Elemental Analysis of Crystal Precipitate from Gray and White MTA
Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in...
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Veröffentlicht in: | Journal of endodontics 2006-05, Vol.32 (5), p.425-428 |
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description | Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in Phosphate Buffered Saline (PBS) solution without Ca. The crystals were analyzed by Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), and Inductively Coupled Plasma—Atomic Emission Spectroscopy (ICP-AES). For part B, three cylinders of each material were suspended in distilled, deionized water. The water was analyzed by ICP-AES for Ca content at 24 h, 72 h, and 5, 7, 10, and 14 days. Data were analyzed using one-way ANOVA and Tukey test. Both MTA materials released more Ca initially, followed by a decline and then rise in elution. GMTA produced the most surface crystal, which may be clinically significant. The crystals on GMTA and WMTA were chemically and structurally similar to hydroxyapatite (HA). |
doi_str_mv | 10.1016/j.joen.2005.08.009 |
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Both MTA materials released more Ca initially, followed by a decline and then rise in elution. GMTA produced the most surface crystal, which may be clinically significant. 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Brian</creatorcontrib><creatorcontrib>Lemon, Ronald R.</creatorcontrib><creatorcontrib>Eleazer, Paul D.</creatorcontrib><title>Elemental Analysis of Crystal Precipitate from Gray and White MTA</title><title>Journal of endodontics</title><addtitle>J Endod</addtitle><description>Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in Phosphate Buffered Saline (PBS) solution without Ca. The crystals were analyzed by Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), and Inductively Coupled Plasma—Atomic Emission Spectroscopy (ICP-AES). For part B, three cylinders of each material were suspended in distilled, deionized water. The water was analyzed by ICP-AES for Ca content at 24 h, 72 h, and 5, 7, 10, and 14 days. Data were analyzed using one-way ANOVA and Tukey test. Both MTA materials released more Ca initially, followed by a decline and then rise in elution. GMTA produced the most surface crystal, which may be clinically significant. The crystals on GMTA and WMTA were chemically and structurally similar to hydroxyapatite (HA).</description><subject>Aluminum Compounds - chemistry</subject><subject>Calcium - analysis</subject><subject>Calcium Compounds - chemistry</subject><subject>Chemical Precipitation</subject><subject>Crystal growth</subject><subject>Crystallization</subject><subject>Crystallography, X-Ray</subject><subject>Dentistry</subject><subject>dissolution</subject><subject>Drug Combinations</subject><subject>Durapatite - analysis</subject><subject>Electron Probe Microanalysis</subject><subject>hydroxyapatite</subject><subject>MTA</subject><subject>Oxides - chemistry</subject><subject>Phosphorus - analysis</subject><subject>Root Canal Filling Materials - chemistry</subject><subject>Silicates - chemistry</subject><subject>Silicon - analysis</subject><subject>Spectrophotometry, Atomic</subject><issn>0099-2399</issn><issn>1878-3554</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kEtLw0AUhQdRbK3-AReSlbvEO5nMI-CmlFqFii4qLofp5Aan5FFnUiH_3oQW3Lm6cPjOgfsRckshoUDFwy7ZtdgkKQBPQCUA-RmZUiVVzDjPzsl0SPI4ZXk-IVch7ACoZExekgkVglGV0SmZLyusselMFc0bU_XBhagto4Xvw5i9e7Ru7zrTYVT6to5W3vSRaYro88sN2etmfk0uSlMFvDndGfl4Wm4Wz_H6bfWymK9jm6XQxVyaXHBuOGSiUOnWUiatkFlZcJtLmnGgpVWFzMEIyFSaMsTMMMoUlTxFy2bk_ri79-33AUOnaxcsVpVpsD0ELaRSuQA-gOkRtL4NwWOp997Vxveagh7F6Z0exelRnAalB01D6e60ftjWWPxVTqYG4PEI4PDjj0Ovg3XYWCzc4KjTRev-2_8F1kh80Q</recordid><startdate>20060501</startdate><enddate>20060501</enddate><creator>Bozeman, T. 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Brian ; Lemon, Ronald R. ; Eleazer, Paul D.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c420t-57a9655a5046d82bc137c674fd5c9714501fc8d790a6048223ee4a31381752ec3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Aluminum Compounds - chemistry</topic><topic>Calcium - analysis</topic><topic>Calcium Compounds - chemistry</topic><topic>Chemical Precipitation</topic><topic>Crystal growth</topic><topic>Crystallization</topic><topic>Crystallography, X-Ray</topic><topic>Dentistry</topic><topic>dissolution</topic><topic>Drug Combinations</topic><topic>Durapatite - analysis</topic><topic>Electron Probe Microanalysis</topic><topic>hydroxyapatite</topic><topic>MTA</topic><topic>Oxides - chemistry</topic><topic>Phosphorus - analysis</topic><topic>Root Canal Filling Materials - chemistry</topic><topic>Silicates - chemistry</topic><topic>Silicon - analysis</topic><topic>Spectrophotometry, Atomic</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bozeman, T. Brian</creatorcontrib><creatorcontrib>Lemon, Ronald R.</creatorcontrib><creatorcontrib>Eleazer, Paul D.</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of endodontics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bozeman, T. Brian</au><au>Lemon, Ronald R.</au><au>Eleazer, Paul D.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Elemental Analysis of Crystal Precipitate from Gray and White MTA</atitle><jtitle>Journal of endodontics</jtitle><addtitle>J Endod</addtitle><date>2006-05-01</date><risdate>2006</risdate><volume>32</volume><issue>5</issue><spage>425</spage><epage>428</epage><pages>425-428</pages><issn>0099-2399</issn><eissn>1878-3554</eissn><abstract>Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in Phosphate Buffered Saline (PBS) solution without Ca. The crystals were analyzed by Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), and Inductively Coupled Plasma—Atomic Emission Spectroscopy (ICP-AES). For part B, three cylinders of each material were suspended in distilled, deionized water. The water was analyzed by ICP-AES for Ca content at 24 h, 72 h, and 5, 7, 10, and 14 days. Data were analyzed using one-way ANOVA and Tukey test. Both MTA materials released more Ca initially, followed by a decline and then rise in elution. GMTA produced the most surface crystal, which may be clinically significant. The crystals on GMTA and WMTA were chemically and structurally similar to hydroxyapatite (HA).</abstract><cop>United States</cop><pub>Elsevier Inc</pub><pmid>16631841</pmid><doi>10.1016/j.joen.2005.08.009</doi><tpages>4</tpages></addata></record> |
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subjects | Aluminum Compounds - chemistry Calcium - analysis Calcium Compounds - chemistry Chemical Precipitation Crystal growth Crystallization Crystallography, X-Ray Dentistry dissolution Drug Combinations Durapatite - analysis Electron Probe Microanalysis hydroxyapatite MTA Oxides - chemistry Phosphorus - analysis Root Canal Filling Materials - chemistry Silicates - chemistry Silicon - analysis Spectrophotometry, Atomic |
title | Elemental Analysis of Crystal Precipitate from Gray and White MTA |
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