Directional lithium hydride Compton profiles of 0.1% statistical accuracy
The present status and accuracy of determining the electron momentum density from experimental Compton profiles is reviewed. The new spectrometers operating at third‐generation synchrotron radiation sources have made possible measurements with 0.1% statistical accuracy at the Compton peak. A compara...
Gespeichert in:
Veröffentlicht in: | Journal of synchrotron radiation 2009-09, Vol.16 (5), p.672-682 |
---|---|
Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext bestellen |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | 682 |
---|---|
container_issue | 5 |
container_start_page | 672 |
container_title | Journal of synchrotron radiation |
container_volume | 16 |
creator | Huotari, Simo Boldrini, Barbara Honkimäki, Veijo Suortti, Pekka Weyrich, Wolf |
description | The present status and accuracy of determining the electron momentum density from experimental Compton profiles is reviewed. The new spectrometers operating at third‐generation synchrotron radiation sources have made possible measurements with 0.1% statistical accuracy at the Compton peak. A comparable accuracy of the Compton profiles is achieved only after careful corrections for departures from the impulse approximation, effects of multiple scattering, and variations in the analyser response function. Detailed descriptions are given of the correction procedures applied to the data collected by the Johann‐type scanning spectrometer that is one of the Compton spectrometers in use at the ESRF. Special attention is paid to the calculation and correction of the glitches that are caused by extra reflections of the analyser crystal. The Fourier transform of the Compton profile, the reciprocal form factor, is calculated, and its use in data treatment and presentation is discussed. |
doi_str_mv | 10.1107/S0909049509029112 |
format | Article |
fullrecord | <record><control><sourceid>proquest_24P</sourceid><recordid>TN_cdi_proquest_miscellaneous_67617180</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>67617180</sourcerecordid><originalsourceid>FETCH-LOGICAL-c4609-61fc8982b501e5ca892b8abc31d8e888ee4af94d3ffebec405830154d2f3de8a3</originalsourceid><addsrcrecordid>eNqFkEFP2zAYhq2JiTLGD-CCcoFbwF8cJ_YRyoAytmlia-FkOc5nYUiaYidi_ffz1Iohcags2T68z_vZDyH7QI8BaHlyS2VcueRxzyRA9oHsQEFpysuSb725j8inEB4phaLM2DYZgSyBFXm2QybnzqPpXTfXTdK4_sENbfKwrL2rMRl37aLv5snCd9Y1GJLOJnH0YRJ63bvQOxMhbczgtVl-Jh-tbgLurc9d8vviy6_xVXrz43IyPr1JTV5QmRZgjZAiqzgF5EYLmVVCV4ZBLVAIgZhrK_OaWYsVmpxywSjwvM4sq1FotkuOVr3xVc8Dhl61LhhsGj3HbgiqKAsoQdCNQZYLzkHyGIRV0PguBI9WLbxrtV8qoOqfaPVOdGQO1uVD1WL9n1ibjQGxCrxEc8vNjer69v7rlNNCRjRdoVEx_nlFtX-Kn2MlV7Pvl-rbjE4vpndn6if7Cyetl6w</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>34855195</pqid></control><display><type>article</type><title>Directional lithium hydride Compton profiles of 0.1% statistical accuracy</title><source>Wiley Online Library Open Access</source><creator>Huotari, Simo ; Boldrini, Barbara ; Honkimäki, Veijo ; Suortti, Pekka ; Weyrich, Wolf</creator><creatorcontrib>Huotari, Simo ; Boldrini, Barbara ; Honkimäki, Veijo ; Suortti, Pekka ; Weyrich, Wolf</creatorcontrib><description>The present status and accuracy of determining the electron momentum density from experimental Compton profiles is reviewed. The new spectrometers operating at third‐generation synchrotron radiation sources have made possible measurements with 0.1% statistical accuracy at the Compton peak. A comparable accuracy of the Compton profiles is achieved only after careful corrections for departures from the impulse approximation, effects of multiple scattering, and variations in the analyser response function. Detailed descriptions are given of the correction procedures applied to the data collected by the Johann‐type scanning spectrometer that is one of the Compton spectrometers in use at the ESRF. Special attention is paid to the calculation and correction of the glitches that are caused by extra reflections of the analyser crystal. The Fourier transform of the Compton profile, the reciprocal form factor, is calculated, and its use in data treatment and presentation is discussed.