X-ray powder diffraction structural characterization of iron(III) chloro- and bromo-complexes of triphenylphosphine oxide

Iron (III) complexes of the composition [FeX2(OPPh3)4][FeX4], where X is Cl or Br were synthesised by several methods. It was found that each particular synthesis has yielded solids with slightly different powder patterns and also their comparison to those of calculated from single crystal data show...

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Veröffentlicht in:	Crystal research and technology (1979) 2003-02, Vol.38 (2), p.174-181
Hauptverfasser:	Jorík, V., Ondrejkovicová, I., von Dreele, R. B., Ehrenberg, H.
Format:	Artikel
Sprache:	eng
Schlagworte:	Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Inorganic compounds iron(III) complexes Metal complexes Physics powder diffraction Rietveld refinement rigid body Single-crystal and powder diffraction Structure of solids and liquids crystallography Structure of specific crystalline solids X-ray diffraction and scattering
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