Anionic clay–Pt metal nanoparticle composite through intercalation of hexachloroplatinate in nickel zinc hydroxysalt
Nickel zinc hydroxysalt–Pt metal nanoparticle composite was prepared by intercalation of the anionic platinum complex, [PtCl 6] 2− in nickel zinc hydroxysalt through ion exchange reaction and subsequent reduction of the platinum complex by ethanol. Powder X-ray diffraction and microscopy studies ind...
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| Veröffentlicht in: | Solid state sciences 2009-07, Vol.11 (7), p.1270-1274 |
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| creator | Rajamathi, Jacqueline T. Ahmed, Mohammed F. Ravishankar, N. Nethravathi, C. Rajamathi, Michael |
| description | Nickel zinc hydroxysalt–Pt metal nanoparticle composite was prepared by intercalation of the anionic platinum complex, [PtCl
6]
2− in nickel zinc hydroxysalt through ion exchange reaction and subsequent reduction of the platinum complex by ethanol. Powder X-ray diffraction and microscopy studies indicate that the process of reduction of the platinum complex in the interlayer region of the anionic clay takes place topotactically without destroying the layers.
Nickel zinc hydroxysalt was intercalated with [PtCl
6]
2− by ion exchange reaction. The intercalated solid was subsequently reduced by refluxing in ethanol to form anionic clay–platinum nanoparticle composite.
[Display omitted] |
| doi_str_mv | 10.1016/j.solidstatesciences.2009.03.020 |
| format | Article |
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6]
2− in nickel zinc hydroxysalt through ion exchange reaction and subsequent reduction of the platinum complex by ethanol. Powder X-ray diffraction and microscopy studies indicate that the process of reduction of the platinum complex in the interlayer region of the anionic clay takes place topotactically without destroying the layers.
Nickel zinc hydroxysalt was intercalated with [PtCl
6]
2− by ion exchange reaction. The intercalated solid was subsequently reduced by refluxing in ethanol to form anionic clay–platinum nanoparticle composite.
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6]
2− in nickel zinc hydroxysalt through ion exchange reaction and subsequent reduction of the platinum complex by ethanol. Powder X-ray diffraction and microscopy studies indicate that the process of reduction of the platinum complex in the interlayer region of the anionic clay takes place topotactically without destroying the layers.
Nickel zinc hydroxysalt was intercalated with [PtCl
6]
2− by ion exchange reaction. The intercalated solid was subsequently reduced by refluxing in ethanol to form anionic clay–platinum nanoparticle composite.
[Display omitted]</description><subject>Anionic clays</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Hexachloroplatinate</subject><subject>Ion exchange</subject><subject>Materials science</subject><subject>Nanocomposite</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Other topics in nanoscale materials and structures</subject><subject>Physics</subject><issn>1293-2558</issn><issn>1873-3085</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNqNkEuO1DAQhiMEEsPAHbwBsUnwM4l3jEYMD40EC1hb7kqFuHHbwXaPpllxB27ISXCrW2zYsLLl-vxV1d80LxntGGX9q22Xo3dTLrZgBocBMHecUt1R0VFOHzQXbBxEK-ioHtY716LlSo2Pmyc5bymlfT_Ii-buKrgYHBDw9vD7569PheywWE-CDXG1qTjwSCDu1phdQVKWFPdfF-JCwQTW21K_kziTBe8tLD6muB4fQx2rQqSqv6EnP1wAshymFO8P2frytHk0W5_x2fm8bL7cvPl8_a69_fj2_fXVbQuSitJOWmotEXCyTA849DiocRyl3OhZoVQbNvPNZsJJCa4onSXMFjWM2oKstUlcNi9O3jXF73vMxexcBvTeBoz7bIRUbOg5r-DrEwgp5pxwNmtyO5sOhlFzDNxszb-Bm2PghgpTA6-K5-deNtdk5mQDuPzXw1mvpVCych9OHNbF7xwmc9ZNLiEUM0X3_03_ABXAqPo</recordid><startdate>20090701</startdate><enddate>20090701</enddate><creator>Rajamathi, Jacqueline T.</creator><creator>Ahmed, Mohammed F.</creator><creator>Ravishankar, N.</creator><creator>Nethravathi, C.</creator><creator>Rajamathi, Michael</creator><general>Elsevier Masson SAS</general><general>Elsevier Masson</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20090701</creationdate><title>Anionic clay–Pt metal nanoparticle composite through intercalation of hexachloroplatinate in nickel zinc hydroxysalt</title><author>Rajamathi, Jacqueline T. ; Ahmed, Mohammed F. ; Ravishankar, N. ; Nethravathi, C. ; Rajamathi, Michael</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c403t-d94994eceda197e76e7588844b9f5e45b1f2bbded532500f4cfae9c89ac4b1fd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Anionic clays</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Hexachloroplatinate</topic><topic>Ion exchange</topic><topic>Materials science</topic><topic>Nanocomposite</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Other topics in nanoscale materials and structures</topic><topic>Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Rajamathi, Jacqueline T.</creatorcontrib><creatorcontrib>Ahmed, Mohammed F.</creatorcontrib><creatorcontrib>Ravishankar, N.</creatorcontrib><creatorcontrib>Nethravathi, C.</creatorcontrib><creatorcontrib>Rajamathi, Michael</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Solid state sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Rajamathi, Jacqueline T.</au><au>Ahmed, Mohammed F.</au><au>Ravishankar, N.</au><au>Nethravathi, C.</au><au>Rajamathi, Michael</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Anionic clay–Pt metal nanoparticle composite through intercalation of hexachloroplatinate in nickel zinc hydroxysalt</atitle><jtitle>Solid state sciences</jtitle><date>2009-07-01</date><risdate>2009</risdate><volume>11</volume><issue>7</issue><spage>1270</spage><epage>1274</epage><pages>1270-1274</pages><issn>1293-2558</issn><eissn>1873-3085</eissn><abstract>Nickel zinc hydroxysalt–Pt metal nanoparticle composite was prepared by intercalation of the anionic platinum complex, [PtCl
6]
2− in nickel zinc hydroxysalt through ion exchange reaction and subsequent reduction of the platinum complex by ethanol. Powder X-ray diffraction and microscopy studies indicate that the process of reduction of the platinum complex in the interlayer region of the anionic clay takes place topotactically without destroying the layers.
Nickel zinc hydroxysalt was intercalated with [PtCl
6]
2− by ion exchange reaction. The intercalated solid was subsequently reduced by refluxing in ethanol to form anionic clay–platinum nanoparticle composite.
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| fulltext | fulltext |
| identifier | ISSN: 1293-2558 |
| ispartof | Solid state sciences, 2009-07, Vol.11 (7), p.1270-1274 |
| issn | 1293-2558 1873-3085 |
| language | eng |
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| source | ScienceDirect |
| subjects | Anionic clays Cross-disciplinary physics: materials science rheology Exact sciences and technology Hexachloroplatinate Ion exchange Materials science Nanocomposite Nanoscale materials and structures: fabrication and characterization Other topics in nanoscale materials and structures Physics |
| title | Anionic clay–Pt metal nanoparticle composite through intercalation of hexachloroplatinate in nickel zinc hydroxysalt |
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