Elemental Analysis of Crystal Precipitate from Gray and White MTA

Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in...

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Veröffentlicht in:Journal of endodontics 2006-05, Vol.32 (5), p.425-428
Hauptverfasser: Bozeman, T. Brian, Lemon, Ronald R., Eleazer, Paul D.
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container_title Journal of endodontics
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creator Bozeman, T. Brian
Lemon, Ronald R.
Eleazer, Paul D.
description Crystal growth and elemental dissolution characteristics of gray Mineral Trioxide Aggregate (GMTA), white MTA (WMTA), and an experimental material, Dentalcrete, were compared. For part A, comparing amount and composition of surface crystal growth, twelve cylinders of each material were suspended in Phosphate Buffered Saline (PBS) solution without Ca. The crystals were analyzed by Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), and Inductively Coupled Plasma—Atomic Emission Spectroscopy (ICP-AES). For part B, three cylinders of each material were suspended in distilled, deionized water. The water was analyzed by ICP-AES for Ca content at 24 h, 72 h, and 5, 7, 10, and 14 days. Data were analyzed using one-way ANOVA and Tukey test. Both MTA materials released more Ca initially, followed by a decline and then rise in elution. GMTA produced the most surface crystal, which may be clinically significant. The crystals on GMTA and WMTA were chemically and structurally similar to hydroxyapatite (HA).
doi_str_mv 10.1016/j.joen.2005.08.009
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subjects Aluminum Compounds - chemistry
Calcium - analysis
Calcium Compounds - chemistry
Chemical Precipitation
Crystal growth
Crystallization
Crystallography, X-Ray
Dentistry
dissolution
Drug Combinations
Durapatite - analysis
Electron Probe Microanalysis
hydroxyapatite
MTA
Oxides - chemistry
Phosphorus - analysis
Root Canal Filling Materials - chemistry
Silicates - chemistry
Silicon - analysis
Spectrophotometry, Atomic
title Elemental Analysis of Crystal Precipitate from Gray and White MTA
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