grant, Christopher V.</creatorcontrib><creatorcontrib>Wu, Chin H.</creatorcontrib><creatorcontrib>De Angelis, Anna A.</creatorcontrib><creatorcontrib>Howell, Stanley C.</creatorcontrib><creatorcontrib>Opella, Stanley J.</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of magnetic resonance (1997)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sinha, Neeraj</au><au>Grant, Christopher V.</au><au>Wu, Chin H.</au><au>De Angelis, Anna A.</au><au>Howell, Stanley C.</au><au>Opella, Stanley J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples</atitle><jtitle>Journal of magnetic resonance (1997)</jtitle><addtitle>J Magn Reson</addtitle><date>2005-12-01</date><risdate>2005</risdate><volume>177</volume><issue>2</issue><spage>197</spage><epage>202</epage><pages>197-202</pages><issn>1090-7807</issn><eissn>1096-0856</eissn><abstract>Continuous wave irradiation has limited bandwidth for heteronuclear
1H decoupling at high fields and for
13C decoupling in
1H/
13C/
15N triple-resonance experiments. SPINAL-16 modulation is shown to improve the efficiency of
1H and
13C heteronuclear decoupling on single crystals of peptides and on magnetically aligned samples of membrane proteins in bicelles, which is of particular importance because aqueous samples of biomolecules are lossy at high fields, which limits the strengths of the RF fields that can be applied.</abstract><cop>United States</cop><pub>Elsevier Inc</pub><pmid>16137902</pmid><doi>10.1016/j.jmr.2005.07.008</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1090-7807 |
| ispartof | Journal of magnetic resonance (1997), 2005-12, Vol.177 (2), p.197-202 |
| issn | 1090-7807 1096-0856 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_68839179 |
| source | MEDLINE; Elsevier ScienceDirect Journals Complete |
| subjects | 900 MHz Aligned samples Bacteriophages - chemistry Carbon Isotopes Decoupling Glycine - analogs & derivatives Glycine - chemistry Hydrogen Bonding Nitrogen Isotopes Nuclear Magnetic Resonance, Biomolecular - methods Peptides - chemistry Single crystals SPINAL |
| title | SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples |
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