Simultaneous analysis of glycyrrhizin, paeoniflorin, quercetin, ferulic acid, liquiritin, formononetin, benzoic acid and isoliquiritigenin in the Chinese proprietary medicine Xiao Yao Wan by HPLC
A high performance liquid chromatography coupled with photodiode-array detection method was developed for simultaneous determination of glycyrrhizin, paeoniflorin, benzoic acid, quercetin, ferulic acid, formononetin, liquiritin and isoliquiritigenin in the Chinese proprietary medicine “Xiao Yao Wan”...
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| Veröffentlicht in: | Journal of pharmaceutical and biomedical analysis 2007-11, Vol.45 (3), p.450-455 |
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| container_title | Journal of pharmaceutical and biomedical analysis |
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| creator | Xie, Junbo Wang, Wenquan Zhang, Yanqing Bai, Yin Yang, Quan |
| description | A high performance liquid chromatography coupled with photodiode-array detection method was developed for simultaneous determination of glycyrrhizin, paeoniflorin, benzoic acid, quercetin, ferulic acid, formononetin, liquiritin and isoliquiritigenin in the Chinese proprietary medicine “Xiao Yao Wan” (XYW). The analysis was performed by reverse phase gradient elution, using an aqueous mobile phase (containing 0.1% phosphoric acid) modified by acetonitrile and detection made simultaneously at four wavelengths. The method was validated for accuracy, precision and limits of detection and quantification. Ten batches of XYW obtained from different pharmaceutical companies were analyzed and found to contain different amounts of the eight bioactive markers. This method could be used for quality assessment of this herbal medicine. |
| doi_str_mv | 10.1016/j.jpba.2007.07.011 |
| format | Article |
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The analysis was performed by reverse phase gradient elution, using an aqueous mobile phase (containing 0.1% phosphoric acid) modified by acetonitrile and detection made simultaneously at four wavelengths. The method was validated for accuracy, precision and limits of detection and quantification. Ten batches of XYW obtained from different pharmaceutical companies were analyzed and found to contain different amounts of the eight bioactive markers. This method could be used for quality assessment of this herbal medicine.</description><identifier>ISSN: 0731-7085</identifier><identifier>EISSN: 1873-264X</identifier><identifier>DOI: 10.1016/j.jpba.2007.07.011</identifier><identifier>PMID: 17709224</identifier><identifier>CODEN: JPBADA</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject><![CDATA[Analysis ; Analytical, structural and metabolic biochemistry ; Benzoates - isolation & purification ; Biological and medical sciences ; Bridged-Ring Compounds - isolation & purification ; Chalcones - isolation & purification ; Chinese proprietary medicine ; Chromatography, High Pressure Liquid ; Coumaric Acids - isolation & purification ; Drugs, Chinese Herbal - chemistry ; Flavanones - isolation & purification ; Flavonoids - isolation & purification ; Fundamental and applied biological sciences. Psychology ; General pharmacology ; Glucosides - isolation & purification ; Glycyrrhizic Acid - isolation & purification ; HPLC-DAD ; Isoflavones - isolation & purification ; Medical sciences ; Medicine, Chinese Traditional ; Molecular Structure ; Monoterpenes ; Pharmacology. Drug treatments ; Quality evaluation ; Quercetin - isolation & purification ; Reference Standards ; Reproducibility of Results ; Sensitivity and Specificity ; Xiao Yao Wan]]></subject><ispartof>Journal of pharmaceutical and biomedical analysis, 2007-11, Vol.45 (3), p.450-455</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c384t-13e6f3fbf7a4cb509056e97ac1c54eecaa90c5b6495c0471a3cdb80726fc2bca3</citedby><cites>FETCH-LOGICAL-c384t-13e6f3fbf7a4cb509056e97ac1c54eecaa90c5b6495c0471a3cdb80726fc2bca3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jpba.2007.07.011$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3549,27923,27924,45994</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=19983989$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/17709224$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Xie, Junbo</creatorcontrib><creatorcontrib>Wang, Wenquan</creatorcontrib><creatorcontrib>Zhang, Yanqing</creatorcontrib><creatorcontrib>Bai, Yin</creatorcontrib><creatorcontrib>Yang, Quan</creatorcontrib><title>Simultaneous