Simultaneous Determination of Anthraquinones, Their 8-β-D-Glucosides, and Sennosides of Rhei Rhizoma by Capillary Electrophoresis
The simultaneous separation and determination of major anthraquinones (emodin, chrysophanol, rhein and their glucosides, aloe-emodin, sennoside A, and sennoside B) of Rhei Rhizoma were achieved by cyclodextrin modified capillary zone electrophoresis. The running electrolyte used in this method was 0...
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| Veröffentlicht in: | Chemical & pharmaceutical bulletin 2005, Vol.53(5), pp.573-575 |
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| container_title | Chemical & pharmaceutical bulletin |
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| creator | Koyama, Junko Morita, Izumi Fujiyoshi, Hirotaka Kobayashi, Norihiro |
| description | The simultaneous separation and determination of major anthraquinones (emodin, chrysophanol, rhein and their glucosides, aloe-emodin, sennoside A, and sennoside B) of Rhei Rhizoma were achieved by cyclodextrin modified capillary zone electrophoresis. The running electrolyte used in this method was 0.005 M α-cyclodextrin in 0.03 M borate buffer (pH 10.0) containing 20% acetonitrile, with an applied voltage of 20 kV. |
| doi_str_mv | 10.1248/cpb.53.573 |
| format | Article |
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The running electrolyte used in this method was 0.005 M α-cyclodextrin in 0.03 M borate buffer (pH 10.0) containing 20% acetonitrile, with an applied voltage of 20 kV.</description><identifier>ISSN: 0009-2363</identifier><identifier>EISSN: 1347-5223</identifier><identifier>DOI: 10.1248/cpb.53.573</identifier><identifier>PMID: 15863933</identifier><language>eng</language><publisher>Japan: The Pharmaceutical Society of Japan</publisher><subject>anthraquinone glucoside ; Anthraquinones - chemistry ; Anthraquinones - isolation & purification ; chrysophanol ; cyclodextrin modified capillary zone electrophoresis ; Electrophoresis, Capillary - methods ; emodin ; Glucosides - chemistry ; Glucosides - isolation & purification ; Plant Extracts - chemistry ; Plant Extracts - isolation & purification ; Plant Preparations - chemistry ; Plant Preparations - isolation & purification ; rhein ; Rheum ; Senna Extract ; sennoside</subject><ispartof>Chemical and Pharmaceutical Bulletin, 2005, Vol.53(5), pp.573-575</ispartof><rights>2005 The Pharmaceutical Society of Japan</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c443t-f5b470e20074b304d6adc77374be06a4cc3982b4867830a673815fcf322cb2553</citedby><cites>FETCH-LOGICAL-c443t-f5b470e20074b304d6adc77374be06a4cc3982b4867830a673815fcf322cb2553</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,778,782,1879,27907,27908</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/15863933$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Koyama, Junko</creatorcontrib><creatorcontrib>Morita, Izumi</creatorcontrib><creatorcontrib>Fujiyoshi, Hirotaka</creatorcontrib><creatorcontrib>Kobayashi, Norihiro</creatorcontrib><title>Simultaneous Determination of Anthraquinones, Their 8-β-D-Glucosides, and Sennosides of Rhei Rhizoma by Capillary Electrophoresis</title><title>Chemical & pharmaceutical bulletin</title><addtitle>Chem. Pharm. Bull.</addtitle><description>The simultaneous separation and determination of major anthraquinones (emodin, chrysophanol, rhein and their glucosides, aloe-emodin, sennoside A, and sennoside B) of Rhei Rhizoma were achieved by cyclodextrin modified capillary zone electrophoresis. The running electrolyte used in this method was 0.005 M α-cyclodextrin in 0.03 M borate buffer (pH 10.0) containing 20% acetonitrile, with an applied voltage of 20 kV.</description><subject>anthraquinone glucoside</subject><subject>Anthraquinones - chemistry</subject><subject>Anthraquinones - isolation & purification</subject><subject>chrysophanol</subject><subject>cyclodextrin modified capillary zone electrophoresis</subject><subject>Electrophoresis, Capillary - methods</subject><subject>emodin</subject><subject>Glucosides - chemistry</subject><subject>Glucosides - isolation & purification</subject><subject>Plant Extracts - chemistry</subject><subject>Plant Extracts - isolation & purification</subject><subject>Plant Preparations - chemistry</subject><subject>Plant Preparations - isolation & purification</subject><subject>rhein</subject><subject>Rheum</subject><subject>Senna