</description><identifier>ISSN: 1600-5775</identifier><identifier>ISSN: 0909-0495</identifier><identifier>EISSN: 1600-5775</identifier><identifier>DOI: 10.1107/S0909049509029112</identifier><identifier>PMID: 19713642</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>directional Compton profiles ; electron momentum density ; lithium hydride ; reciprocal form factor</subject><ispartof>Journal of synchrotron radiation, 2009-09, Vol.16 (5), p.672-682</ispartof><rights>International Union of Crystallography, 2009</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4609-61fc8982b501e5ca892b8abc31d8e888ee4af94d3ffebec405830154d2f3de8a3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1107%2FS0909049509029112$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1107%2FS0909049509029112$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,11542,27903,27904,45553,45554,46030,46454</link.rule.ids><linktorsrc>$$Uhttps://onlinelibrary.wiley.com/doi/abs/10.1107%2FS0909049509029112$$EView_record_in_Wiley-Blackwell$$FView_record_in_$$GWiley-Blackwell</linktorsrc><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/19713642$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Huotari, Simo</creatorcontrib><creatorcontrib>Boldrini, Barbara</creatorcontrib><creatorcontrib>Honkimäki, Veijo</creatorcontrib><creatorcontrib>Suortti, Pekka</creatorcontrib><creatorcontrib>Weyrich, Wolf</creatorcontrib><title>Directional lithium hydride Compton profiles of 0.1% statistical accuracy</title><title>Journal of synchrotron radiation</title><addtitle>J. Synchrotron Rad</addtitle><description>The present status and accuracy of determining the electron momentum density from experimental Compton profiles is reviewed. The new spectrometers operating at third‐generation synchrotron radiation sources have made possible measurements with 0.1% statistical accuracy at the Compton peak. A comparable accuracy of the Compton profiles is achieved only after careful corrections for departures from the impulse approximation, effects of multiple scattering, and variations in the analyser response function. Detailed descriptions are given of the correction procedures applied to the data collected by the Johann‐type scanning spectrometer that is one of the Compton spectrometers in use at the ESRF. Special attention is paid to the calculation and correction of the glitches that are caused by extra reflections of the analyser crystal. The Fourier transform of the Compton profile, the reciprocal form factor, is calculated, and its use in data treatment and presentation is discussed.</description><subject>directional Compton profiles</subject><subject>electron momentum density</subject><subject>lithium hydride</subject><subject>reciprocal form factor</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNqFkEFP2zAYhq2JiTLGD-CCcoFbwF8cJ_YRyoAytmlia-FkOc5nYUiaYidi_ffz1Iohcags2T68z_vZDyH7QI8BaHlyS2VcueRxzyRA9oHsQEFpysuSb725j8inEB4phaLM2DYZgSyBFXm2QybnzqPpXTfXTdK4_sENbfKwrL2rMRl37aLv5snCd9Y1GJLOJnH0YRJ63bvQOxMhbczgtVl-Jh-tbgLurc9d8vviy6_xVXrz43IyPr1JTV5QmRZgjZAiqzgF5EYLmVVCV4ZBLVAIgZhrK_OaWYsVmpxywSjwvM4sq1FotkuOVr3xVc8Dhl61LhhsGj3HbgiqKAsoQdCNQZYLzkHyGIRV0PguBI9WLbxrtV8qoOqfaPVOdGQO1uVD1WL9n1ibjQGxCrxEc8vNjer69v7rlNNCRjRdoVEx_nlFtX-Kn2MlV7Pvl-rbjE4vpndn6if7Cyetl6w</recordid><startdate>200909</startdate><enddate>200909</enddate><creator>Huotari, Simo</creator><creator>Boldrini, Barbara</creator><creator>Honkimäki, Veijo</creator><creator>Suortti, Pekka</creator><creator>Weyrich, Wolf</creator><general>International Union of