analysis of glycyrrhizin, paeoniflorin, quercetin, ferulic acid, liquiritin, formononetin, benzoic acid and isoliquiritigenin in the Chinese proprietary medicine Xiao Yao Wan by HPLC</title><title>Journal of pharmaceutical and biomedical analysis</title><addtitle>J Pharm Biomed Anal</addtitle><description>A high performance liquid chromatography coupled with photodiode-array detection method was developed for simultaneous determination of glycyrrhizin, paeoniflorin, benzoic acid, quercetin, ferulic acid, formononetin, liquiritin and isoliquiritigenin in the Chinese proprietary medicine “Xiao Yao Wan” (XYW). The analysis was performed by reverse phase gradient elution, using an aqueous mobile phase (containing 0.1% phosphoric acid) modified by acetonitrile and detection made simultaneously at four wavelengths. The method was validated for accuracy, precision and limits of detection and quantification. Ten batches of XYW obtained from different pharmaceutical companies were analyzed and found to contain different amounts of the eight bioactive markers. This method could be used for quality assessment of this herbal medicine.</description><subject>Analysis</subject><subject>Analytical, structural and metabolic biochemistry</subject><subject>Benzoates - isolation & purification</subject><subject>Biological and medical sciences</subject><subject>Bridged-Ring Compounds - isolation & purification</subject><subject>Chalcones - isolation & purification</subject><subject>Chinese proprietary medicine</subject><subject>Chromatography, High Pressure Liquid</subject><subject>Coumaric Acids - isolation & purification</subject><subject>Drugs, Chinese Herbal - chemistry</subject><subject>Flavanones - isolation & purification</subject><subject>Flavonoids - isolation & purification</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>General pharmacology</subject><subject>Glucosides - isolation & purification</subject><subject>Glycyrrhizic Acid - isolation & purification</subject><subject>HPLC-DAD</subject><subject>Isoflavones - isolation & purification</subject><subject>Medical sciences</subject><subject>Medicine, Chinese Traditional</subject><subject>Molecular Structure</subject><subject>Monoterpenes</subject><subject>Pharmacology. Drug treatments</subject><subject>Quality evaluation</subject><subject>Quercetin - isolation & purification</subject><subject>Reference Standards</subject><subject>Reproducibility of Results</subject><subject>Sensitivity and Specificity</subject><subject>Xiao Yao Wan</subject><issn>0731-7085</issn><issn>1873-264X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kV2L1DAUhoso7rj6B7yQ3OjVdkza9Au8kUFdYUBBxfUqpKcnO2foJLNJK3T_nn_MlBb3TjghX885yXnfJHkp-FZwUb49bo_nVm8zzqvtHEI8SjairvI0K-XN42TDq1ykFa-Li-RZCEfOeSEa-TS5EFXFmyyTm-TPNzqN_aAtujEwbXU_BQrMGXbbTzB5f6B7slfsrNFZMr3z8-5uRA84zEuDfuwJmAbqrlhPdyN5Wm6cPznr7MK1aO_dysV3OkbB_aNv0ZJlMYYDst2BLAZkZ-_OnnDQfmIn7AjiMbsh7divOH5qy9qJXX_d754nT4zuA75Y58vkx8cP33fX6f7Lp8-79_sU8loOqcixNLlpTaUltAVveFFiU2kQUEhE0LrhULSlbArgshI6h66teZWVBrIWdH6ZvFnqxp9FBcKgThQA-35RT5W1zKTgPILZAoJ3IXg0KjZyin0owdVsnTqq2To1W6fmECImvVqrj21s9yFl9SoCr1dAB9C98doChQeuaeq8qZvIvVs4jFr8JvQqAKGFKKFHGFTn6H__-As6_70K</recordid><startdate>20071105</startdate><enddate>20071105</enddate><creator>Xie, Junbo</creator><creator>Wang, Wenquan</creator><creator>Zhang, Yanqing</creator><creator>Bai, Yin</creator><creator>Yang, Quan</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20071105</creationdate><title>Simultaneous analysis of glycyrrhizin, paeoniflorin, quercetin, ferulic acid, liquiritin, formononetin, benzoic acid and isoliquiritigenin in the Chinese proprietary medicine Xiao Yao Wan by HPLC</title><author>Xie, Junbo ; Wang, Wenquan ; Zhang, Yanqing ; Bai, Yin ; Yang, Quan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c384t-13e6f3fbf7a4cb509056e97ac1c54eecaa90c5b6495c0471a3cdb80726fc2bca3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Analysis</topic><topic>Analytical, structural and metabolic biochemistry</topic><topic>Benzoates - isolation & purification</topic><topic>Biological and medical sciences</topic><topic>Bridged-Ring Compounds - isolation & purification</topic><topic>Chalcones - isolation & purification</topic><topic>Chinese proprietary medicine</topic><topic>Chromatography, High