Large-Domain Colloidal Crystal Films Fabricated Using a Fluidic Cell

Large-Domain Colloidal Crystal Films Fabricated Using a Fluidic Cell

The growth of colloidal crystal films from a dispersion of monodispersed silica spheres using a simple cell with one opening was investigated. Colloidal crystal films with large domain sizes were successfully fabricated almost over the cell (∼10 cm2) without applying any external force at room tempe...

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Veröffentlicht in:Langmuir 2005-06, Vol.21 (12), p.5367-5371
Hauptverfasser: Ishii, Masahiko, Nakamura, Hiroshi, Nakano, Hideyuki, Tsukigase, Azusa, Harada, Masashi
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Sprache:eng
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Chemistry
Colloidal state and disperse state
Exact sciences and technology
General and physical chemistry
Physical and chemical studies. Granulometry. Electrokinetic phenomena
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container_issue 12
container_start_page 5367
container_title Langmuir
container_volume 21
creator Ishii, Masahiko
Nakamura, Hiroshi
Nakano, Hideyuki
Tsukigase, Azusa
Harada, Masashi
description The growth of colloidal crystal films from a dispersion of monodispersed silica spheres using a simple cell with one opening was investigated. Colloidal crystal films with large domain sizes were successfully fabricated almost over the cell (∼10 cm2) without applying any external force at room temperature. During the drying process, three distinct conditions were observed, in each of which the films exhibited different optical properties. Films with high transmittance were formed in the first stage. Upon further solvent evaporation, the films entered a medium transmittance state via an extremely low transmittance state. Angle-resolved reflection spectroscopy, which was used to analyze the three conditions, revealed that close-packed arrays with water-filled spaces between were formed in the first stage. One-directional flow was generated in the cell because water evaporation occurred only at the opening. The flow caused the spheres to be arranged epitaxially, resulting in a large domain size.
doi_str_mv 10.1021/la050124v
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subjects Chemistry
Colloidal state and disperse state
Exact sciences and technology
General and physical chemistry
Physical and chemical studies. Granulometry. Electrokinetic phenomena
title Large-Domain Colloidal Crystal Films Fabricated Using a Fluidic Cell
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