validated gas chromatographic method for the evaluation of enzymatic enantioselectivity in kinetic resolution applications

An enantioselective gas chromatography (GC) method has been developed and validated for determination of the enantiomers of citronellol in kinetic resolution experiments. S-(-)-β-Citronellol is a precursor of rose oxide. After solid-phase extraction (SPE) with ethyl acetate, the enantiomers of R-(+)...

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Veröffentlicht in:	Journal of separation science 2005-04, Vol.28 (6), p.501-505
Hauptverfasser:	Boersma, Ykelien L, Scheltinga, Paula C, Dröge, Melloney J, Bos, Rein, Quax, Wim J
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Bacillus subtilis lipase A Bioconversions. Hemisynthesis Biological and medical sciences Biotechnology Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Gas - methods Citronellol Enantiomeric separation Enantioselective gas chromatography Enzymes - chemistry Enzymes - metabolism Evaluation Studies as Topic Exact sciences and technology Fundamental and applied biological sciences. Psychology Gas chromatographic methods Kinetic resolution Kinetics Methods. Procedures. Technologies Monoterpenes - chemistry Reproducibility of Results Stereoisomerism
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