Residual diesel measurement in sand columns after surfactant/alcohol washing
A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N2 technique is based on drying of sand columns by circulating helium gas to drag oil dropl...
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| Veröffentlicht in: | Ground Water 1996-01, Vol.34 (1), p.162-167 |
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| creator | Martel, R. (Laval University, Quebec, Qc., Canada.) Gelinas, P.J |
| description | A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N2 technique is based on drying of sand columns by circulating helium gas to drag oil droplets in a cold trap (liquid nitrogen). With this technique, residual diesel measurement can be performed easily immediately after alcohol/surfactant washing and in the same lab. For high residual diesel content in Ottawa sand (25 to 30 g/kg, the technique is much more accurate (+/- 2% or 600 mg/kg) than the standard analytical methods for the determination of mineral oil and grease. The average relative error on partial diesel dissolution in sand column estimated after alcohol/surfactant flooding (residual saturation of 10 to 15 g/kg) is as low as 5%. The precision of the He/N2 technique is adequate to compare relative efficiency of washing solutions when partial extraction of residual oil in Ottawa sand columns is performed. However, this technique is not adapted for determination of traces of oil in sediment or for environmental control of contaminated soils. Each diesel determination by the He/N2 technique costs less than 8 $US in chemical products (helium and liquid nitrogen). A simple laboratory drying setup can be built for less than 400 $US which makes this technique valuable for diesel analyses when a large number of tests are required |
| doi_str_mv | 10.1111/j.1745-6584.1996.tb01876.x |
| format | Article |
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(Laval University, Quebec, Qc., Canada.) ; Gelinas, P.J</creator><creatorcontrib>Martel, R. (Laval University, Quebec, Qc., Canada.) ; Gelinas, P.J</creatorcontrib><description>A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N2 technique is based on drying of sand columns by circulating helium gas to drag oil droplets in a cold trap (liquid nitrogen). With this technique, residual diesel measurement can be performed easily immediately after alcohol/surfactant washing and in the same lab. For high residual diesel content in Ottawa sand (25 to 30 g/kg, the technique is much more accurate (+/- 2% or 600 mg/kg) than the standard analytical methods for the determination of mineral oil and grease. The average relative error on partial diesel dissolution in sand column estimated after alcohol/surfactant flooding (residual saturation of 10 to 15 g/kg) is as low as 5%. The precision of the He/N2 technique is adequate to compare relative efficiency of washing solutions when partial extraction of residual oil in Ottawa sand columns is performed. However, this technique is not adapted for determination of traces of oil in sediment or for environmental control of contaminated soils. Each diesel determination by the He/N2 technique costs less than 8 $US in chemical products (helium and liquid nitrogen). A simple laboratory drying setup can be built for less than 400 $US which makes this technique valuable for diesel analyses when a large number of tests are required</description><identifier>ISSN: 0017-467X</identifier><identifier>EISSN: 1745-6584</identifier><identifier>DOI: 10.1111/j.1745-6584.1996.tb01876.x</identifier><identifier>CODEN: GRWAAP</identifier><language>eng</language><publisher>Oxford, UK: Blackwell Publishing Ltd</publisher><subject>02 PETROLEUM ; ACCURACY ; ACEITE DIESEL ; AGUAS SUBTERRANEAS ; ALCOHOLES ; ALCOHOLS ; ALCOOL ; Analysis ; AQUIFERS ; ARENA ; AZOTE ; BENCH-SCALE EXPERIMENTS ; CAPA FREATICA ; CARBURANT DIESEL ; DIESEL FUELS ; EAU SOUTERRAINE ; GRAVIMETRIA ; GRAVIMETRIC ANALYSIS ; GRAVIMETRIE ; Groundwater ; HYDROCARBONS ; Measurement ; MEDICION ; MESURE ; METALLOIDE ; NAPPE SOUTERRAINE ; NITROGENO ; NO METALES ; Oil pollution ; OIL SATURATION ; OIL SPILLS ; Pollutants ; Pollution ; POLLUTION DE L'EAU ; POLUCION DEL AGUA ; REMEDIAL ACTION ; REMOVAL ; RESIDU ; RESIDUES ; RESIDUOS ; SABLE ; Sand ; SIMULACION ; SIMULATION ; Surface active agents ; SURFACTANT ; SURFACTANTES ; SURFACTANTS ; TECHNIQUE ANALYTIQUE ; TECNICAS ANALITICAS ; Tests</subject><ispartof>Ground Water, 1996-01, Vol.34 (1), p.162-167</ispartof><rights>COPYRIGHT 1996 National Ground Water Association</rights><rights>Copyright Ground Water Publishing Company Jan 1996</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a5502-75befb02ebbae1c0515482e1cedb8adaf2d5d57e806c9f0c4816dc399ad9a2dd3</citedby><cites>FETCH-LOGICAL-a5502-75befb02ebbae1c0515482e1cedb8adaf2d5d57e806c9f0c4816dc399ad9a2dd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fj.1745-6584.1996.tb01876.x$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fj.1745-6584.1996.tb01876.x$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,885,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/194771$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Martel, R. (Laval University, Quebec, Qc., Canada.)</creatorcontrib><creatorcontrib>Gelinas, P.J</creatorcontrib><title>Residual diesel measurement in sand columns after surfactant/alcohol washing</title><title>Ground Water</title><description>A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N2 technique is based on drying of sand columns by circulating helium gas to drag oil droplets in a cold trap (liquid nitrogen). With this technique, residual diesel measurement can be performed easily immediately after alcohol/surfactant washing and in the same lab. For high residual diesel content in Ottawa sand (25 to 30 g/kg, the technique is much more accurate (+/- 2% or 600 mg/kg) than the standard analytical methods for the determination of mineral oil and grease. The average relative error on partial diesel dissolution in sand column estimated after alcohol/surfactant flooding (residual saturation of 10 to 15 g/kg) is as low as 5%. The precision of the He/N2 technique is adequate to compare relative efficiency of washing solutions when partial extraction of residual oil in Ottawa sand columns is performed. However, this technique is not adapted for determination of traces of oil in sediment or for environmental control of contaminated soils. Each diesel determination by the He/N2 technique costs less than 8 $US in chemical products (helium and liquid nitrogen). A simple laboratory drying setup can be built for less than 400 $US which makes this technique valuable for diesel analyses when a large number of tests are required</description><subject>02 PETROLEUM</subject><subject>ACCURACY</subject><subject>ACEITE DIESEL</subject><subject>AGUAS SUBTERRANEAS</subject><subject>ALCOHOLES</subject><subject>ALCOHOLS</subject><subject>ALCOOL</subject><subject>Analysis</subject><subject>AQUIFERS</subject><subject>ARENA</subject><subject>AZOTE</subject><subject>BENCH-SCALE EXPERIMENTS</subject><subject>CAPA FREATICA</subject><subject>CARBURANT DIESEL</subject><subject>DIESEL FUELS</subject><subject>EAU SOUTERRAINE</subject><subject>GRAVIMETRIA</subject><subject>GRAVIMETRIC ANALYSIS</subject><subject>GRAVIMETRIE</subject><subject>Groundwater</subject><subject>HYDROCARBONS</subject><subject>Measurement</subject><subject>MEDICION</subject><subject>MESURE</subject><subject>METALLOIDE</subject><subject>NAPPE SOUTERRAINE</subject><subject>NITROGENO</subject><subject>NO METALES</subject><subject>Oil pollution</subject><subject>OIL SATURATION</subject><subject>OIL SPILLS</subject><subject>Pollutants</subject><subject>Pollution</subject><subject>POLLUTION DE L'EAU</subject><subject>POLUCION DEL AGUA</subject><subject>REMEDIAL ACTION</subject><subject>REMOVAL</subject><subject>RESIDU</subject><subject>RESIDUES</subject><subject>RESIDUOS</subject><subject>SABLE</subject><subject>Sand</subject><subject>SIMULACION</subject><subject>SIMULATION</subject><subject>Surface active