Preparation and Characterization of NiO Nanoparticles by Anodic Arc Plasma Method
NiO nanoparticles with average particle size of 25 nm were successfully prepared by anodic arc plasma method. The composition, morphology, crystal microstructure, specific surface area, infrared spectra, and particle size distribution of product were analyzed by using X-ray diffraction (XRD), transm...
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| Veröffentlicht in: | Journal of nanomaterials 2009-01, Vol.2009 (2009), p.1-5 |
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| container_issue | 2009 |
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| container_title | Journal of nanomaterials |
| container_volume | 2009 |
| creator | Qiao, Hongxia Wei, Zhiqiang Yang, Hua Zhu, Lin Yan, Xiaoyan |
| description | NiO nanoparticles with average particle size of 25 nm were successfully prepared by anodic arc plasma method. The composition, morphology, crystal microstructure, specific surface area, infrared spectra, and particle size distribution of product were analyzed by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectrum, and Brunauer-Emmett-Teller (BET) N2 adsorption. The experiment results show that the NiO nanoparticles are bcc structure with spherical shape and well dispersed, the particle size distribution ranging from 15 to 45 nm with the average particle size is about 25 nm, and the specific surface area is 33 m2/g. The infrared absorption band of NiO nanoparticles shows blue shifts compared with that of bulk NiO. |
| doi_str_mv | 10.1155/2009/795928 |
| format | Article |
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The composition, morphology, crystal microstructure, specific surface area, infrared spectra, and particle size distribution of product were analyzed by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectrum, and Brunauer-Emmett-Teller (BET) N2 adsorption. The experiment results show that the NiO nanoparticles are bcc structure with spherical shape and well dispersed, the particle size distribution ranging from 15 to 45 nm with the average particle size is about 25 nm, and the specific surface area is 33 m2/g. The infrared absorption band of NiO nanoparticles shows blue shifts compared with that of bulk NiO.</description><identifier>ISSN: 1687-4110</identifier><identifier>EISSN: 1687-4129</identifier><identifier>DOI: 10.1155/2009/795928</identifier><language>eng</language><publisher>Cairo, Egypt: Hindawi Puplishing Corporation</publisher><subject>Adsorption ; Atoms & subatomic particles ; Colleges & universities ; Fourier transforms ; Gases ; Grain size ; High temperature ; Methods ; Mineralogy ; Nanocrystals ; Nanomaterials ; Spectrum analysis ; Vibration</subject><ispartof>Journal of nanomaterials, 2009-01, Vol.2009 (2009), p.1-5</ispartof><rights>Copyright © 2009</rights><rights>Copyright © 2009 Hongxia Qiao et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a520t-e5c4483f66ec7049c0c05565bf603cc990a59d124e92ccb8bc1a3a72f0c0ebd13</citedby><cites>FETCH-LOGICAL-a520t-e5c4483f66ec7049c0c05565bf603cc990a59d124e92ccb8bc1a3a72f0c0ebd13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><contributor>Xu, Min</contributor><creatorcontrib>Qiao, Hongxia</creatorcontrib><creatorcontrib>Wei, Zhiqiang</creatorcontrib><creatorcontrib>Yang, Hua</creatorcontrib><creatorcontrib>Zhu, Lin</creatorcontrib><creatorcontrib>Yan, Xiaoyan</creatorcontrib><title>Preparation and Characterization of NiO Nanoparticles by Anodic Arc Plasma Method</title><title>Journal of nanomaterials</title><description>NiO nanoparticles with average particle size of 25 nm were successfully prepared by anodic arc plasma method. The composition, morphology, crystal microstructure, specific surface area, infrared spectra, and particle size distribution of product were analyzed by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectrum, and Brunauer-Emmett-Teller (BET) N2 adsorption. The experiment results show that the NiO nanoparticles are bcc structure with spherical shape and well dispersed, the particle size distribution ranging from 15 to 45 nm with the average particle size is about 25 nm, and the specific surface area is 33 m2/g. The infrared absorption band of NiO nanoparticles shows blue shifts compared with that of bulk NiO.</description><subject>Adsorption</subject><subject>Atoms & subatomic particles</subject><subject>Colleges & universities</subject><subject>Fourier transforms</subject><subject>Gases</subject><subject>Grain size</subject><subject>High temperature</subject><subject>Methods</subject><subject>Mineralogy</subject><subject>Nanocrystals</subject><subject>Nanomaterials</subject><subject>Spectrum analysis</subject><subject>Vibration</subject><issn>1687-4110</issn><issn>1687-4129</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><sourceid>RHX</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqF0M9LwzAUB_AgCs7pybMQPHhQ6pI0aZvjGP6CuU3Qc3hNU5bRNTPpkPnXm1HZwYun94MPj8cXoUtK7ikVYsQIkaNcCsmKIzSgWZEnnDJ5fOgpOUVnIawI4UIKNkBvC2824KGzrsXQVniyjJPujLff_dLVeGbneAati7CzujEBlzs8bl1lNR57jRcNhDXgV9MtXXWOTmpogrn4rUP08fjwPnlOpvOnl8l4moBgpEuM0JwXaZ1lRueES000ESITZZ2RVGspCQhZUcaNZFqXRakppJCzOjpTVjQdopv-7sa7z60JnVrboE3TQGvcNqiUp5QzkUd4_Qeu3Na38TdViIxwynkW0V2PtHcheFOrjbdr8DtFidpnq_bZqj7bqG97vbRtBV_2H3zVYxOJqeGAuSwKStMfuT2Bdg</recordid><startdate>20090101</startdate><enddate>20090101</enddate><creator>Qiao, Hongxia</creator><creator>Wei, Zhiqiang</creator><creator>Yang, Hua</creator><creator>Zhu, Lin</creator><creator>Yan, Xiaoyan</creator><general>Hindawi Puplishing Corporation</general><general>Hindawi Publishing Corporation</general><general>Hindawi Limited</general><scope>ADJCN</scope><scope>AHFXO</scope><scope>RHU</scope><scope>RHW</scope><scope>RHX</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>CWDGH</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>F28</scope><scope>FR3</scope></search><sort><creationdate>20090101</creationdate><title>Preparation and Characterization of NiO Nanoparticles by Anodic Arc Plasma Method</title><author>Qiao, Hongxia ; 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The composition, morphology, crystal microstructure, specific surface area, infrared spectra, and particle size distribution of product were analyzed by using X-ray diffraction (XRD), transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectrum, and Brunauer-Emmett-Teller (BET) N2 adsorption. The experiment results show that the NiO nanoparticles are bcc structure with spherical shape and well dispersed, the particle size distribution ranging from 15 to 45 nm with the average particle size is about 25 nm, and the specific surface area is 33 m2/g. The infrared absorption band of NiO nanoparticles shows blue shifts compared with that of bulk NiO.</abstract><cop>Cairo, Egypt</cop><pub>Hindawi Puplishing Corporation</pub><doi>10.1155/2009/795928</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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| source | Wiley Online Library Open Access; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection; Free Full-Text Journals in Chemistry |
| subjects | Adsorption Atoms & subatomic particles Colleges & universities Fourier transforms Gases Grain size High temperature Methods Mineralogy Nanocrystals Nanomaterials Spectrum analysis Vibration |
| title | Preparation and Characterization of NiO Nanoparticles by Anodic Arc Plasma Method |
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