Facilitated column selection in pharmaceutical analyses using a simple column classification system
In this paper, the performance of a previously developed classification system applied to pharmaceutical chromatographic analyses, is investigated. The separation of seven different drug substances from their respective impurities was studied. The chromatographic procedure for acetylsalicylic acid,...
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Veröffentlicht in: | Journal of Chromatography A 2006-01, Vol.1101 (1), p.103-114 |
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container_title | Journal of Chromatography A |
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creator | Visky, Dóra Haghedooren, Erik Dehouck, Pieter Kovács, Zsuzsanna Kóczián, Kristof Noszál, Béla Hoogmartens, Jos Adams, Erwin |
description | In this paper, the performance of a previously developed classification system applied to pharmaceutical chromatographic analyses, is investigated. The separation of seven different drug substances from their respective impurities was studied. The chromatographic procedure for acetylsalicylic acid, clindamycin hydrochloride, buflomedil hydrochloride, chloramphenicol sodium succinate, nimesulide and phenoxymethylpenicillin was performed according to the corresponding European Pharmacopoeia (Ph. Eur.) monograph. The separation of dihydrostreptomycin sulphate was performed according to the literature. It is shown that the column ranking system is a helpful tool in the selection of a suitable column in these analyses. |
doi_str_mv | 10.1016/j.chroma.2005.09.069 |
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The separation of seven different drug substances from their respective impurities was studied. The chromatographic procedure for acetylsalicylic acid, clindamycin hydrochloride, buflomedil hydrochloride, chloramphenicol sodium succinate, nimesulide and phenoxymethylpenicillin was performed according to the corresponding European Pharmacopoeia (Ph. Eur.) monograph. The separation of dihydrostreptomycin sulphate was performed according to the literature. It is shown that the column ranking system is a helpful tool in the selection of a suitable column in these analyses.</description><identifier>ISSN: 0021-9673</identifier><identifier>DOI: 10.1016/j.chroma.2005.09.069</identifier><identifier>PMID: 16242136</identifier><identifier>CODEN: JOCRAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject><![CDATA[Analysis ; Analytical chemistry ; Aspirin - isolation & purification ; Biological and medical sciences ; Chemistry ; Chloramphenicol - analogs & derivatives ; Chloramphenicol - isolation & purification ; Chromatographic methods and physical methods associated with chromatography ; Chromatographic tests ; Chromatography, Liquid - instrumentation ; Chromatography, Liquid - methods ; Clindamycin - isolation & purification ; Column characterisation ; Column classification ; Dihydrostreptomycin Sulfate - isolation & purification ; Exact sciences and technology ; General pharmacology ; Medical sciences ; Other chromatographic methods ; Penicillin V - isolation & purification ; Pharmaceutical Preparations - isolation & purification ; Pharmacology. Drug treatments ; Pyrrolidines - isolation & purification ; Sensitivity and Specificity ; Sulfonamides - isolation & purification]]></subject><ispartof>Journal of Chromatography A, 2006-01, Vol.1101 (1), p.103-114</ispartof><rights>2005 Elsevier B.V.</rights><rights>2006 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c390t-a61512be245b0bd2171e8580cf07a94ee5c63fb43e8eacfaf6a7ef0a5f2a04a63</citedby><cites>FETCH-LOGICAL-c390t-a61512be245b0bd2171e8580cf07a94ee5c63fb43e8eacfaf6a7ef0a5f2a04a63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0021967305018753$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=17373793$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/16242136$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Visky, Dóra</creatorcontrib><creatorcontrib>Haghedooren, Erik</creatorcontrib><creatorcontrib>Dehouck, Pieter</creatorcontrib><creatorcontrib>Kovács, Zsuzsanna</creatorcontrib><creatorcontrib>Kóczián, Kristof</creatorcontrib><creatorcontrib>Noszál, Béla</creatorcontrib><creatorcontrib>Hoogmartens, Jos</creatorcontrib><creatorcontrib>Adams, Erwin</creatorcontrib><title>Facilitated column selection in pharmaceutical analyses using a simple column classification system</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>In this paper, the performance of a previously developed classification system applied to pharmaceutical chromatographic analyses, is investigated. The separation of seven different drug substances from their respective impurities was studied. The chromatographic procedure for acetylsalicylic acid, clindamycin hydrochloride, buflomedil hydrochloride, chloramphenicol sodium succinate, nimesulide and phenoxymethylpenicillin was performed according to the corresponding European Pharmacopoeia (Ph. Eur.) monograph. The separation of dihydrostreptomycin sulphate was performed according to the literature. It is shown that the column ranking system is a helpful tool in the selection of a suitable column in these analyses.