Retention-time database of 126 polybrominated diphenyl ether congeners and two Bromkal technical mixtures on seven capillary gas chromatographic columns
The elution order of 126 polybrominated diphenyl ethers (PBDE) was determined for seven different gas chromatographic (GC) stationary phases. The resulting database facilitates selection of the most suitable GC columns for developing a quantitative, congener-specific BDE analysis and the testing of...
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| Veröffentlicht in: | Journal of Chromatography A 2005-02, Vol.1065 (2), p.239-249 |
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| container_end_page | 249 |
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| container_issue | 2 |
| container_start_page | 239 |
| container_title | Journal of Chromatography A |
| container_volume | 1065 |
| creator | Korytár, Peter Covaci, Adrian de Boer, Jacob Gelbin, Anke Brinkman, Udo A.Th |
| description | The elution order of 126 polybrominated diphenyl ethers (PBDE) was determined for seven different gas chromatographic (GC) stationary phases. The resulting database facilitates selection of the most suitable GC columns for developing a quantitative, congener-specific BDE analysis and the testing of retention prediction algorithms based on structure relationships of GC phases and congener substitution patterns. In addition, co-elutions of the principal BDE congeners with other BDEs and/or with other brominated flame retardants were investigated and, as an application, the composition of two Bromkal mixtures (70-5DE and 79-8DE) was studied. |
| doi_str_mv | 10.1016/j.chroma.2004.12.059 |
| format | Article |
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The resulting database facilitates selection of the most suitable GC columns for developing a quantitative, congener-specific BDE analysis and the testing of retention prediction algorithms based on structure relationships of GC phases and congener substitution patterns. 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The resulting database facilitates selection of the most suitable GC columns for developing a quantitative, congener-specific BDE analysis and the testing of retention prediction algorithms based on structure relationships of GC phases and congener substitution patterns. In addition, co-elutions of the principal BDE congeners with other BDEs and/or with other brominated flame retardants were investigated and, as an application, the composition of two Bromkal mixtures (70-5DE and 79-8DE) was studied.</description><subject>Algorithms</subject><subject>Analytical chemistry</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Chromatography, Gas - instrumentation</subject><subject>Chromatography, Gas - methods</subject><subject>Elution order</subject><subject>Ethers - analysis</subject><subject>Exact sciences and technology</subject><subject>Gas chromatographic methods</subject><subject>Gas chromatography</subject><subject>Halogenated Diphenyl Ethers</subject><subject>Hydrocarbons, Brominated - analysis</subject><subject>Phenyl Ethers - analysis</subject><subject>Polybrominated Biphenyls - analysis</subject><subject>Polybrominated Biphenyls - chemistry</subject><subject>Polybrominated diphenyl ethers</subject><subject>Stationary phase</subject><issn>0021-9673</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kcFu1TAQRb0A0VL4A4S8gV2C7SR2vEGCClqkSkgI1pZjT178SOxgO4X3J3wurvKk7ljNLM5c3bkXoVeU1JRQ_u5YmymGRdeMkLamrCadfIIuCWG0klw0F-h5SkdCqCCCPUMXtBM9k4Jcor_fIIPPLvgquwWw1VkPOgEOI6aM4zXMp6FIO68zWGzdOoE_zRjyBBGb4A_gISasvcX5d8AfC_tTzziDmbwzZVvcn7xFSDh4nOAePDZ6dfOs4wkfdMK78xwOUa-TM0Vz3hafXqCno54TvDzPK_Tj86fv17fV3debL9cf7irTSJKrhhEhBAfTMc6GQQjNAVg3NiCGXkjopZBd3wO3QwuyafqCCpAc2pY20trmCr3dddcYfm2QslpcMlD8eQhbUlx0LWF9W8B2B00MKUUY1RrdUr5QlKiHFtRR7b-ohxYUZaq0UM5en_W3YQH7eHSuoABvzoBOJa8xam9ceuR4x1ouaeHe7xyUNO4dRJWMA2_AuggmKxvc_538A-6JrPs</recordid><startdate>20050218</startdate><enddate>20050218</enddate><creator>Korytár, Peter</creator><creator>Covaci, Adrian</creator><creator>de Boer, Jacob</creator><creator>Gelbin, Anke</creator><creator>Brinkman, Udo A.Th</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20050218</creationdate><title>Retention-time database of 126 polybrominated diphenyl ether congeners and two Bromkal technical mixtures on seven capillary gas chromatographic columns</title><author>Korytár, Peter ; Covaci, Adrian ; de Boer, Jacob ; Gelbin, Anke ; Brinkman, Udo A.Th</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c390t-3207776ec5262bb77a6ee25f3e7b879e8979588e6db4e93386ec7e96e44139dd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Algorithms</topic><topic>Analytical chemistry</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Chromatography, Gas - instrumentation</topic><topic>Chromatography, Gas - methods</topic><topic>Elution order</topic><topic>Ethers - analysis</topic><topic>Exact sciences and technology</topic><topic>Gas chromatographic methods</topic><topic>Gas chromatography</topic><topic>Halogenated Diphenyl Ethers</topic><topic>Hydrocarbons, Brominated - analysis</topic><topic>Phenyl Ethers - analysis</topic><topic>Polybrominated Biphenyls - analysis</topic><topic>Polybrominated Biphenyls - chemistry</topic><topic>Polybrominated diphenyl ethers</topic><topic>Stationary phase</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Korytár, Peter</creatorcontrib><creatorcontrib>Covaci, Adrian</creatorcontrib><creatorcontrib>de Boer, Jacob</creatorcontrib><creatorcontrib>Gelbin, Anke</creatorcontrib><creatorcontrib>Brinkman, Udo A.Th</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Korytár, Peter</au><au>Covaci, Adrian</au><au>de Boer, Jacob</au><au>Gelbin, Anke</au><au>Brinkman, Udo A.Th</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Retention-time database of 126 polybrominated diphenyl ether congeners and two Bromkal technical mixtures on seven capillary gas chromatographic columns</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2005-02-18</date><risdate>2005</risdate><volume>1065</volume><issue>2</issue><spage>239</spage><epage>249</epage><pages>239-249</pages><issn>0021-9673</issn><coden>JOCRAM</coden><abstract>The elution order of 126 polybrominated diphenyl ethers (PBDE) was determined for seven different gas chromatographic (GC) stationary phases. The resulting database facilitates selection of the most suitable GC columns for developing a quantitative, congener-specific BDE analysis and the testing of retention prediction algorithms based on structure relationships of GC phases and congener substitution patterns. In addition, co-elutions of the principal BDE congeners with other BDEs and/or with other brominated flame retardants were investigated and, as an application, the composition of two Bromkal mixtures (70-5DE and 79-8DE) was studied.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>15782970</pmid><doi>10.1016/j.chroma.2004.12.059</doi><tpages>11</tpages></addata></record> |
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| ispartof | Journal of Chromatography A, 2005-02, Vol.1065 (2), p.239-249 |
| issn | 0021-9673 |
| language | eng |
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| subjects | Algorithms Analytical chemistry Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Gas - instrumentation Chromatography, Gas - methods Elution order Ethers - analysis Exact sciences and technology Gas chromatographic methods Gas chromatography Halogenated Diphenyl Ethers Hydrocarbons, Brominated - analysis Phenyl Ethers - analysis Polybrominated Biphenyls - analysis Polybrominated Biphenyls - chemistry Polybrominated diphenyl ethers Stationary phase |
| title | Retention-time database of 126 polybrominated diphenyl ether congeners and two Bromkal technical mixtures on seven capillary gas chromatographic columns |
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