LC-MS/MS method for the confirmatory determination of aromatic amines and its application in textile analysis

LC-MS/MS method for the confirmatory determination of aromatic amines and its application in textile analysis

A confirmation method for the determination of 18 aromatic amines originating from azo dyes after reductive cleavage was developed. The method is based on the use of high-performance liquid chromatography/tandem mass spectrometry with atmospheric-pressure chemical ionization. For the identification...

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Veröffentlicht in:Analytical and bioanalytical chemistry 2005-01, Vol.381 (1), p.268-276
Hauptverfasser: Sutthivaiyakit, P, Achatz, S, Lintelmann, J, Aungpradit, T, Chanwirat, R, Chumanee, S, Kettrup, A
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container_issue 1
container_start_page 268
container_title Analytical and bioanalytical chemistry
container_volume 381
creator Sutthivaiyakit, P
Achatz, S
Lintelmann, J
Aungpradit, T
Chanwirat, R
Chumanee, S
Kettrup, A
description A confirmation method for the determination of 18 aromatic amines originating from azo dyes after reductive cleavage was developed. The method is based on the use of high-performance liquid chromatography/tandem mass spectrometry with atmospheric-pressure chemical ionization. For the identification of the analytes one precursor ion and two daughter ions (multi-reaction monitoring, MRM) were selected and the LC-MS/MS parameters optimized to obtain high sensitivity and selectivity. The linear ranges varied from 0.1-1 to 30-50 microg mL(-1) with correlation coefficients of 0.99 or better. The applicability of the method to determine o-tolidine (3,3'-dimethylbenzidine) and 3,3'-dimethoxybenzidine in textiles following reductive cleavage of acid red 114, trypan blue, and Chicago sky blue 6B was demonstrated.
doi_str_mv 10.1007/s00216-004-2852-2
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title LC-MS/MS method for the confirmatory determination of aromatic amines and its application in textile analysis
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