</description><subject>Analysis</subject><subject>Analytical chemistry</subject><subject>Aspirin - isolation & purification</subject><subject>Biological and medical sciences</subject><subject>Chemistry</subject><subject>Chloramphenicol - analogs & derivatives</subject><subject>Chloramphenicol - isolation & purification</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatographic tests</subject><subject>Chromatography, Liquid - instrumentation</subject><subject>Chromatography, Liquid - methods</subject><subject>Clindamycin - isolation & purification</subject><subject>Column characterisation</subject><subject>Column classification</subject><subject>Dihydrostreptomycin Sulfate - isolation & purification</subject><subject>Exact sciences and technology</subject><subject>General pharmacology</subject><subject>Medical sciences</subject><subject>Other chromatographic methods</subject><subject>Penicillin V - isolation & purification</subject><subject>Pharmaceutical Preparations - isolation & purification</subject><subject>Pharmacology. Drug treatments</subject><subject>Pyrrolidines - isolation & purification</subject><subject>Sensitivity and Specificity</subject><subject>Sulfonamides - isolation & purification</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2006</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kMFu1DAQQH0AtaXlDxDKBW6bjp3EXl-QUNVCpUpc6NmaOGPqlZMsngRp_74uu6g3NIe5vDcaPSE-SKglSH29q_1TnkesFUBXg61B2zfiAkDJjdWmORfvmHcA0oBRZ-JcatUq2egL4e_QxxQXXGio_JzWcaqYEvklzlMVp2r_hHlET-sSPaYKJ0wHJq5WjtOvCiuO4z7RP9UnZI6hoH99PvBC45V4GzAxvT_tS_F4d_vz5vvm4ce3-5uvDxvfWFg2qGUnVU-q7XroByWNpG23BR_AoG2JOq-b0LcNbQl9wKDRUADsgkJoUTeX4vPx7j7Pv1fixY2RPaWEE80rO206Y1tjC9geQZ9n5kzB7XMcMR-cBPcS1O3cMah7CerAuhK0aB9P99d-pOFVOtUswKcTgFxihYyTj_zKmaaMbQr35chRqfEnUnbsI02ehphLeTfM8f-fPAP1YZrI</recordid><startdate>20060106</startdate><enddate>20060106</enddate><creator>Visky, Dóra</creator><creator>Haghedooren, Erik</creator><creator>Dehouck, Pieter</creator><creator>Kovács, Zsuzsanna</creator><creator>Kóczián, Kristof</creator><creator>Noszál, Béla</creator><creator>Hoogmartens, Jos</creator><creator>Adams, Erwin</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20060106</creationdate><title>Facilitated column selection in pharmaceutical analyses using a simple column classification system</title><author>Visky, Dóra ; Haghedooren, Erik ; Dehouck, Pieter ; Kovács, Zsuzsanna ; Kóczián, Kristof ; Noszál, Béla ; Hoogmartens, Jos ; Adams, Erwin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-a61512be245b0bd2171e8580cf07a94ee5c63fb43e8eacfaf6a7ef0a5f2a04a63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2006</creationdate><topic>Analysis</topic><topic>Analytical chemistry</topic><topic>Aspirin - isolation & purification</topic><topic>Biological and medical sciences</topic><topic>Chemistry</topic><topic>Chloramphenicol - analogs & derivatives</topic><topic>Chloramphenicol - isolation & purification</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatographic tests</topic><topic>Chromatography, Liquid - instrumentation</topic><topic>Chromatography, Liquid - methods</topic><topic>Clindamycin - isolation & purification</topic><topic>Column characterisation</topic><topic>Column classification</topic><topic>Dihydrostreptomycin Sulfate - isolation & purification</topic><topic>Exact sciences and technology</topic><topic>General pharmacology</topic><topic>Medical sciences</topic><topic>Other chromatographic methods</topic><topic>Penicillin V - isolation & purification</topic><topic>Pharmaceutical Preparations - isolation & purification</topic><topic>Pharmacology. Drug treatments</topic><topic>Pyrrolidines - isolation & purification</topic><topic>Sensitivity and Specificity</topic><topic>Sulfonamides - isolation & purification</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Visky, Dóra</creatorcontrib><creatorcontrib>Haghedooren, Erik</creatorcontrib><creatorcontrib>Dehouck, Pieter</creatorcontrib><creatorcontrib>Kovács, Zsuzsanna</creatorcontrib><creatorcontrib>Kóczián, Kristof</creatorcontrib><creatorcontrib>Noszál, Béla</creatorcontrib><creatorcontrib>Hoogmartens, Jos</creatorcontrib><creatorcontrib>Adams, Erwin</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Visky, Dóra</au><au>Haghedooren, Erik</au><au>Dehouck, Pieter</au><au>Kovács, Zsuzsanna</au><au>Kóczián, Kristof</au><au>Noszál, Béla</au><au>Hoogmartens, Jos</au><au>Adams, Erwin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Facilitated column selection in pharmaceutical analyses using a simple column classification system</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2006-01-06</date><risdate>2006</risdate><volume>1101</volume><issue>1</issue><spage>103</spage><epage>114</epage><pages>103-114</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>In this paper, the performance of a previously developed classification system applied to pharmaceutical chromatographic analyses, is investigated. The separation of seven different drug substances from their respective impurities was studied. The chromatographic procedure for acetylsalicylic acid, clindamycin hydrochloride, buflomedil hydrochloride, chloramphenicol sodium succinate, nimesulide and phenoxymethylpenicillin was performed according to the corresponding European Pharmacopoeia (Ph. Eur.) monograph. The separation of dihydrostreptomycin sulphate was performed according to the literature. It is shown that the column ranking system is a helpful tool in the selection of a suitable column in these analyses.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>16242136</pmid><doi>10.1016/j.chroma.2005.09.069</doi><tpages>12</tpages></addata></record> |
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subjects | Analysis Analytical chemistry Aspirin - isolation & purification Biological and medical sciences Chemistry Chloramphenicol - analogs & derivatives Chloramphenicol - isolation & purification Chromatographic methods and physical methods associated with chromatography Chromatographic tests Chromatography, Liquid - instrumentation Chromatography, Liquid - methods Clindamycin - isolation & purification Column characterisation Column classification Dihydrostreptomycin Sulfate - isolation & purification Exact sciences and technology General pharmacology Medical sciences Other chromatographic methods Penicillin V - isolation & purification Pharmaceutical Preparations - isolation & purification Pharmacology. Drug treatments Pyrrolidines - isolation & purification Sensitivity and Specificity Sulfonamides - isolation & purification |
title | Facilitated column selection in pharmaceutical analyses using a simple column classification system |
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