Advanced detection systems for X-ray fluorescence excitation spectroscopy

This paper accounts for selected detector developments carried out over the past 15 years within the ESRF X‐ray Absorption Spectroscopy group. This includes various types of photodiodes used as integrated current detectors. Special emphasis is put on the long‐standing development of a Si drift‐diode...

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Veröffentlicht in:Journal of synchrotron radiation 2005-01, Vol.12 (1), p.57-69
Hauptverfasser: Goulon, J., Rogalev, A., Goujon, G., Gauthier, Ch, Moguiline, E., Solé, A., Feite, S., Wilhelm, F., Jaouen, N., Goulon-Ginet, Ch, Dressler, P., Rohr, P., Lampert, M.-O., Henck, R.
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container_end_page 69
container_issue 1
container_start_page 57
container_title Journal of synchrotron radiation
container_volume 12
creator Goulon, J.
Rogalev, A.
Goujon, G.
Gauthier, Ch
Moguiline, E.
Solé, A.
Feite, S.
Wilhelm, F.
Jaouen, N.
Goulon-Ginet, Ch
Dressler, P.
Rohr, P.
Lampert, M.-O.
Henck, R.
description This paper accounts for selected detector developments carried out over the past 15 years within the ESRF X‐ray Absorption Spectroscopy group. This includes various types of photodiodes used as integrated current detectors. Special emphasis is put on the long‐standing development of a Si drift‐diode array suitable for energy‐dispersive detection of X‐ray fluorescence. This detector, which is now operational, was used to record high‐quality XMCD/XAFS spectra on [Fe70Pt30] nanoparticles highly dispersed on a Si wafer. Using numerically deconvoluted spectra, energy resolution was decreased to 82 eV for the Si Kαβ line, 126 eV for the Fe Kα line and 176 eV for the Pt Lα line. A high‐vacuum‐compatible high‐energy‐resolution crystal analyzer was also installed on ID12, making it possible to record X‐ray fluorescence excitation spectra in the photon‐in/photon‐out mode over a wide spectral range. Prospects of adapting these methods in order to investigate biological samples are briefly discussed.
doi_str_mv 10.1107/S090904950402878X
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Synchrotron Rad</addtitle><description>This paper accounts for selected detector developments carried out over the past 15 years within the ESRF X‐ray Absorption Spectroscopy group. This includes various types of photodiodes used as integrated current detectors. Special emphasis is put on the long‐standing development of a Si drift‐diode array suitable for energy‐dispersive detection of X‐ray fluorescence. This detector, which is now operational, was used to record high‐quality XMCD/XAFS spectra on [Fe70Pt30] nanoparticles highly dispersed on a Si wafer. Using numerically deconvoluted spectra, energy resolution was decreased to 82 eV for the Si Kαβ line, 126 eV for the Fe Kα line and 176 eV for the Pt Lα line. A high‐vacuum‐compatible high‐energy‐resolution crystal analyzer was also installed on ID12, making it possible to record X‐ray fluorescence excitation spectra in the photon‐in/photon‐out mode over a wide spectral range. 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issn 1600-5775
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source Wiley Online Library Open Access
subjects Applied sciences
digital filtering
Electronics
Equipment Design
Exact sciences and technology
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Optoelectronic devices
Photons
Physics
Semiconductor electronics. Microelectronics. Optoelectronics. Solid state devices
silicon drift-diodes
Spectrometry, Fluorescence - instrumentation
Spectrum Analysis - instrumentation
Synchrotron radiation instrumentation
X- and γ-ray instruments and techniques
X-ray absorption spectroscopy
X-ray detectors
X-Rays
title Advanced detection systems for X-ray fluorescence excitation spectroscopy
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