Synthesis and characterization of bis(nicotinamide) m-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II)
The mixed-ligand m -hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) with nicotinamide were synthesized and characterized. The chemical, FT IR and UV-vis spectrophotometric, thermal and mass spectral analyses, magnetic susceptibility measurements revealed that the compounds contain two...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2008-08, Vol.93 (2), p.509-514 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Kose, D A Necefoglu, H |
| description | The mixed-ligand
m
-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) with nicotinamide were synthesized and characterized. The chemical, FT IR and UV-vis spectrophotometric, thermal and mass spectral analyses, magnetic susceptibility measurements revealed that the compounds contain two water molecules, two
m
-hydroxybenzoate (
m
-hba) and two nicotinamide (na) ligands per formula unit.
m
-Hydroxybenzoate and nicotinamide ligands bind to the metal atoms monodentately through their acidic oxygen and pyridinic nitrogen atoms, respectively. The thermal decomposition pathways and the stability of the complexes are interpreted in the terms of the structural data. |
| doi_str_mv | 10.1007/s10973-007-8712-5 |
| format | Article |
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m
-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) with nicotinamide were synthesized and characterized. The chemical, FT IR and UV-vis spectrophotometric, thermal and mass spectral analyses, magnetic susceptibility measurements revealed that the compounds contain two water molecules, two
m
-hydroxybenzoate (
m
-hba) and two nicotinamide (na) ligands per formula unit.
m
-Hydroxybenzoate and nicotinamide ligands bind to the metal atoms monodentately through their acidic oxygen and pyridinic nitrogen atoms, respectively. The thermal decomposition pathways and the stability of the complexes are interpreted in the terms of the structural data.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>EISSN: 1572-8943</identifier><identifier>DOI: 10.1007/s10973-007-8712-5</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Analytical Chemistry ; Chemistry ; Chemistry and Materials Science ; Coordination compounds ; Exact sciences and technology ; Inorganic Chemistry ; Inorganic chemistry and origins of life ; Measurement Science and Instrumentation ; Physical Chemistry ; Polymer Sciences ; Preparations and properties</subject><ispartof>Journal of thermal analysis and calorimetry, 2008-08, Vol.93 (2), p.509-514</ispartof><rights>Springer Science+Business Media, LLC. 2008</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c349t-f2ac742cf3711b9d706ef58ecfd1212613a13cf6e7f137051cb58c8812ac60493</citedby><cites>FETCH-LOGICAL-c349t-f2ac742cf3711b9d706ef58ecfd1212613a13cf6e7f137051cb58c8812ac60493</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-007-8712-5$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-007-8712-5$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20534713$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Kose, D A</creatorcontrib><creatorcontrib>Necefoglu, H</creatorcontrib><title>Synthesis and characterization of bis(nicotinamide) m-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II)</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>The mixed-ligand
m
-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) with nicotinamide were synthesized and characterized. The chemical, FT IR and UV-vis spectrophotometric, thermal and mass spectral analyses, magnetic susceptibility measurements revealed that the compounds contain two water molecules, two
m
-hydroxybenzoate (
m
-hba) and two nicotinamide (na) ligands per formula unit.
m
-Hydroxybenzoate and nicotinamide ligands bind to the metal atoms monodentately through their acidic oxygen and pyridinic nitrogen atoms, respectively. The thermal decomposition pathways and the stability of the complexes are interpreted in the terms of the structural data.</description><subject>Analytical Chemistry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Coordination compounds</subject><subject>Exact sciences and technology</subject><subject>Inorganic Chemistry</subject><subject>Inorganic chemistry and origins of life</subject><subject>Measurement Science and Instrumentation</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Preparations and properties</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNp9kE9LxDAUxIsouKgfwFsvygpW85KmSY-y-GdB9KBevIQ0TdxIm6xJF1w_vakVj57mB29m4E2WHQO6AITYZQRUM1IkLDgDXNCdbAaU8wLXuNpNTBJXQNF-dhSjbRAGVNWU17NseNq6YaWjjbl0ba5WMkg16GC_5GC9y73JGxvnzio_WCd72-qzvC9W2zb4z22j3ZeXg86V79ed_tRxDCz8fLk8O88f7KSLzag__a9uxMNsz8gu6qNfPchebq6fF3fF_ePtcnF1XyhS1kNhsFSsxMoQBtDULUOVNpRrZVrAgCsgEogylWYGCEMUVEO54hxSrkJlTQ6y06l3HfzHRsdB9DYq3XXSab-JgpTJxUmVjDAZVfAxBm3EOthehq0AJMaJxTSxGHGcWNCUOfktl1HJzgTplI1_QYwoKRmQ5MOTL6aTe9NBvPtNcOnvf8q_Aaoaibs</recordid><startdate>20080801</startdate><enddate>20080801</enddate><creator>Kose, D A</creator><creator>Necefoglu, H</creator><general>Springer Netherlands</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20080801</creationdate><title>Synthesis and characterization of bis(nicotinamide) m-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II)</title><author>Kose, D A ; Necefoglu, H</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c349t-f2ac742cf3711b9d706ef58ecfd1212613a13cf6e7f137051cb58c8812ac60493</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Analytical Chemistry</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Coordination compounds</topic><topic>Exact sciences and technology</topic><topic>Inorganic Chemistry</topic><topic>Inorganic chemistry and origins of life</topic><topic>Measurement Science and Instrumentation</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Preparations and properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kose, D A</creatorcontrib><creatorcontrib>Necefoglu, H</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kose, D A</au><au>Necefoglu, H</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of bis(nicotinamide) m-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II)</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2008-08-01</date><risdate>2008</risdate><volume>93</volume><issue>2</issue><spage>509</spage><epage>514</epage><pages>509-514</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><eissn>1572-8943</eissn><abstract>The mixed-ligand
m
-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) with nicotinamide were synthesized and characterized. The chemical, FT IR and UV-vis spectrophotometric, thermal and mass spectral analyses, magnetic susceptibility measurements revealed that the compounds contain two water molecules, two
m
-hydroxybenzoate (
m
-hba) and two nicotinamide (na) ligands per formula unit.
m
-Hydroxybenzoate and nicotinamide ligands bind to the metal atoms monodentately through their acidic oxygen and pyridinic nitrogen atoms, respectively. The thermal decomposition pathways and the stability of the complexes are interpreted in the terms of the structural data.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-007-8712-5</doi><tpages>6</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Analytical Chemistry Chemistry Chemistry and Materials Science Coordination compounds Exact sciences and technology Inorganic Chemistry Inorganic chemistry and origins of life Measurement Science and Instrumentation Physical Chemistry Polymer Sciences Preparations and properties |
| title | Synthesis and characterization of bis(nicotinamide) m-hydroxybenzoate complexes of Co(II), Ni(II), Cu(II) and Zn(II) |
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