Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol
Nanocrystalline 3 mol.-% yttria doped tetragonal zirconia polycrstal was synthesised by coprecipitation method. Presence of ammonium sulphate (inorganic) and polyethylene glycol (organic) in optimised quantity in the precipitating bath facilitated formation of an easily filterable precipitate. Calci...
Gespeichert in:
| Veröffentlicht in: | Advances in applied ceramics 2009-04, Vol.108 (3), p.183-188 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 188 |
|---|---|
| container_issue | 3 |
| container_start_page | 183 |
| container_title | Advances in applied ceramics |
| container_volume | 108 |
| creator | Ghosh, A. Suri, A. K. Rao, B. T. Ramamohan, T. R. |
| description | Nanocrystalline 3 mol.-% yttria doped tetragonal zirconia polycrstal was synthesised by coprecipitation method. Presence of ammonium sulphate (inorganic) and polyethylene glycol (organic) in optimised quantity in the precipitating bath facilitated formation of an easily filterable precipitate. Calcination of this precursor at 800°C yielded soft agglomerated nanocrystalline powder (∼22 nm). Compaction behaviour of the calcined powder as well as pore size distribution of the compact mass indicated formation of soft agglomerate. Owing to its high sinteractivity, this powder could be sintered to ∼95% of its theoretical density (%TD) at temperature as low as 1150°C. At 1200°C, the powder compact densified to >98%TD. |
| doi_str_mv | 10.1179/174367608X353629 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_infor</sourceid><recordid>TN_cdi_proquest_miscellaneous_33930928</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sage_id>10.1179_174367608X353629</sage_id><sourcerecordid>33930928</sourcerecordid><originalsourceid>FETCH-LOGICAL-c364t-77c09e612935aec0b9703416b5caaba1711ba65506856d95aa680549c0ff69d13</originalsourceid><addsrcrecordid>eNp9kM1L5TAUxYso-Ll3mdXsqslLkzS4GkRnBEFBBXVT7ktvfZE0qUmq9L-3jzfMQtDVvRx-53DvKYpjRk8YU_qUqYpLJWn9yAWXC71V7K2lctbY9v9d8N1iP6VXSrlSdbVXvN1NPq8w2URCRzz4YOKUMjhnPZJkfcYIJtt3JPypvH--JUP4aDES68kQMaE3uHZC3wdvx56k0Q0ryEjAtzPrJoJ5NTmc017cZII7LHY6cAmP_s2D4uHy4v78b3l98-fq_Pd1abiscqmUoRolW2guAA1dakV5xeRSGIAlMMXYEqQQVNZCtloAyJqKShvadVK3jB8Uvza5QwxvI6bc9DYZdA48hjE1nGtO9aKeQboBTQwpReyaIdoe4tQw2qy7bb52O1vKjSXBCzavYYx-fuUn_mzDW9-F2MNHiK5tMkwuxC6CN3a-51v3Jyf8je4</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>33930928</pqid></control><display><type>article</type><title>Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol</title><source>SAGE Complete A-Z List</source><creator>Ghosh, A. ; Suri, A. K. ; Rao, B. T. ; Ramamohan, T. R.</creator><creatorcontrib>Ghosh, A. ; Suri, A. K. ; Rao, B. T. ; Ramamohan, T. R.</creatorcontrib><description>Nanocrystalline 3 mol.-% yttria doped tetragonal zirconia polycrstal was synthesised by coprecipitation method. Presence of ammonium sulphate (inorganic) and polyethylene glycol (organic) in optimised quantity in the precipitating bath facilitated formation of an easily filterable precipitate. Calcination of this precursor at 800°C yielded soft agglomerated nanocrystalline powder (∼22 nm). Compaction behaviour of the calcined powder as well as pore size distribution of the compact mass indicated formation of soft agglomerate. Owing to its high sinteractivity, this powder could be sintered to ∼95% of its theoretical density (%TD) at temperature as low as 1150°C. At 1200°C, the powder compact densified to >98%TD.</description><identifier>ISSN: 1743-6753</identifier><identifier>EISSN: 1743-6761</identifier><identifier>DOI: 10.1179/174367608X353629</identifier><language>eng</language><publisher>London, England: Taylor & Francis</publisher><subject>AGGLOMERATION ; COMPACTION ; COPRECIPITATION ; NANOCRYSTALLINE ; SINTERING ; TETRAGONAL ZIRCONIA POLYCRYSTAL</subject><ispartof>Advances in applied ceramics, 2009-04, Vol.108 (3), p.183-188</ispartof><rights>2009 Maney Publishing 2009</rights><rights>2009 Maney Publishing</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c364t-77c09e612935aec0b9703416b5caaba1711ba65506856d95aa680549c0ff69d13</citedby><cites>FETCH-LOGICAL-c364t-77c09e612935aec0b9703416b5caaba1711ba65506856d95aa680549c0ff69d13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://journals.sagepub.com/doi/pdf/10.1179/174367608X353629$$EPDF$$P50$$Gsage$$H</linktopdf><linktohtml>$$Uhttps://journals.sagepub.com/doi/10.1179/174367608X353629$$EHTML$$P50$$Gsage$$H</linktohtml><link.rule.ids>314,780,784,21819,27924,27925,43621,43622</link.rule.ids></links><search><creatorcontrib>Ghosh, A.</creatorcontrib><creatorcontrib>Suri, A. K.</creatorcontrib><creatorcontrib>Rao, B. T.</creatorcontrib><creatorcontrib>Ramamohan, T. R.</creatorcontrib><title>Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol</title><title>Advances in applied ceramics</title><description>Nanocrystalline 3 mol.