Intercalation of n-C(1(2H(2(5NH(2) into layered titanate with the aid of microwave radiation

Intercalation of n-C(1(2H(2(5NH(2) into layered titanate with the aid of microwave radiation

Synthesis of layered tetratitanate-n-C(1(2H(2(5NH(2) intercalation compounds under microwave radiation was reported in this paper. Under microwave radiation, conversion of K(2)Ti(4)O(9) to H(2)Ti(4)O(9) in 1 M HCl solution needs only 1 h with 0.88 nm of interlayer distance, and the intercalation of...

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Veröffentlicht in:Materials letters 2009-09, Vol.63 (23), p.1992-1994
Hauptverfasser: Tang, Y, Nian, J, Yu, B., Yang, W
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container_end_page 1994
container_issue 23
container_start_page 1992
container_title Materials letters
container_volume 63
creator Tang, Y
Nian, J
Yu, B.
Yang, W
description Synthesis of layered tetratitanate-n-C(1(2H(2(5NH(2) intercalation compounds under microwave radiation was reported in this paper. Under microwave radiation, conversion of K(2)Ti(4)O(9) to H(2)Ti(4)O(9) in 1 M HCl solution needs only 1 h with 0.88 nm of interlayer distance, and the intercalation of n-C(1(2H(2(5NH(2) could be achieved in 3 h. The formations of the layered hydrogen tetratitanate and the intercalation compounds were confirmed by X-ray diffraction, elemental, thermal gravimetric and differential scanning calorimetric analyses. The interlayer distance of the composite material could expand to 3.92 nm after the intercalation. High power of microwave is favorable during the intercalation of n-C(1(2H(2(5NH(2) into the layered hydrogen tetratitanate.
doi_str_mv 10.1016/j.matlet.2009.06.022
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title Intercalation of n-C(1(2H(2(5NH(2) into layered titanate with the aid of microwave radiation
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