Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers
The influence of several experimental parameters on the ultrasonic extraction of Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and s...
Gespeichert in:
| Veröffentlicht in: | Ultrasonics sonochemistry 2006-04, Vol.13 (3), p.242-250 |
|---|---|
| Hauptverfasser: | , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 250 |
|---|---|
| container_issue | 3 |
| container_start_page | 242 |
| container_title | Ultrasonics sonochemistry |
| container_volume | 13 |
| creator | Soares Melecchi, Maria Inês Péres, Valéria Flores Dariva, Cláudio Zini, Claudia Alcaraz Abad, Fernanda Contieri Martinez, Migdália Miranda Caramão, Elina Bastos |
| description | The influence of several experimental parameters on the ultrasonic extraction of
Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and solvent polarity. The optimized procedure employed 5
g of ground flowers, 150
mL of methanol and 140
min of extraction. The extracts were fractionated using preparative silica columns and the resulting fractions were analyzed by GC/MS. Some saturated hydrocarbons, fatty acids, fatty acid methyl esters, phytosterols, and vitamin E were identified in the plant extracts. |
| doi_str_mv | 10.1016/j.ultsonch.2005.02.003 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_67700047</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S1350417705000325</els_id><sourcerecordid>67700047</sourcerecordid><originalsourceid>FETCH-LOGICAL-c449t-a0a099512b3284c9e620e2b1dbfc5e2338ee436a6bc935d5181ca0db84ae76403</originalsourceid><addsrcrecordid>eNqFkE1r3DAQhkVpyPdfCL60NzujL9u6tYS0CSyEQHIWsjxmtdjWVpLz0V9fbXdLjj3Ny_DMaPQQckWhokDr6021jCn62a4rBiArYBUA_0ROadvwkrWs_Zwzl1AK2jQn5CzGDWRCMTgmJ1QqxWuuTsnjwza5yf02yfm58EOR1ljkvc7uO_iWgrF_44Rp7fsdc-c6F-0Si-RGZyzmtKqKYfSvGOIFORrMGPHyUM_J84_bp5u7cvXw8_7m-6q0QqhUGjCglKSs46wVVmHNAFlH-26wEhnnLaLgtak7q7jsJW2pNdB3rTDY1AL4Ofm637sN_teCMekpH4XjaGb0S9R10-QPiyaD9R60wccYcNDb4CYT3jUFvZOpN_qfTL2TqYHprCoPXh1eWLoJ-4-xg70MfDkAJlozDsHM1sUPrpGCKSYz923PYfbx4jDoaB3OFnsX0Cbde_e_W_4AyquW8A</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>67700047</pqid></control><display><type>article</type><title>Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers</title><source>MEDLINE</source><source>Elsevier ScienceDirect Journals Complete</source><creator>Soares Melecchi, Maria Inês ; Péres, Valéria Flores ; Dariva, Cláudio ; Zini, Claudia Alcaraz ; Abad, Fernanda Contieri ; Martinez, Migdália Miranda ; Caramão, Elina Bastos</creator><creatorcontrib>Soares Melecchi, Maria Inês ; Péres, Valéria Flores ; Dariva, Cláudio ; Zini, Claudia Alcaraz ; Abad, Fernanda Contieri ; Martinez, Migdália Miranda ; Caramão, Elina Bastos</creatorcontrib><description>The influence of several experimental parameters on the ultrasonic extraction of
Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and solvent polarity. The optimized procedure employed 5
g of ground flowers, 150
mL of methanol and 140
min of extraction. The extracts were fractionated using preparative silica columns and the resulting fractions were analyzed by GC/MS. Some saturated hydrocarbons, fatty acids, fatty acid methyl esters, phytosterols, and vitamin E were identified in the plant extracts.</description><identifier>ISSN: 1350-4177</identifier><identifier>EISSN: 1873-2828</identifier><identifier>DOI: 10.1016/j.ultsonch.2005.02.003</identifier><identifier>PMID: 15993639</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Chemistry ; Exact sciences and technology ; Flowers - chemistry ; GC/MS ; General and physical chemistry ; Hibiscus - chemistry ; Hibiscus tiliaceus L ; Physical chemistry of induced reactions (with radiations, particles and ultrasonics) ; Plant Extracts - analysis ; Solvents - chemistry ; Sonication ; Ultrasonic chemistry</subject><ispartof>Ultrasonics sonochemistry, 2006-04, Vol.13 (3), p.242-250</ispartof><rights>2005 Elsevier B.V.