-% yttria doped tetragonal zirconia polycrstal was synthesised by coprecipitation method. Presence of ammonium sulphate (inorganic) and polyethylene glycol (organic) in optimised quantity in the precipitating bath facilitated formation of an easily filterable precipitate. Calcination of this precursor at 800°C yielded soft agglomerated nanocrystalline powder (∼22 nm). Compaction behaviour of the calcined powder as well as pore size distribution of the compact mass indicated formation of soft agglomerate. Owing to its high sinteractivity, this powder could be sintered to ∼95% of its theoretical density (%TD) at temperature as low as 1150°C. At 1200°C, the powder compact densified to >98%TD.</description><subject>AGGLOMERATION</subject><subject>COMPACTION</subject><subject>COPRECIPITATION</subject><subject>NANOCRYSTALLINE</subject><subject>SINTERING</subject><subject>TETRAGONAL ZIRCONIA POLYCRYSTAL</subject><issn>1743-6753</issn><issn>1743-6761</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNp9kM1L5TAUxYso-Ll3mdXsqslLkzS4GkRnBEFBBXVT7ktvfZE0qUmq9L-3jzfMQtDVvRx-53DvKYpjRk8YU_qUqYpLJWn9yAWXC71V7K2lctbY9v9d8N1iP6VXSrlSdbVXvN1NPq8w2URCRzz4YOKUMjhnPZJkfcYIJtt3JPypvH--JUP4aDES68kQMaE3uHZC3wdvx56k0Q0ryEjAtzPrJoJ5NTmc017cZII7LHY6cAmP_s2D4uHy4v78b3l98-fq_Pd1abiscqmUoRolW2guAA1dakV5xeRSGIAlMMXYEqQQVNZCtloAyJqKShvadVK3jB8Uvza5QwxvI6bc9DYZdA48hjE1nGtO9aKeQboBTQwpReyaIdoe4tQw2qy7bb52O1vKjSXBCzavYYx-fuUn_mzDW9-F2MNHiK5tMkwuxC6CN3a-51v3Jyf8je4</recordid><startdate>20090401</startdate><enddate>20090401</enddate><creator>Ghosh, A.</creator><creator>Suri, A. K.</creator><creator>Rao, B. T.</creator><creator>Ramamohan, T. R.</creator><general>Taylor & Francis</general><general>SAGE Publications</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20090401</creationdate><title>Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol</title><author>Ghosh, A. ; Suri, A. K. ; Rao, B. T. ; Ramamohan, T. R.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c364t-77c09e612935aec0b9703416b5caaba1711ba65506856d95aa680549c0ff69d13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>AGGLOMERATION</topic><topic>COMPACTION</topic><topic>COPRECIPITATION</topic><topic>NANOCRYSTALLINE</topic><topic>SINTERING</topic><topic>TETRAGONAL ZIRCONIA POLYCRYSTAL</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ghosh, A.</creatorcontrib><creatorcontrib>Suri, A. K.</creatorcontrib><creatorcontrib>Rao, B. T.</creatorcontrib><creatorcontrib>Ramamohan, T. R.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Advances in applied ceramics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ghosh, A.</au><au>Suri, A. K.</au><au>Rao, B. T.</au><au>Ramamohan, T. R.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol</atitle><jtitle>Advances in applied ceramics</jtitle><date>2009-04-01</date><risdate>2009</risdate><volume>108</volume><issue>3</issue><spage>183</spage><epage>188</epage><pages>183-188</pages><issn>1743-6753</issn><eissn>1743-6761</eissn><abstract>Nanocrystalline 3 mol.-% yttria doped tetragonal zirconia polycrstal was synthesised by coprecipitation method. Presence of ammonium sulphate (inorganic) and polyethylene glycol (organic) in optimised quantity in the precipitating bath facilitated formation of an easily filterable precipitate. Calcination of this precursor at 800°C yielded soft agglomerated nanocrystalline powder (∼22 nm). Compaction behaviour of the calcined powder as well as pore size distribution of the compact mass indicated formation of soft agglomerate. Owing to its high sinteractivity, this powder could be sintered to ∼95% of its theoretical density (%TD) at temperature as low as 1150°C. At 1200°C, the powder compact densified to >98%TD.</abstract><cop>London, England</cop><pub>Taylor & Francis</pub><doi>10.1179/174367608X353629</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1743-6753 |
| ispartof | Advances in applied ceramics, 2009-04, Vol.108 (3), p.183-188 |
| issn | 1743-6753 1743-6761 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_33930928 |
| source | SAGE Complete A-Z List |
| subjects | AGGLOMERATION COMPACTION COPRECIPITATION NANOCRYSTALLINE SINTERING TETRAGONAL ZIRCONIA POLYCRYSTAL |
| title | Synthesis of nanocrystalline sinteractive 3Y-TZP powder in presence of ammonium sulphate and poly ethylene glycol |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-05T14%3A33%3A41IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_infor&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Synthesis%20of%20nanocrystalline%20sinteractive%203Y-TZP%20powder%20in%20presence%20of%20ammonium%20sulphate%20and%20poly%20ethylene%20glycol&rft.jtitle=Advances%20in%20applied%20ceramics&rft.au=Ghosh,%20A.&rft.date=2009-04-01&rft.volume=108&rft.issue=3&rft.spage=183&rft.epage=188&rft.pages=183-188&rft.issn=1743-6753&rft.eissn=1743-6761&rft_id=info:doi/10.1179/174367608X353629&rft_dat=%3Cproquest_infor%3E33930928%3C/proquest_infor%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=33930928&rft_id=info:pmid/&rft_sage_id=10.1179_174367608X353629&rfr_iscdi=true |