Extract</subject><subject>sennoside</subject><issn>0009-2363</issn><issn>1347-5223</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpFkMFu1DAQhi0EokvhwgMgnzhUZHE8dpw9oWpbClIlJFrOluNMWFeJndrOoRx5JB6EZ8LLrtrLjEbzza9_fkLe1mxdc9F-tHO3lrCWCp6RVQ1CVZJzeE5WjLFNxaGBE_IqpTvGuGQKXpKTWrYNbABW5PeNm5YxG49hSfQCM8bJeZNd8DQM9NznXTT3i_PBY_pAb3foIm2rv3-qi-pqXGxIrt8vjO_pDXp_mPen3wtaivsVJkO7B7o1sxtHEx_o5Yg2xzDvQsTk0mvyYjBjwjfHfkp-fL683X6prr9dfd2eX1dWCMjVIDuhGHLGlOiAib4xvVUKyoSsMcJa2LS8E22jWmCmUdDWcrADcG47LiWckvcH3TmG-wVT1pNLFoun_8_rcseYFFDAswNoY0gp4qDn6KbiXNdM7xPXJXEtQZfEC_zuqLp0E_ZP6DHiAnw6AHcpm5_4CJiYnR3xUetYFDxtdiZq9PAPyeaUtQ</recordid><startdate>20050501</startdate><enddate>20050501</enddate><creator>Koyama, Junko</creator><creator>Morita, Izumi</creator><creator>Fujiyoshi, Hirotaka</creator><creator>Kobayashi, Norihiro</creator><general>The Pharmaceutical Society of Japan</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20050501</creationdate><title>Simultaneous Determination of Anthraquinones, Their 8-β-D-Glucosides, and Sennosides of Rhei Rhizoma by Capillary Electrophoresis</title><author>Koyama, Junko ; Morita, Izumi ; Fujiyoshi, Hirotaka ; Kobayashi, Norihiro</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c443t-f5b470e20074b304d6adc77374be06a4cc3982b4867830a673815fcf322cb2553</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>anthraquinone glucoside</topic><topic>Anthraquinones - chemistry</topic><topic>Anthraquinones - isolation & purification</topic><topic>chrysophanol</topic><topic>cyclodextrin modified capillary zone electrophoresis</topic><topic>Electrophoresis, Capillary - methods</topic><topic>emodin</topic><topic>Glucosides - chemistry</topic><topic>Glucosides - isolation & purification</topic><topic>Plant Extracts - chemistry</topic><topic>Plant Extracts - isolation & purification</topic><topic>Plant Preparations - chemistry</topic><topic>Plant Preparations - isolation & purification</topic><topic>rhein</topic><topic>Rheum</topic><topic>Senna Extract</topic><topic>sennoside</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Koyama, Junko</creatorcontrib><creatorcontrib>Morita, Izumi</creatorcontrib><creatorcontrib>Fujiyoshi, Hirotaka</creatorcontrib><creatorcontrib>Kobayashi, Norihiro</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Chemical & pharmaceutical bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Koyama, Junko</au><au>Morita, Izumi</au><au>Fujiyoshi, Hirotaka</au><au>Kobayashi, Norihiro</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Simultaneous Determination of Anthraquinones, Their 8-β-D-Glucosides, and Sennosides of Rhei Rhizoma by Capillary Electrophoresis</atitle><jtitle>Chemical & pharmaceutical bulletin</jtitle><addtitle>Chem. Pharm. Bull.</addtitle><date>2005-05-01</date><risdate>2005</risdate><volume>53</volume><issue>5</issue><spage>573</spage><epage>575</epage><pages>573-575</pages><issn>0009-2363</issn><eissn>1347-5223</eissn><abstract>The simultaneous separation and determination of major anthraquinones (emodin, chrysophanol, rhein and their glucosides, aloe-emodin, sennoside A, and sennoside B) of Rhei Rhizoma were achieved by cyclodextrin modified capillary zone electrophoresis. The running electrolyte used in this method was 0.005 M α-cyclodextrin in 0.03 M borate buffer (pH 10.0) containing 20% acetonitrile, with an applied voltage of 20 kV.</abstract><cop>Japan</cop><pub>The Pharmaceutical Society of Japan</pub><pmid>15863933</pmid><doi>10.1248/cpb.53.573</doi><tpages>3</tpages><oa>free_for_read</oa></addata></record> |
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| language | eng |
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| source | J-STAGE Free; MEDLINE; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Free Full-Text Journals in Chemistry |
| subjects | anthraquinone glucoside Anthraquinones - chemistry Anthraquinones - isolation & purification chrysophanol cyclodextrin modified capillary zone electrophoresis Electrophoresis, Capillary - methods emodin Glucosides - chemistry Glucosides - isolation & purification Plant Extracts - chemistry Plant Extracts - isolation & purification Plant Preparations - chemistry Plant Preparations - isolation & purification rhein Rheum Senna Extract sennoside |
| title | Simultaneous Determination of Anthraquinones, Their 8-β-D-Glucosides, and Sennosides of Rhei Rhizoma by Capillary Electrophoresis |
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