Pressure Liquid</topic><topic>Coumaric Acids - isolation & purification</topic><topic>Drugs, Chinese Herbal - chemistry</topic><topic>Flavanones - isolation & purification</topic><topic>Flavonoids - isolation & purification</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>General pharmacology</topic><topic>Glucosides - isolation & purification</topic><topic>Glycyrrhizic Acid - isolation & purification</topic><topic>HPLC-DAD</topic><topic>Isoflavones - isolation & purification</topic><topic>Medical sciences</topic><topic>Medicine, Chinese Traditional</topic><topic>Molecular Structure</topic><topic>Monoterpenes</topic><topic>Pharmacology. Drug treatments</topic><topic>Quality evaluation</topic><topic>Quercetin - isolation & purification</topic><topic>Reference Standards</topic><topic>Reproducibility of Results</topic><topic>Sensitivity and Specificity</topic><topic>Xiao Yao Wan</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xie, Junbo</creatorcontrib><creatorcontrib>Wang, Wenquan</creatorcontrib><creatorcontrib>Zhang, Yanqing</creatorcontrib><creatorcontrib>Bai, Yin</creatorcontrib><creatorcontrib>Yang, Quan</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of pharmaceutical and biomedical analysis</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xie, Junbo</au><au>Wang, Wenquan</au><au>Zhang, Yanqing</au><au>Bai, Yin</au><au>Yang, Quan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Simultaneous analysis of glycyrrhizin, paeoniflorin, quercetin, ferulic acid, liquiritin, formononetin, benzoic acid and isoliquiritigenin in the Chinese proprietary medicine Xiao Yao Wan by HPLC</atitle><jtitle>Journal of pharmaceutical and biomedical analysis</jtitle><addtitle>J Pharm Biomed Anal</addtitle><date>2007-11-05</date><risdate>2007</risdate><volume>45</volume><issue>3</issue><spage>450</spage><epage>455</epage><pages>450-455</pages><issn>0731-7085</issn><eissn>1873-264X</eissn><coden>JPBADA</coden><abstract>A high performance liquid chromatography coupled with photodiode-array detection method was developed for simultaneous determination of glycyrrhizin, paeoniflorin, benzoic acid, quercetin, ferulic acid, formononetin, liquiritin and isoliquiritigenin in the Chinese proprietary medicine “Xiao Yao Wan” (XYW). The analysis was performed by reverse phase gradient elution, using an aqueous mobile phase (containing 0.1% phosphoric acid) modified by acetonitrile and detection made simultaneously at four wavelengths. The method was validated for accuracy, precision and limits of detection and quantification. Ten batches of XYW obtained from different pharmaceutical companies were analyzed and found to contain different amounts of the eight bioactive markers. This method could be used for quality assessment of this herbal medicine.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>17709224</pmid><doi>10.1016/j.jpba.2007.07.011</doi><tpages>6</tpages></addata></record> |
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| ispartof | Journal of pharmaceutical and biomedical analysis, 2007-11, Vol.45 (3), p.450-455 |
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| source | MEDLINE; ScienceDirect Journals (5 years ago - present) |
| subjects | Analysis Analytical, structural and metabolic biochemistry Benzoates - isolation & purification Biological and medical sciences Bridged-Ring Compounds - isolation & purification Chalcones - isolation & purification Chinese proprietary medicine Chromatography, High Pressure Liquid Coumaric Acids - isolation & purification Drugs, Chinese Herbal - chemistry Flavanones - isolation & purification Flavonoids - isolation & purification Fundamental and applied biological sciences. Psychology General pharmacology Glucosides - isolation & purification Glycyrrhizic Acid - isolation & purification HPLC-DAD Isoflavones - isolation & purification Medical sciences Medicine, Chinese Traditional Molecular Structure Monoterpenes Pharmacology. Drug treatments Quality evaluation Quercetin - isolation & purification Reference Standards Reproducibility of Results Sensitivity and Specificity Xiao Yao Wan |
| title | Simultaneous analysis of glycyrrhizin, paeoniflorin, quercetin, ferulic acid, liquiritin, formononetin, benzoic acid and isoliquiritigenin in the Chinese proprietary medicine Xiao Yao Wan by HPLC |
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