Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin
To evaluate the effect of smear layer thickness (SL) on early and 6-month bond strength (BS) of self-etching adhesives to dentin and to measure the ultimate microtensile strength (UTS) of the adhesives. Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as co...
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creator | Reis, Alessandra Grandi, Viviane Carlotto, Larissa Bortoli, Giana Patzlaff, Rafael Rodrigues Accorinte, Maria de Lourdes Dourado Loguercio, Alessandro |
description | To evaluate the effect of smear layer thickness (SL) on early and 6-month bond strength (BS) of self-etching adhesives to dentin and to measure the ultimate microtensile strength (UTS) of the adhesives.
Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application (
n=6) a resin build-up was made. After 24
h, resin–dentin beams (0.8
mm
2) were prepared to be tested immediately and after 6-month (6M) at 0.5
mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive (
α=0.05).
The SL thickness was not significant (
p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS (
R=0.95,
p=0.02).
The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS. |
doi_str_mv | 10.1016/j.jdent.2004.12.003 |
format | Article |
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Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application (
n=6) a resin build-up was made. After 24
h, resin–dentin beams (0.8
mm
2) were prepared to be tested immediately and after 6-month (6M) at 0.5
mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive (
α=0.05).
The SL thickness was not significant (
p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS (
R=0.95,
p=0.02).
The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS.</description><identifier>ISSN: 0300-5712</identifier><identifier>EISSN: 1879-176X</identifier><identifier>DOI: 10.1016/j.jdent.2004.12.003</identifier><identifier>PMID: 16005794</identifier><language>eng</language><publisher>England: Elsevier Ltd</publisher><subject>Acid Etching, Dental - methods ; Adhesives ; Analysis of Variance ; Bond strength ; Care and treatment ; Collagen ; Dental Bonding ; Dental Stress Analysis ; Dentin ; Dentin adhesion ; Dentin-Bonding Agents ; Dentistry ; Diagnosis ; Etching ; Humans ; Hydrogen-Ion Concentration ; Long-term bond strength ; Materials Testing ; Methacrylates ; Microtensile test ; Molar ; Resin Cements ; Resin–dentin bond strength ; Self-etching adhesives ; Smear Layer ; Smear layer thickness ; Solvents ; Standard deviation ; Statistics, Nonparametric ; Studies ; Tensile Strength ; Tooth diseases ; Total-etch adhesives ; Ultimate microtensile strength</subject><ispartof>Journal of dentistry, 2005-08, Vol.33 (7), p.549-559</ispartof><rights>2005 Elsevier Ltd</rights><rights>COPYRIGHT 2005 The Lancet Publishing Group, a division of Elsevier Science Ltd.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c518t-812c18f0307b00d7d5e3bc50ceef5f283a615d826b8c9279c1d8fd60ed79e0b3</citedby><cites>FETCH-LOGICAL-c518t-812c18f0307b00d7d5e3bc50ceef5f283a615d826b8c9279c1d8fd60ed79e0b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0300571205000102$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/16005794$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Reis, Alessandra</creatorcontrib><creatorcontrib>Grandi, Viviane</creatorcontrib><creatorcontrib>Carlotto, Larissa</creatorcontrib><creatorcontrib>Bortoli, Giana</creatorcontrib><creatorcontrib>Patzlaff, Rafael</creatorcontrib><creatorcontrib>Rodrigues Accorinte, Maria de Lourdes</creatorcontrib><creatorcontrib>Dourado Loguercio, Alessandro</creatorcontrib><title>Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin</title><title>Journal of dentistry</title><addtitle>J Dent</addtitle><description>To evaluate the effect of smear layer thickness (SL) on early and 6-month bond strength (BS) of self-etching adhesives to dentin and to measure the ultimate microtensile strength (UTS) of the adhesives.
Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application (
n=6) a resin build-up was made. After 24
h, resin–dentin beams (0.8
mm
2) were prepared to be tested immediately and after 6-month (6M) at 0.5
mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive (
α=0.05).
The SL thickness was not significant (
p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS (
R=0.95,
p=0.02).