agents</subject><subject>SURFACTANT</subject><subject>SURFACTANTES</subject><subject>SURFACTANTS</subject><subject>TECHNIQUE ANALYTIQUE</subject><subject>TECNICAS ANALITICAS</subject><subject>Tests</subject><issn>0017-467X</issn><issn>1745-6584</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1996</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNqVkkFv1DAQhSMEEkvhD3AKPXAiWzuJ7ZgLWipYkFYg0ZYiLtbEnux6SexiJ-r235MoVZFQpQr7YGvme88j6yXJMSVLOq6T_ZKKkmWcVeWSSsmXfU1oJfjy8ChZ3LUeJwtCqMhKLn48TZ7FuCeEFJLIRbL5htGaAdrUWIzYph1CHAJ26PrUujSCM6n27dC5mELTY0jHdgO6B9efQKv9zrfpNcSdddvnyZMG2ogvbs-j5OLjh_PTT9nm6_rz6WqTAWMkzwSrsalJjnUNSDVhlJVVPt7Q1BUYaHLDDBNYEa5lQ3RZUW50ISUYCbkxxVHyavb1sbcqatuj3mnvHOpeUVkKQUfm9cxcBf97wNirzkaNbQsO_RBVwamshGQPgjmlQuSSPAhSPhnS6enjf8C9H4Ibf0TlBZeEcjG5vZmhLbSorGt8H0Bv0WGA1jts7Fhe0YpILoUc8ewefNwGO6vv49_OvA4-xoCNugq2g3CjKFFTdNReTflQUz7UFB11Gx11GMXvZvH1aHrzH0q1vlydU57_HdfGHg93DhB-KS4KwdTll7XavF8XhJ_9VN9H_uXMN-AVbION6uJMCsp5yYs_ExDjUg</recordid><startdate>199601</startdate><enddate>199601</enddate><creator>Martel, R. 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(Laval University, Quebec, Qc., Canada.)</au><au>Gelinas, P.J</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Residual diesel measurement in sand columns after surfactant/alcohol washing</atitle><jtitle>Ground Water</jtitle><date>1996-01</date><risdate>1996</risdate><volume>34</volume><issue>1</issue><spage>162</spage><epage>167</epage><pages>162-167</pages><issn>0017-467X</issn><eissn>1745-6584</eissn><coden>GRWAAP</coden><abstract>A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N2 technique is based on drying of sand columns by circulating helium gas to drag oil droplets in a cold trap (liquid nitrogen). With this technique, residual diesel measurement can be performed easily immediately after alcohol/surfactant washing and in the same lab. For high residual diesel content in Ottawa sand (25 to 30 g/kg, the technique is much more accurate (+/- 2% or 600 mg/kg) than the standard analytical methods for the determination of mineral oil and grease. The average relative error on partial diesel dissolution in sand column estimated after alcohol/surfactant flooding (residual saturation of 10 to 15 g/kg) is as low as 5%. The precision of the He/N2 technique is adequate to compare relative efficiency of washing solutions when partial extraction of residual oil in Ottawa sand columns is performed. However, this technique is not adapted for determination of traces of oil in sediment or for environmental control of contaminated soils. Each diesel determination by the He/N2 technique costs less than 8 $US in chemical products (helium and liquid nitrogen). A simple laboratory drying setup can be built for less than 400 $US which makes this technique valuable for diesel analyses when a large number of tests are required</abstract><cop>Oxford, UK</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1111/j.1745-6584.1996.tb01876.x</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
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| ispartof | Ground Water, 1996-01, Vol.34 (1), p.162-167 |
| issn | 0017-467X 1745-6584 |
| language | eng |
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| source | Wiley Journals |
| subjects | 02 PETROLEUM ACCURACY ACEITE DIESEL AGUAS SUBTERRANEAS ALCOHOLES ALCOHOLS ALCOOL Analysis AQUIFERS ARENA AZOTE BENCH-SCALE EXPERIMENTS CAPA FREATICA CARBURANT DIESEL DIESEL FUELS EAU SOUTERRAINE GRAVIMETRIA GRAVIMETRIC ANALYSIS GRAVIMETRIE Groundwater HYDROCARBONS Measurement MEDICION MESURE METALLOIDE NAPPE SOUTERRAINE NITROGENO NO METALES Oil pollution OIL SATURATION OIL SPILLS Pollutants Pollution POLLUTION DE L'EAU POLUCION DEL AGUA REMEDIAL ACTION REMOVAL RESIDU RESIDUES RESIDUOS SABLE Sand SIMULACION SIMULATION Surface active agents SURFACTANT SURFACTANTES SURFACTANTS TECHNIQUE ANALYTIQUE TECNICAS ANALITICAS Tests |
| title | Residual diesel measurement in sand columns after surfactant/alcohol washing |
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