Preparation and properties of poly(etber ketone)s derived from 2,6-naphthalenedicarboxylic acid chloride

Preparation and properties of poly(etber ketone)s derived from 2,6-naphthalenedicarboxylic acid chloride

Poly(ether ketone)s derived from diphenyl ether and mixed diacid chlorides containing 2,6-naphthalenedicarboxyliUc acid chloride (NDC) with terephthaloyl chloride (TPC) or isophthaloyl chloride (IPC) were prepared by Friedel-Crafts acylation in 1,2-dichloroethane with aluminium trichloride as a cata...

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Veröffentlicht in:High performance polymers 1995-06, Vol.7 (3), p.267-274
Hauptverfasser: Tokai, Masaya, Sakaguchi, Yoshimitsu, Kato, Yasuo
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container_issue 3
container_start_page 267
container_title High performance polymers
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creator Tokai, Masaya
Sakaguchi, Yoshimitsu
Kato, Yasuo
description Poly(ether ketone)s derived from diphenyl ether and mixed diacid chlorides containing 2,6-naphthalenedicarboxyliUc acid chloride (NDC) with terephthaloyl chloride (TPC) or isophthaloyl chloride (IPC) were prepared by Friedel-Crafts acylation in 1,2-dichloroethane with aluminium trichloride as a catalyst. Their thermal properties were widely controlled by changing the composition of diacid chlorides; the glass transision temperature was in the range of 156-203 °C and the melting temperature was 235-390 °C. The order of the structural effect of acid chlorides in increasing the glass transition temperature was NDC > TPC> IPC, and that in decreasing the gas permeability was IPC — NDC > TPC.
doi_str_mv 10.1088/0954-0083/7/3/003
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title Preparation and properties of poly(etber ketone)s derived from 2,6-naphthalenedicarboxylic acid chloride
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