Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic: Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic

Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic: Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic

Neodymium-doped yttrium aluminum garnet (Nd:YAG) precursor powders were fabricated by co-precipitation method, using Al(NO3)3.9E120, Y(NO3)3.6H20, (NH4)2SO4 and Nd(NO3)3 as raw materials, NH4HCO3 as precipitator, TEOS as sintering additive. After calcining the Nd:YAG precursor at 1200 deg C for 5h,...

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Veröffentlicht in:Wu ji cai liao xue bao 2008-09, Vol.23 (5), p.1037-1040
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description Neodymium-doped yttrium aluminum garnet (Nd:YAG) precursor powders were fabricated by co-precipitation method, using Al(NO3)3.9E120, Y(NO3)3.6H20, (NH4)2SO4 and Nd(NO3)3 as raw materials, NH4HCO3 as precipitator, TEOS as sintering additive. After calcining the Nd:YAG precursor at 1200 deg C for 5h, the well dispersive, spherical pure cubic YAG nano-powders with average particle size of about 100nm were obtained. Subsequently, calcined powders were molded by cold isostatic presses. Transparent ceramics of excellent transmission were obtained by sintering Nd:YAG green body at 1700-1800 deg C for 10h in vacuum. The ceramic crystal grains with average size of about 15,am appear uniformity. There is no impurity and core in grain interface and inner-grain. No scattering center can be detected. The transmission of the sample with thickness of 1.5mm is 83.5% at the near infrared wavelength of 1064nm, which is very close to the theoretical value of Nd:YAG single crystal.
doi_str_mv 10.3724/SP.J.1077.2008.001037
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After calcining the Nd:YAG precursor at 1200 deg C for 5h, the well dispersive, spherical pure cubic YAG nano-powders with average particle size of about 100nm were obtained. Subsequently, calcined powders were molded by cold isostatic presses. Transparent ceramics of excellent transmission were obtained by sintering Nd:YAG green body at 1700-1800 deg C for 10h in vacuum. The ceramic crystal grains with average size of about 15,am appear uniformity. There is no impurity and core in grain interface and inner-grain. No scattering center can be detected. 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title Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic: Preparation and Characteristic of Properties of High Transmission Nd:YAG Transparent Ceramic
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