</rights><rights>2006 INIST-CNRS</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c449t-a0a099512b3284c9e620e2b1dbfc5e2338ee436a6bc935d5181ca0db84ae76403</citedby><cites>FETCH-LOGICAL-c449t-a0a099512b3284c9e620e2b1dbfc5e2338ee436a6bc935d5181ca0db84ae76403</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S1350417705000325$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17542925$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/15993639$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Soares Melecchi, Maria Inês</creatorcontrib><creatorcontrib>Péres, Valéria Flores</creatorcontrib><creatorcontrib>Dariva, Cláudio</creatorcontrib><creatorcontrib>Zini, Claudia Alcaraz</creatorcontrib><creatorcontrib>Abad, Fernanda Contieri</creatorcontrib><creatorcontrib>Martinez, Migdália Miranda</creatorcontrib><creatorcontrib>Caramão, Elina Bastos</creatorcontrib><title>Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers</title><title>Ultrasonics sonochemistry</title><addtitle>Ultrason Sonochem</addtitle><description>The influence of several experimental parameters on the ultrasonic extraction of
Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and solvent polarity. The optimized procedure employed 5
g of ground flowers, 150
mL of methanol and 140
min of extraction. The extracts were fractionated using preparative silica columns and the resulting fractions were analyzed by GC/MS. Some saturated hydrocarbons, fatty acids, fatty acid methyl esters, phytosterols, and vitamin E were identified in the plant extracts.</description><subject>Chemistry</subject><subject>Exact sciences and technology</subject><subject>Flowers - chemistry</subject><subject>GC/MS</subject><subject>General and physical chemistry</subject><subject>Hibiscus - chemistry</subject><subject>Hibiscus tiliaceus L</subject><subject>Physical chemistry of induced reactions (with radiations, particles and ultrasonics)</subject><subject>Plant Extracts - analysis</subject><subject>Solvents - chemistry</subject><subject>Sonication</subject><subject>Ultrasonic chemistry</subject><issn>1350-4177</issn><issn>1873-2828</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkE1r3DAQhkVpyPdfCL60NzujL9u6tYS0CSyEQHIWsjxmtdjWVpLz0V9fbXdLjj3Ny_DMaPQQckWhokDr6021jCn62a4rBiArYBUA_0ROadvwkrWs_Zwzl1AK2jQn5CzGDWRCMTgmJ1QqxWuuTsnjwza5yf02yfm58EOR1ljkvc7uO_iWgrF_44Rp7fsdc-c6F-0Si-RGZyzmtKqKYfSvGOIFORrMGPHyUM_J84_bp5u7cvXw8_7m-6q0QqhUGjCglKSs46wVVmHNAFlH-26wEhnnLaLgtak7q7jsJW2pNdB3rTDY1AL4Ofm637sN_teCMekpH4XjaGb0S9R10-QPiyaD9R60wccYcNDb4CYT3jUFvZOpN_qfTL2TqYHprCoPXh1eWLoJ-4-xg70MfDkAJlozDsHM1sUPrpGCKSYz923PYfbx4jDoaB3OFnsX0Cbde_e_W_4AyquW8A</recordid><startdate>20060401</startdate><enddate>20060401</enddate><creator>Soares Melecchi, Maria Inês</creator><creator>Péres, Valéria Flores</creator><creator>Dariva, Cláudio</creator><creator>Zini, Claudia Alcaraz</creator><creator>Abad, Fernanda Contieri</creator><creator>Martinez, Migdália Miranda</creator><creator>Caramão, Elina Bastos</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20060401</creationdate><title>Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers</title><author>Soares Melecchi, Maria Inês ; Péres, Valéria Flores ; Dariva, Cláudio ; Zini, Claudia Alcaraz ; Abad, Fernanda Contieri ; Martinez, Migdália Miranda ; Caramão, Elina Bastos</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c449t-a0a099512b3284c9e620e2b1dbfc5e2338ee436a6bc935d5181ca0db84ae76403</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Chemistry</topic><topic>Exact