ADHESION OF THE BIOACTIVE LAYER ON TITANIUM ALLOY SUBSTRATE BY TAPE-TEST

ADHESION OF THE BIOACTIVE LAYER ON TITANIUM ALLOY SUBSTRATE BY TAPE-TEST

An attempt was made to assess whether the ASTM D 3359 test is a suitable method for adhesion measurement of layers formed on Ti6Al4V surfaces by: alkali treatment in 10 mol/l NaOH; precalcification in SCS (supersaturated calcification solution); and in-vitro tests in SBF (simulated body fluid). The...

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Veröffentlicht in:Ceramics (Praha) 2008-01, Vol.52 (3), p.130-138
Hauptverfasser: Horkavcova, D, Plesingerova, B, Helebrant, A, Vojtko, M, Prochazka, V
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container_end_page 138
container_issue 3
container_start_page 130
container_title Ceramics (Praha)
container_volume 52
creator Horkavcova, D
Plesingerova, B
Helebrant, A
Vojtko, M
Prochazka, V
description An attempt was made to assess whether the ASTM D 3359 test is a suitable method for adhesion measurement of layers formed on Ti6Al4V surfaces by: alkali treatment in 10 mol/l NaOH; precalcification in SCS (supersaturated calcification solution); and in-vitro tests in SBF (simulated body fluid). The tape-test is suitable for the evaluation of adhesion of coatings after chemical treatment and after short-time precalcification. Adhesion of the coatings was excellent, classified as category 5. The test is not suitable for coatings precalcified for a long time when large spherical crystals are formed. The cracking of the coatings during drying prevented reliable results of adhesion of HA-coatings to substrate after in-vitro tests to be obtained. 12 refs.
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