Concentration measurements of sucrose and sugar surfactants solutions by using the 1H NMR ERETIC method
The ERETIC method has been used to determine precise concentrations of aqueous solutions of sucrose and sugar surfactants, namely octyl glucoside and fatty acid sucrose esters by 1H NMR spectroscopy. The effects of NMR tuning, acquisition parameters, and spectrum processing on the measurement have b...
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| Veröffentlicht in: | Carbohydrate research 2006-08, Vol.341 (11), p.1890-1895 |
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| container_end_page | 1895 |
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| container_issue | 11 |
| container_start_page | 1890 |
| container_title | Carbohydrate research |
| container_volume | 341 |
| creator | Molinier, Valérie Fenet, Bernard Fitremann, Juliette Bouchu, Alain Queneau, Yves |
| description | The ERETIC method has been used to determine precise concentrations of aqueous solutions of sucrose and sugar surfactants, namely octyl glucoside and fatty acid sucrose esters by
1H NMR spectroscopy. The effects of NMR tuning, acquisition parameters, and spectrum processing on the measurement have been assessed in these particular cases. The linearity upholds over the whole concentration range, with both sucrose and octyl glucoside, whatever the physicochemical phenomena occurring, either an increasing viscosity or the micellization of the surfactant. For sucrose solutions, an accuracy of 2% is measured for concentrations between 0.1 and 200
mmol/L, which is consistent with literature data. |
| doi_str_mv | 10.1016/j.carres.2006.04.034 |
| format | Article |
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1H NMR spectroscopy. The effects of NMR tuning, acquisition parameters, and spectrum processing on the measurement have been assessed in these particular cases. The linearity upholds over the whole concentration range, with both sucrose and octyl glucoside, whatever the physicochemical phenomena occurring, either an increasing viscosity or the micellization of the surfactant. For sucrose solutions, an accuracy of 2% is measured for concentrations between 0.1 and 200
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1H NMR spectroscopy. The effects of NMR tuning, acquisition parameters, and spectrum processing on the measurement have been assessed in these particular cases. The linearity upholds over the whole concentration range, with both sucrose and octyl glucoside, whatever the physicochemical phenomena occurring, either an increasing viscosity or the micellization of the surfactant. For sucrose solutions, an accuracy of 2% is measured for concentrations between 0.1 and 200
mmol/L, which is consistent with literature data.</description><subject>Alkyl glucoside</subject><subject>Calibration</subject><subject>Carbohydrate</subject><subject>Glucosides - analysis</subject><subject>Glucosides - chemistry</subject><subject>Magnetic Resonance Spectroscopy - methods</subject><subject>Micelle</subject><subject>Molecular Structure</subject><subject>Solutions</subject><subject>Sucrose - analysis</subject><subject>Sucrose - chemistry</subject><subject>Sucrose ester</subject><subject>Surface-Active Agents - analysis</subject><subject>Surface-Active Agents - chemistry</subject><subject>Surfactant</subject><issn>0008-6215</issn><issn>1873-426X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kFFL5DAUhYO4rLPj_gORPPnWepOmmfRFkGFcBd0FccG3kEluxg7TRpNW8N-bMgO--ZLkhnPO5XyEnDEoGTB5uS2tiRFTyQFkCaKEShyRGVOLqhBcPh-TGQCoQnJWn5BfKW3zCHIhf5ITJmWzaBo-I5tl6C32QzRDG3raoUljxC7_JBo8TaONISE1vcvvjYn5jN7YwUyCFHbjZEt0_UHH1PYbOrwgZbf078MjXT2unu6WOXJ4Ce6U_PBml_D34Z6T_zerp-Vtcf_vz93y-r6wHGpeKCeRK-cbCzVa5NxXHIStmfJ1tQaLTgjPGsYrxdE0dW2UR-ms86IRaymrObnY577G8DZiGnTXJou7nekxjElLBUpCZjQnYi-cCqaIXr_GtjPxQzPQE2C91XvAegKsQegMONvOD_njukP3ZToQzYKrvQBzy_cWo062xczYtRHtoF1ov9_wCcESjzU</recordid><startdate>20060814</startdate><enddate>20060814</enddate><creator>Molinier, Valérie</creator><creator>Fenet, Bernard</creator><creator>Fitremann, Juliette</creator><creator>Bouchu, Alain</creator><creator>Queneau, Yves</creator><general>Elsevier Ltd</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20060814</creationdate><title>Concentration measurements of sucrose and sugar surfactants solutions by using the 1H NMR ERETIC method</title><author>Molinier, Valérie ; Fenet, Bernard ; Fitremann, Juliette ; Bouchu, Alain ; Queneau, Yves</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2052-8d6e28df9c05ece22f3204c518f53b0ced44f1912382ea955a8fe6dcdf494b663</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Alkyl glucoside</topic><topic>Calibration</topic><topic>Carbohydrate</topic><topic>Glucosides - analysis</topic><topic>Glucosides - chemistry</topic><topic>Magnetic Resonance Spectroscopy - methods</topic><topic>Micelle</topic><topic>Molecular Structure</topic><topic>Solutions</topic><topic>Sucrose - analysis</topic><topic>Sucrose - chemistry</topic><topic>Sucrose ester</topic><topic>Surface-Active Agents - analysis</topic><topic>Surface-Active Agents - chemistry</topic><topic>Surfactant</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Molinier, Valérie</creatorcontrib><creatorcontrib>Fenet, Bernard</creatorcontrib><creatorcontrib>Fitremann, Juliette</creatorcontrib><creatorcontrib>Bouchu, Alain</creatorcontrib><creatorcontrib>Queneau, Yves</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Carbohydrate research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Molinier, Valérie</au><au>Fenet, Bernard</au><au>Fitremann, Juliette</au><au>Bouchu, Alain</au><au>Queneau, Yves</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Concentration measurements of sucrose and sugar surfactants solutions by using the 1H NMR ERETIC method</atitle><jtitle>Carbohydrate research</jtitle><addtitle>Carbohydr Res</addtitle><date>2006-08-14</date><risdate>2006</risdate><volume>341</volume><issue>11</issue><spage>1890</spage><epage>1895</epage><pages>1890-1895</pages><issn>0008-6215</issn><eissn>1873-426X</eissn><abstract>The ERETIC method has been used to determine precise concentrations of aqueous solutions of sucrose and sugar surfactants, namely octyl glucoside and fatty acid sucrose esters by
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| ispartof | Carbohydrate research, 2006-08, Vol.341 (11), p.1890-1895 |
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| source | MEDLINE; Elsevier ScienceDirect Journals |
| subjects | Alkyl glucoside Calibration Carbohydrate Glucosides - analysis Glucosides - chemistry Magnetic Resonance Spectroscopy - methods Micelle Molecular Structure Solutions Sucrose - analysis Sucrose - chemistry Sucrose ester Surface-Active Agents - analysis Surface-Active Agents - chemistry Surfactant |
| title | Concentration measurements of sucrose and sugar surfactants solutions by using the 1H NMR ERETIC method |
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