Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin

To evaluate the effect of smear layer thickness (SL) on early and 6-month bond strength (BS) of self-etching adhesives to dentin and to measure the ultimate microtensile strength (UTS) of the adhesives. Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as co...

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Veröffentlicht in:Journal of dentistry 2005-08, Vol.33 (7), p.549-559
Hauptverfasser: Reis, Alessandra, Grandi, Viviane, Carlotto, Larissa, Bortoli, Giana, Patzlaff, Rafael, Rodrigues Accorinte, Maria de Lourdes, Dourado Loguercio, Alessandro
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container_end_page 559
container_issue 7
container_start_page 549
container_title Journal of dentistry
container_volume 33
creator Reis, Alessandra
Grandi, Viviane
Carlotto, Larissa
Bortoli, Giana
Patzlaff, Rafael
Rodrigues Accorinte, Maria de Lourdes
Dourado Loguercio, Alessandro
description To evaluate the effect of smear layer thickness (SL) on early and 6-month bond strength (BS) of self-etching adhesives to dentin and to measure the ultimate microtensile strength (UTS) of the adhesives. Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application ( n=6) a resin build-up was made. After 24 h, resin–dentin beams (0.8 mm 2) were prepared to be tested immediately and after 6-month (6M) at 0.5 mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive ( α=0.05). The SL thickness was not significant ( p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS ( R=0.95, p=0.02). The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS.
doi_str_mv 10.1016/j.jdent.2004.12.003
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Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application ( n=6) a resin build-up was made. After 24 h, resin–dentin beams (0.8 mm 2) were prepared to be tested immediately and after 6-month (6M) at 0.5 mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive ( α=0.05). The SL thickness was not significant ( p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS ( R=0.95, p=0.02). The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. 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Clearfil SE Bond; Optibond Solo Plus Self-Etch Primer; Tyrian Self Priming Etchant (TY) and as controls, Single Bond (SB) and Scotchbond Multi-Purpose Plus (SBMP) were applied on flat superficial dentin surface with thick and thin SL thicknesses. After adhesive's application ( n=6) a resin build-up was made. After 24 h, resin–dentin beams (0.8 mm 2) were prepared to be tested immediately and after 6-month (6M) at 0.5 mm/min. For the UTS measurement, hour-glass specimens were prepared with the bonding resin alone or after mixing (1:1). BS values were analyzed by three-way repeated measures ANOVA and Tukey's multiple comparison tests. Two-way ANOVA (bonding resin and bonding resin+self-etching primer) and Tukey's test were used for the UTS values. The bonding resins were re-evaluated separately by a one-way ANOVA and Tukey's test, since Single Bond is a one-bottle adhesive ( α=0.05). The SL thickness was not significant ( p=0.64). BS values were reduced after 6M, except for the SBMP. TY provided the lowest BS mean while SB and SBMP the highest BS. The UTS of the SBMP was the highest. TY yielded the lowest UTS. Regression analysis revealed a linear and significant relationship between the UTS of self-etch systems and the mean BS ( R=0.95, p=0.02). The performance of a self-etching system does not seem to be dependent on the SL thickness. The total-etch, three-step system provided the highest BS to dentin and maintained the BS stable over 6 months. The performance of the self-etching systems can be envisaged by their UTS.</abstract><cop>England</cop><pub>Elsevier Ltd</pub><pmid>16005794</pmid><doi>10.1016/j.jdent.2004.12.003</doi><tpages>11</tpages></addata></record>
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source MEDLINE; Elsevier ScienceDirect Journals
subjects Acid Etching, Dental - methods
Adhesives
Analysis of Variance
Bond strength
Care and treatment
Collagen
Dental Bonding
Dental Stress Analysis
Dentin
Dentin adhesion
Dentin-Bonding Agents
Dentistry
Diagnosis
Etching
Humans
Hydrogen-Ion Concentration
Long-term bond strength
Materials Testing
Methacrylates
Microtensile test
Molar
Resin Cements
Resin–dentin bond strength
Self-etching adhesives
Smear Layer
Smear layer thickness
Solvents
Standard deviation
Statistics, Nonparametric
Studies
Tensile Strength
Tooth diseases
Total-etch adhesives
Ultimate microtensile strength
title Effect of smear layer thickness and acidity of self-etching solutions on early and long-term bond strength to dentin
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