Investigation of magnetron sputtered titanium–nickel–nitride thin films for use as mould coatings
Titanium–nickel–nitride coatings (Ti–Ni–N) were prepared by unbalanced magnetron sputtering with a pulsed DC discharge at the targets. The amount of nickel in the coatings ranged from 8 to 32 at.% and the nitrogen-to-titanium ratio was less than 1. Polished samples of steel (X42Cr13) were used as su...
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| Veröffentlicht in: | Surface & coatings technology 2008-12, Vol.203 (5), p.717-720 |
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| creator | Stock, H.-R. Diesselberg, M. Zoch, H.-W. |
| description | Titanium–nickel–nitride coatings (Ti–Ni–N) were prepared by unbalanced magnetron sputtering with a pulsed DC discharge at the targets. The amount of nickel in the coatings ranged from 8 to 32 at.% and the nitrogen-to-titanium ratio was less than 1. Polished samples of steel (X42Cr13) were used as substrates, both shims and moulding inserts. Plastic universal hardness was between 7 and 21 GPa. Cross-section SEM images reveal a slightly columnar structure with a very smooth surface.
The inserts were used in moulding experiments with polymethylmethacrylate (PMMA). They revealed a remarkable performance. No delamination of the coating was observed. The only wear detectable was some abrasion occurring at the dome-shaped top of the columns of the coating. This results in a decrease of the average roughness Ra and even better surface smoothness of the moulded PMMA parts. |
| doi_str_mv | 10.1016/j.surfcoat.2008.08.037 |
| format | Article |
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The inserts were used in moulding experiments with polymethylmethacrylate (PMMA). They revealed a remarkable performance. No delamination of the coating was observed. The only wear detectable was some abrasion occurring at the dome-shaped top of the columns of the coating. This results in a decrease of the average roughness Ra and even better surface smoothness of the moulded PMMA parts.</description><identifier>ISSN: 0257-8972</identifier><identifier>EISSN: 1879-3347</identifier><identifier>DOI: 10.1016/j.surfcoat.2008.08.037</identifier><identifier>CODEN: SCTEEJ</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Applied sciences ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Injection moulding ; Magnetron sputtering ; Materials science ; Metals. Metallurgy ; Methods of deposition of films and coatings; film growth and epitaxy ; Nonmetallic coatings ; Physics ; Production techniques ; Surface treatment ; Surface treatments ; Titanium–nickel–nitride coatings</subject><ispartof>Surface & coatings technology, 2008-12, Vol.203 (5), p.717-720</ispartof><rights>2008 Elsevier B.V.</rights><rights>2009 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c373t-851dac871a9cc9c32b1b8453428ef1687b3700ebdcc496cdd2afed3ed1aca3f93</citedby><cites>FETCH-LOGICAL-c373t-851dac871a9cc9c32b1b8453428ef1687b3700ebdcc496cdd2afed3ed1aca3f93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.surfcoat.2008.08.037$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>309,310,314,780,784,789,790,3550,23930,23931,25140,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=21206248$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Stock, H.-R.</creatorcontrib><creatorcontrib>Diesselberg, M.</creatorcontrib><creatorcontrib>Zoch, H.-W.</creatorcontrib><title>Investigation of magnetron sputtered titanium–nickel–nitride thin films for use as mould coatings</title><title>Surface & coatings technology</title><description>Titanium–nickel–nitride coatings (Ti–Ni–N) were prepared by unbalanced magnetron sputtering with a pulsed DC discharge at the targets. The amount of nickel in the coatings ranged from 8 to 32 at.% and the nitrogen-to-titanium ratio was less than 1. Polished samples of steel (X42Cr13) were used as substrates, both shims and moulding inserts. Plastic universal hardness was between 7 and 21 GPa. Cross-section SEM images reveal a slightly columnar structure with a very smooth surface.