sciences and technology</topic><topic>Flowers - chemistry</topic><topic>GC/MS</topic><topic>General and physical chemistry</topic><topic>Hibiscus - chemistry</topic><topic>Hibiscus tiliaceus L</topic><topic>Physical chemistry of induced reactions (with radiations, particles and ultrasonics)</topic><topic>Plant Extracts - analysis</topic><topic>Solvents - chemistry</topic><topic>Sonication</topic><topic>Ultrasonic chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Soares Melecchi, Maria Inês</creatorcontrib><creatorcontrib>Péres, Valéria Flores</creatorcontrib><creatorcontrib>Dariva, Cláudio</creatorcontrib><creatorcontrib>Zini, Claudia Alcaraz</creatorcontrib><creatorcontrib>Abad, Fernanda Contieri</creatorcontrib><creatorcontrib>Martinez, Migdália Miranda</creatorcontrib><creatorcontrib>Caramão, Elina Bastos</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Ultrasonics sonochemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Soares Melecchi, Maria Inês</au><au>Péres, Valéria Flores</au><au>Dariva, Cláudio</au><au>Zini, Claudia Alcaraz</au><au>Abad, Fernanda Contieri</au><au>Martinez, Migdália Miranda</au><au>Caramão, Elina Bastos</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers</atitle><jtitle>Ultrasonics sonochemistry</jtitle><addtitle>Ultrason Sonochem</addtitle><date>2006-04-01</date><risdate>2006</risdate><volume>13</volume><issue>3</issue><spage>242</spage><epage>250</epage><pages>242-250</pages><issn>1350-4177</issn><eissn>1873-2828</eissn><abstract>The influence of several experimental parameters on the ultrasonic extraction of
Hibiscus tiliaceus L. flowers were investigated: extraction time, solvent polarity, sample amount, solvent volume and sample particle size. It was concluded that the most influential variables were extraction time and solvent polarity. The optimized procedure employed 5
g of ground flowers, 150
mL of methanol and 140
min of extraction. The extracts were fractionated using preparative silica columns and the resulting fractions were analyzed by GC/MS. Some saturated hydrocarbons, fatty acids, fatty acid methyl esters, phytosterols, and vitamin E were identified in the plant extracts.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>15993639</pmid><doi>10.1016/j.ultsonch.2005.02.003</doi><tpages>9</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1350-4177 |
| ispartof | Ultrasonics sonochemistry, 2006-04, Vol.13 (3), p.242-250 |
| issn | 1350-4177 1873-2828 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_67700047 |
| source | MEDLINE; Elsevier ScienceDirect Journals Complete |
| subjects | Chemistry Exact sciences and technology Flowers - chemistry GC/MS General and physical chemistry Hibiscus - chemistry Hibiscus tiliaceus L Physical chemistry of induced reactions (with radiations, particles and ultrasonics) Plant Extracts - analysis Solvents - chemistry Sonication Ultrasonic chemistry |
| title | Optimization of the sonication extraction method of Hibiscus tiliaceus L. flowers |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-21T18%3A38%3A20IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Optimization%20of%20the%20sonication%20extraction%20method%20of%20Hibiscus%20tiliaceus%20L.%20flowers&rft.jtitle=Ultrasonics%20sonochemistry&rft.au=Soares%20Melecchi,%20Maria%20In%C3%AAs&rft.date=2006-04-01&rft.volume=13&rft.issue=3&rft.spage=242&rft.epage=250&rft.pages=242-250&rft.issn=1350-4177&rft.eissn=1873-2828&rft_id=info:doi/10.1016/j.ultsonch.2005.02.003&rft_dat=%3Cproquest_cross%3E67700047%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=67700047&rft_id=info:pmid/15993639&rft_els_id=S1350417705000325&rfr_iscdi=true |