Premelting at Defects Within Bulk Colloidal Crystals
Premelting is the localized loss of crystalline order at surfaces and defects at temperatures below the bulk melting transition. It can be thought of as the nucleation of the melting process. Premelting has been observed at the surfaces of crystals but not within. We report observations of premeltin...
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| Veröffentlicht in: | Science (American Association for the Advancement of Science) 2005-08, Vol.309 (5738), p.1207-1210 |
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| creator | Alsayed, A. M Islam, M. F Zhang, J Collings, P. J Yodh, A. G |
| description | Premelting is the localized loss of crystalline order at surfaces and defects at temperatures below the bulk melting transition. It can be thought of as the nucleation of the melting process. Premelting has been observed at the surfaces of crystals but not within. We report observations of premelting at grain boundaries and dislocations within bulk colloidal crystals using real-time video microscopy. The crystals are equilibrium close-packed, three-dimensional colloidal structures made from thermally responsive microgel spheres. Particle tracking reveals increased disorder in crystalline regions bordering defects, the amount of which depends on the type of defect, distance from the defect, and particle volume fraction. Our observations suggest that interfacial free energy is the crucial parameter for premelting in colloidal and atomic-scale crystals. |
| doi_str_mv | 10.1126/science.1112399 |
| format | Article |
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M ; Islam, M. F ; Zhang, J ; Collings, P. J ; Yodh, A. G</creator><creatorcontrib>Alsayed, A. M ; Islam, M. F ; Zhang, J ; Collings, P. J ; Yodh, A. G</creatorcontrib><description>Premelting is the localized loss of crystalline order at surfaces and defects at temperatures below the bulk melting transition. It can be thought of as the nucleation of the melting process. Premelting has been observed at the surfaces of crystals but not within. We report observations of premelting at grain boundaries and dislocations within bulk colloidal crystals using real-time video microscopy. The crystals are equilibrium close-packed, three-dimensional colloidal structures made from thermally responsive microgel spheres. Particle tracking reveals increased disorder in crystalline regions bordering defects, the amount of which depends on the type of defect, distance from the defect, and particle volume fraction. Our observations suggest that interfacial free energy is the crucial parameter for premelting in colloidal and atomic-scale crystals.</description><identifier>ISSN: 0036-8075</identifier><identifier>EISSN: 1095-9203</identifier><identifier>DOI: 10.1126/science.1112399</identifier><identifier>PMID: 15994377</identifier><identifier>CODEN: SCIEAS</identifier><language>eng</language><publisher>Washington, DC: American Association for the Advancement of Science</publisher><subject>Applied sciences ; Atoms & subatomic particles ; Chemical synthesis ; Chemistry ; Climate ; Colloidal state and disperse state ; Colloids ; Condensed matter: structure, mechanical and thermal properties ; Crystals ; Energy ; Equations of state, phase equilibria, and phase transitions ; Exact sciences and technology ; Free energy ; General and physical chemistry ; Grain boundaries ; Laboratory Equipment ; Material concentration ; Melting ; Melting points ; Organic polymers ; Particle tracks ; Physical and chemical studies. Granulometry. Electrokinetic phenomena ; Physicochemistry of polymers ; Physics ; Properties and characterization ; Solid-liquid transitions ; Specific phase transitions ; Stacking faults ; Structure, morphology and analysis ; Video Technology ; Water</subject><ispartof>Science (American Association for the Advancement of Science), 2005-08, Vol.309 (5738), p.1207-1210</ispartof><rights>Copyright 2005 American Association for the Advancement of Science</rights><rights>2005 INIST-CNRS</rights><rights>COPYRIGHT 2005 American Association for the Advancement of Science</rights><rights>COPYRIGHT 2005 American Association for the Advancement of Science</rights><rights>Copyright American Association for the Advancement of Science Aug 19, 2005</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c747t-bcf0e864be4a8c875e6be98715fcddb9963c3c4d667dd7e86202a9b8395960ff3</citedby><cites>FETCH-LOGICAL-c747t-bcf0e864be4a8c875e6be98715fcddb9963c3c4d667dd7e86202a9b8395960ff3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.jstor.org/stable/pdf/3842444$$EPDF$$P50$$Gjstor$$H</linktopdf><linktohtml>$$Uhttps://www.jstor.org/stable/3842444$$EHTML$$P50$$Gjstor$$H</linktohtml><link.rule.ids>314,777,781,800,2871,2872,27905,27906,57998,58231</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17036964$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/15994377$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Alsayed, A. M</creatorcontrib><creatorcontrib>Islam, M. F</creatorcontrib><creatorcontrib>Zhang, J</creatorcontrib><creatorcontrib>Collings, P. J</creatorcontrib><creatorcontrib>Yodh, A. G</creatorcontrib><title>Premelting at Defects Within Bulk Colloidal Crystals</title><title>Science (American Association for the Advancement of Science)</title><addtitle>Science</addtitle><description>Premelting is the localized loss of crystalline order at surfaces and defects at temperatures below the bulk melting transition. It can be thought of as the nucleation of the melting process. Premelting has been observed at the surfaces of crystals but not within. We report observations of premelting at grain boundaries and dislocations within bulk colloidal crystals using real-time video microscopy. The crystals are equilibrium close-packed, three-dimensional colloidal structures made from thermally responsive microgel spheres. Particle tracking reveals increased disorder in crystalline regions bordering defects, the amount of which depends on the type of defect, distance from the defect, and particle volume fraction. Our observations suggest that interfacial free energy is the crucial parameter for premelting in colloidal and atomic-scale crystals.</description><subject>Applied sciences</subject><subject>Atoms & subatomic particles</subject><subject>Chemical synthesis</subject><subject>Chemistry</subject><subject>Climate</subject><subject>Colloidal state and disperse state</subject><subject>Colloids</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Crystals</subject><subject>Energy</subject><subject>Equations of state, phase equilibria, and phase transitions</subject><subject>Exact sciences and technology</subject><subject>Free energy</subject><subject>General and physical chemistry</subject><subject>Grain boundaries</subject><subject>Laboratory Equipment</subject><subject>Material concentration</subject><subject>Melting</subject><subject>Melting points</subject><subject>Organic polymers</subject><subject>Particle tracks</subject><subject>Physical and chemical studies. 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The crystals are equilibrium close-packed, three-dimensional colloidal structures made from thermally responsive microgel spheres. Particle tracking reveals increased disorder in crystalline regions bordering defects, the amount of which depends on the type of defect, distance from the defect, and particle volume fraction. Our observations suggest that interfacial free energy is the crucial parameter for premelting in colloidal and atomic-scale crystals.</abstract><cop>Washington, DC</cop><pub>American Association for the Advancement of Science</pub><pmid>15994377</pmid><doi>10.1126/science.1112399</doi><tpages>4</tpages><oa>free_for_read</oa></addata></record> |
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| source | American Association for the Advancement of Science; Jstor Complete Legacy |
| subjects | Applied sciences Atoms & subatomic particles Chemical synthesis Chemistry Climate Colloidal state and disperse state Colloids Condensed matter: structure, mechanical and thermal properties Crystals Energy Equations of state, phase equilibria, and phase transitions Exact sciences and technology Free energy General and physical chemistry Grain boundaries Laboratory Equipment Material concentration Melting Melting points Organic polymers Particle tracks Physical and chemical studies. Granulometry. Electrokinetic phenomena Physicochemistry of polymers Physics Properties and characterization Solid-liquid transitions Specific phase transitions Stacking faults Structure, morphology and analysis Video Technology Water |
| title | Premelting at Defects Within Bulk Colloidal Crystals |
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