The inserts were used in moulding experiments with polymethylmethacrylate (PMMA). They revealed a remarkable performance. No delamination of the coating was observed. The only wear detectable was some abrasion occurring at the dome-shaped top of the columns of the coating. This results in a decrease of the average roughness Ra and even better surface smoothness of the moulded PMMA parts.</description><subject>Applied sciences</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Injection moulding</subject><subject>Magnetron sputtering</subject><subject>Materials science</subject><subject>Metals. Metallurgy</subject><subject>Methods of deposition of films and coatings; film growth and epitaxy</subject><subject>Nonmetallic coatings</subject><subject>Physics</subject><subject>Production techniques</subject><subject>Surface treatment</subject><subject>Surface treatments</subject><subject>Titanium–nickel–nitride coatings</subject><issn>0257-8972</issn><issn>1879-3347</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNqFUM2KFDEQDqLgOPoKkoveesxPTye5KYs_Cwte9BwylcqYsTsZk_SCN9_BN_RJ7HZ2vS4UVBV8Vd8PIS8523HGhzenXZ1LgOzaTjCmd2tJ9YhsuFamk7JXj8mGib3qtFHiKXlW64kxxpXpNwSv0y3WFo-uxZxoDnRyx4StLEs9z61hQU9bbC7Fefrz63eK8B3Hf0Mr0SNt32KiIY5TpSEXOlekrtIpz6Onq6iYjvU5eRLcWPHFXd-Srx_ef7n61N18_nh99e6mA6lk6_SeewdacWcADEhx4Afd72UvNAY-aHWQijE8eIDeDOC9cAG9RM8dOBmM3JLXl7_nkn_Miy87xQo4ji5hnquVe2OEMStwuACh5FoLBnsucXLlp-XMrqnak71P1a6p2rUWkVvy6o7BVXBjKC5BrP-vBRdsEL1ecG8vOFzs3kYstkLEBOhjQWjW5_gQ1V_lW5bY</recordid><startdate>20081225</startdate><enddate>20081225</enddate><creator>Stock, H.-R.</creator><creator>Diesselberg, M.</creator><creator>Zoch, H.-W.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20081225</creationdate><title>Investigation of magnetron sputtered titanium–nickel–nitride thin films for use as mould coatings</title><author>Stock, H.-R. ; Diesselberg, M. ; Zoch, H.-W.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c373t-851dac871a9cc9c32b1b8453428ef1687b3700ebdcc496cdd2afed3ed1aca3f93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Applied sciences</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Injection moulding</topic><topic>Magnetron sputtering</topic><topic>Materials science</topic><topic>Metals. Metallurgy</topic><topic>Methods of deposition of films and coatings; film growth and epitaxy</topic><topic>Nonmetallic coatings</topic><topic>Physics</topic><topic>Production techniques</topic><topic>Surface treatment</topic><topic>Surface treatments</topic><topic>Titanium–nickel–nitride coatings</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Stock, H.-R.</creatorcontrib><creatorcontrib>Diesselberg, M.</creatorcontrib><creatorcontrib>Zoch, H.-W.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Surface & coatings technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Stock, H.-R.</au><au>Diesselberg, M.</au><au>Zoch, H.-W.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigation of magnetron sputtered titanium–nickel–nitride thin films for use as mould coatings</atitle><jtitle>Surface & coatings technology</jtitle><date>2008-12-25</date><risdate>2008</risdate><volume>203</volume><issue>5</issue><spage>717</spage><epage>720</epage><pages>717-720</pages><issn>0257-8972</issn><eissn>1879-3347</eissn><coden>SCTEEJ</coden><abstract>Titanium–nickel–nitride coatings (Ti–Ni–N) were prepared by unbalanced magnetron sputtering with a pulsed DC discharge at the targets. The amount of nickel in the coatings ranged from 8 to 32 at.% and the nitrogen-to-titanium ratio was less than 1. Polished samples of steel (X42Cr13) were used as substrates, both shims and moulding inserts. Plastic universal hardness was between 7 and 21 GPa. Cross-section SEM images reveal a slightly columnar structure with a very smooth surface.
The inserts were used in moulding experiments with polymethylmethacrylate (PMMA). They revealed a remarkable performance. No delamination of the coating was observed. The only wear detectable was some abrasion occurring at the dome-shaped top of the columns of the coating. This results in a decrease of the average roughness Ra and even better surface smoothness of the moulded PMMA parts.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.surfcoat.2008.08.037</doi><tpages>4</tpages></addata></record> |
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| identifier | ISSN: 0257-8972 |
| ispartof | Surface & coatings technology, 2008-12, Vol.203 (5), p.717-720 |
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| language | eng |
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| source | Access via ScienceDirect (Elsevier) |
| subjects | Applied sciences Cross-disciplinary physics: materials science rheology Exact sciences and technology Injection moulding Magnetron sputtering Materials science Metals. Metallurgy Methods of deposition of films and coatings film growth and epitaxy Nonmetallic coatings Physics Production techniques Surface treatment Surface treatments Titanium–nickel–nitride coatings |
| title | Investigation of magnetron sputtered titanium–nickel–nitride thin films for use as mould coatings |
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