The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS.</description><subject>Acid Etching, Dental - methods</subject><subject>Adhesives</subject><subject>Analysis of Variance</subject><subject>Bond strength</subject><subject>Care and treatment</subject><subject>Collagen</subject><subject>Dental Bonding</subject><subject>Dental Stress Analysis</subject><subject>Dentin</subject><subject>Dentin adhesion</subject><subject>Dentin-Bonding Agents</subject><subject>Dentistry</subject><subject>Diagnosis</subject><subject>Etching</subject><subject>Humans</subject><subject>Hydrogen-Ion Concentration</subject><subject>Long-term bond strength</subject><subject>Materials Testing</subject><subject>Methacrylates</subject><subject>Microtensile test</subject><subject>Molar</subject><subject>Resin Cements</subject><subject>Resin–dentin bond strength</subject><subject>Self-etching adhesives</subject><subject>Smear Layer</subject><subject>Smear layer thickness</subject><subject>Solvents</subject><subject>Standard deviation</subject><subject>Statistics, Nonparametric</subject><subject>Studies</subject><subject>Tensile Strength</subject><subject>Tooth diseases</subject><subject>Total-etch adhesives</subject><subject>Ultimate microtensile strength</subject><issn>0300-5712</issn><issn>1879-176X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kU1rFTEUhgdR7LX6CwQJCO5mPMl8ZRYuSmmrUHDThbuQSU7uzTiT1CRTuP_e3A_wA5EsQsLznnOSpyjeUqgo0O7jVE0aXaoYQFNRVgHUz4oN5f1Q0r779rzYQA1Qtj1lF8WrGCfIILDhZXFBO4C2H5pNkW6MQZWINyQuKAOZ5R4DSTurvjuMkUiniVRW27Q_QjibEpPaWbcl0c9rst5F4h3J4Xl_xGfvtmXCsJDR52NMAd027Ujy5DCwda-LF0bOEd-c98vi4fbm4fpzef_17sv11X2pWspTySlTlJv8in4E0L1usR5VCwrRtIbxWna01Zx1I1cD6wdFNTe6A9T9gDDWl8WHU9nH4H-sGJNYbFQ4z9KhX6PoONBmYJDB93-Bk1-Dy6MJCnXNKG_4b9RWziisMz4FqQ4lxRVt2oEzRptMVf-g8tK4WOUdGpvv_wjUp4AKPsaARjwGu8iwz73FQbSYxFG0OIgWlIksOqfenUdexwX1r8zZbAY-nQDMH_xkMYioLDqF2oYsXGhv_9vgJ7IUuZ0</recordid><startdate>20050801</startdate><enddate>20050801</enddate><creator>Reis, Alessandra</creator><creator>Grandi, Viviane</creator><creator>Carlotto, Larissa</creator><creator>Bortoli, Giana</creator><creator>Patzlaff, Rafael</creator><creator>Rodrigues Accorinte, Maria de Lourdes</creator><creator>Dourado Loguercio, Alessandro</creator><general>Elsevier Ltd</general><general>The Lancet Publishing Group, a division of Elsevier Science Ltd</general><general>Elsevier Limited</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QP</scope><scope>7QQ</scope><scope>7SE</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>H8G</scope><scope>JG9</scope><scope>K9.</scope><scope>7X8</scope></search><sort><creationdate>20050801</creationdate><title>Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin</title><author>Reis, Alessandra ; 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Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application (
n=6) a resin build-up was made. After 24
h, resin–dentin beams (0.8
mm
2) were prepared to be tested immediately and after 6-month (6M) at 0.5
mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive (
α=0.05).
The SL thickness was not significant (
p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS (
R=0.95,
p=0.02).
The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS.</abstract><cop>England</cop><pub>Elsevier Ltd</pub><pmid>16005794</pmid><doi>10.1016/j.jdent.2004.12.003</doi><tpages>11</tpages></addata></record> |
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source | MEDLINE; Elsevier ScienceDirect Journals |
subjects | Acid Etching, Dental - methods Adhesives Analysis of Variance Bond strength Care and treatment Collagen Dental Bonding Dental Stress Analysis Dentin Dentin adhesion Dentin-Bonding Agents Dentistry Diagnosis Etching Humans Hydrogen-Ion Concentration Long-term bond strength Materials Testing Methacrylates Microtensile test Molar Resin Cements Resin–dentin bond strength Self-etching adhesives Smear Layer Smear layer thickness Solvents Standard deviation Statistics, Nonparametric Studies Tensile Strength Tooth diseases Total-etch adhesives Ultimate microtensile strength |
title | Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin |
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