Crystallography</general><scope>BSCLL</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>200909</creationdate><title>Directional lithium hydride Compton profiles of 0.1% statistical accuracy</title><author>Huotari, Simo ; Boldrini, Barbara ; Honkimäki, Veijo ; Suortti, Pekka ; Weyrich, Wolf</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4609-61fc8982b501e5ca892b8abc31d8e888ee4af94d3ffebec405830154d2f3de8a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>directional Compton profiles</topic><topic>electron momentum density</topic><topic>lithium hydride</topic><topic>reciprocal form factor</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Huotari, Simo</creatorcontrib><creatorcontrib>Boldrini, Barbara</creatorcontrib><creatorcontrib>Honkimäki, Veijo</creatorcontrib><creatorcontrib>Suortti, Pekka</creatorcontrib><creatorcontrib>Weyrich, Wolf</creatorcontrib><collection>Istex</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of synchrotron radiation</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Huotari, Simo</au><au>Boldrini, Barbara</au><au>Honkimäki, Veijo</au><au>Suortti, Pekka</au><au>Weyrich, Wolf</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Directional lithium hydride Compton profiles of 0.1% statistical accuracy</atitle><jtitle>Journal of synchrotron radiation</jtitle><addtitle>J. Synchrotron Rad</addtitle><date>2009-09</date><risdate>2009</risdate><volume>16</volume><issue>5</issue><spage>672</spage><epage>682</epage><pages>672-682</pages><issn>1600-5775</issn><issn>0909-0495</issn><eissn>1600-5775</eissn><abstract>The present status and accuracy of determining the electron momentum density from experimental Compton profiles is reviewed. The new spectrometers operating at third‐generation synchrotron radiation sources have made possible measurements with 0.1% statistical accuracy at the Compton peak. A comparable accuracy of the Compton profiles is achieved only after careful corrections for departures from the impulse approximation, effects of multiple scattering, and variations in the analyser response function. Detailed descriptions are given of the correction procedures applied to the data collected by the Johann‐type scanning spectrometer that is one of the Compton spectrometers in use at the ESRF. Special attention is paid to the calculation and correction of the glitches that are caused by extra reflections of the analyser crystal. The Fourier transform of the Compton profile, the reciprocal form factor, is calculated, and its use in data treatment and presentation is discussed.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><pmid>19713642</pmid><doi>10.1107/S0909049509029112</doi><tpages>11</tpages><oa>free_for_read</oa></addata></record> |
fulltext | fulltext_linktorsrc |
identifier | ISSN: 1600-5775 |
ispartof | Journal of synchrotron radiation, 2009-09, Vol.16 (5), p.672-682 |
issn | 1600-5775 0909-0495 1600-5775 |
language | eng |
recordid | cdi_proquest_miscellaneous_67617180 |
source | Wiley Online Library Open Access |
subjects | directional Compton profiles electron momentum density lithium hydride reciprocal form factor |
title | Directional lithium hydride Compton profiles of 0.1% statistical accuracy |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T07%3A52%3A08IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_24P&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Directional%20lithium%20hydride%20Compton%20profiles%20of%200.1%25%20statistical%20accuracy&rft.jtitle=Journal%20of%20synchrotron%20radiation&rft.au=Huotari,%20Simo&rft.date=2009-09&rft.volume=16&rft.issue=5&rft.spage=672&rft.epage=682&rft.pages=672-682&rft.issn=1600-5775&rft.eissn=1600-5775&rft_id=info:doi/10.1107/S0909049509029112&rft_dat=%3Cproquest_24P%3E67617180%3C/proquest_24P%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=34855195&rft_id=info:pmid/19713642&rfr_iscdi=true |