IR, MS studies on (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt
The vibration spectrum and FAB mass spectrum of (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt was studied. By comparing with the spectra of free base, different bands of IR were found in the NH + stretching, the NH + defomatio...
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| Veröffentlicht in: | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy Molecular and biomolecular spectroscopy, 2005-02, Vol.61 (4), p.717-720 |
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| container_title | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy |
| container_volume | 61 |
| creator | Qin, Bingjie Lin, Jimao Lin, Zhenguang Ren, Huixue Xue, Yun |
| description | The vibration spectrum and FAB mass spectrum of (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt was studied. By comparing with the spectra of free base, different bands of IR were found in the NH
+ stretching, the NH
+ defomation motion, the CH
2 of N
CH
2 group symmetric stretching, the CH
2 of N
CH
2 group twisting and the CN stretching. FAB shows the basic peak is
M + H. Other
m/
e peaks are consistent with the structrue. |
| doi_str_mv | 10.1016/j.saa.2004.04.030 |
| format | Article |
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+ stretching, the NH
+ defomation motion, the CH
2 of N
CH
2 group symmetric stretching, the CH
2 of N
CH
2 group twisting and the CN stretching. FAB shows the basic peak is
M + H. Other
m/
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+ stretching, the NH
+ defomation motion, the CH
2 of N
CH
2 group symmetric stretching, the CH
2 of N
CH
2 group twisting and the CN stretching. FAB shows the basic peak is
M + H. Other
m/
e peaks are consistent with the structrue.</description><subject>(±)-1-[3-(2-Methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt</subject><subject>Carbon - chemistry</subject><subject>FAB</subject><subject>Free base</subject><subject>Hydrogen Bonding</subject><subject>Mass Spectrometry - methods</subject><subject>Models, Chemical</subject><subject>Nitrogen - chemistry</subject><subject>Piperazines - chemistry</subject><subject>Spectrophotometry, Infrared - methods</subject><subject>Vibration spectrum</subject><issn>1386-1425</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp9kNtq3DAQhnXRkGMfoDfFV2UXoq1kHSKTq7C0TSAh0MNVCEKWxqwW23Ikb6n7CHmbvEKeLHZ2IXeBgUGjb36YD6FPlCwoofLrepGMWeSE8MVUjHxAh5QpiSnPxQE6SmlNCKEqJ_vogArJC0XEIXq8-nma3fzKUr9xHlIW2mz2_DTHFN8xPMtxA_0q_Bu6FbRjm-McrwYXp0kM3VDfY47vZvmpxM5P6FBP5FDPTePbYE0sw_ja_tx3voNo_vsWMudfY-yqDtE7yJKp-xO0V5k6wcddP0Z_vn_7vbzE17c_rpYX19gyQXucF0xZ7qxkriipLBmVQlWMMU4UL0tTKQK2cMQwY1UhKs7ObFlZJ6iF0Y5gx-jLNnc84WEDqdeNTxbq2rQQNknLMya5EhNIt6CNIaUIle6ib0wcNCV6kq7XepSuJ-l6KkbGnc-78E3ZgHvb2BkfgfMtAOOJfz1EnayH1oLzEWyvXfDvxL8A_mmWVA</recordid><startdate>20050201</startdate><enddate>20050201</enddate><creator>Qin, Bingjie</creator><creator>Lin, Jimao</creator><creator>Lin, Zhenguang</creator><creator>Ren, Huixue</creator><creator>Xue, Yun</creator><general>Elsevier B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20050201</creationdate><title>IR, MS studies on (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt</title><author>Qin, Bingjie ; Lin, Jimao ; Lin, Zhenguang ; Ren, Huixue ; Xue, Yun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c351t-2938c4dc63d9b16b31658f3334084bbaf80ec9d0a3ac895f437cbfcd51ce00453</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>(±)-1-[3-(2-Methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt</topic><topic>Carbon - chemistry</topic><topic>FAB</topic><topic>Free base</topic><topic>Hydrogen Bonding</topic><topic>Mass Spectrometry - methods</topic><topic>Models, Chemical</topic><topic>Nitrogen - chemistry</topic><topic>Piperazines - chemistry</topic><topic>Spectrophotometry, Infrared - methods</topic><topic>Vibration spectrum</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Qin, Bingjie</creatorcontrib><creatorcontrib>Lin, Jimao</creatorcontrib><creatorcontrib>Lin, Zhenguang</creatorcontrib><creatorcontrib>Ren, Huixue</creatorcontrib><creatorcontrib>Xue, Yun</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Qin, Bingjie</au><au>Lin, Jimao</au><au>Lin, Zhenguang</au><au>Ren, Huixue</au><au>Xue, Yun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>IR, MS studies on (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt</atitle><jtitle>Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy</jtitle><addtitle>Spectrochim Acta A Mol Biomol Spectrosc</addtitle><date>2005-02-01</date><risdate>2005</risdate><volume>61</volume><issue>4</issue><spage>717</spage><epage>720</epage><pages>717-720</pages><issn>1386-1425</issn><abstract>The vibration spectrum and FAB mass spectrum of (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt was studied. By comparing with the spectra of free base, different bands of IR were found in the NH
+ stretching, the NH
+ defomation motion, the CH
2 of N
CH
2 group symmetric stretching, the CH
2 of N
CH
2 group twisting and the CN stretching. FAB shows the basic peak is
M + H. Other
m/
e peaks are consistent with the structrue.</abstract><cop>England</cop><pub>Elsevier B.V</pub><pmid>15649805</pmid><doi>10.1016/j.saa.2004.04.030</doi><tpages>4</tpages></addata></record> |
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| identifier | ISSN: 1386-1425 |
| ispartof | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 2005-02, Vol.61 (4), p.717-720 |
| issn | 1386-1425 |
| language | eng |
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| source | MEDLINE; Elsevier ScienceDirect Journals Complete |
| subjects | (±)-1-[3-(2-Methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt Carbon - chemistry FAB Free base Hydrogen Bonding Mass Spectrometry - methods Models, Chemical Nitrogen - chemistry Piperazines - chemistry Spectrophotometry, Infrared - methods Vibration spectrum |
| title | IR, MS studies on (±)-1-[3-(2-methoxyphenoxy)-2-hydroxypropyl]-4-[(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine dihydrochloride salt |
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