An anelastic spectroscopy, differential scanning calorimetry and X-ray diffraction study of the crystallization process of Mg–Ni–Fe alloys
The effects of heating-induced crystallization on the structural and mechanical properties of Mg–Ni–Fe amorphous ribbons were studied by anelastic spectroscopy, differential scanning calorimetry (DSC) and X-ray diffraction. DSC results show that the crystallization occurs through several non-reversi...
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Veröffentlicht in: | Journal of alloys and compounds 2008-09, Vol.463 (1), p.148-152 |
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container_title | Journal of alloys and compounds |
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creator | Palumbo, O. Paolone, A. Cantelli, R. Giannini, C. Gagliardi, A. Reale, P. Scrosati, B. Russo, S. Lo Maddalena, A. Palade, P. Principi, G. Schinteie, G. |
description | The effects of heating-induced crystallization on the structural and mechanical properties of Mg–Ni–Fe amorphous ribbons were studied by anelastic spectroscopy, differential scanning calorimetry (DSC) and X-ray diffraction. DSC results show that the crystallization occurs through several non-reversible steps, which correspond to significant changes in the Young's modulus and concomitant irreversible elastic energy loss peaks. Moreover, an anelastic peak is found at 215
K, which for the first time indicates the presence of some dynamical process related to the simultaneous presence of different phases. The formation of a metastable Mg
6Ni phase is detected, which transforms into Mg and Mg
2Ni stable phases. A quantitative analysis of the different phases present at the different steps was also carried out. |
doi_str_mv | 10.1016/j.jallcom.2007.08.081 |
format | Article |
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K, which for the first time indicates the presence of some dynamical process related to the simultaneous presence of different phases. The formation of a metastable Mg
6Ni phase is detected, which transforms into Mg and Mg
2Ni stable phases. A quantitative analysis of the different phases present at the different steps was also carried out.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2007.08.081</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Cross-disciplinary physics: materials science; rheology ; Crystal structure and symmetry ; Exact sciences and technology ; Growth from solid phases (including multiphase diffusion and recrystallization) ; Materials science ; Methods of crystal growth; physics of crystal growth ; Physics ; Thermal analysis ; X-ray diffraction</subject><ispartof>Journal of alloys and compounds, 2008-09, Vol.463 (1), p.148-152</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c370t-33a5ae300f35a37743e5355ddd777603b7d16a3774261cd639a7f36c2bb3aa2c3</citedby><cites>FETCH-LOGICAL-c370t-33a5ae300f35a37743e5355ddd777603b7d16a3774261cd639a7f36c2bb3aa2c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jallcom.2007.08.081$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20557598$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Palumbo, O.</creatorcontrib><creatorcontrib>Paolone, A.</creatorcontrib><creatorcontrib>Cantelli, R.</creatorcontrib><creatorcontrib>Giannini, C.</creatorcontrib><creatorcontrib>Gagliardi, A.</creatorcontrib><creatorcontrib>Reale, P.</creatorcontrib><creatorcontrib>Scrosati, B.</creatorcontrib><creatorcontrib>Russo, S. Lo</creatorcontrib><creatorcontrib>Maddalena, A.</creatorcontrib><creatorcontrib>Palade, P.</creatorcontrib><creatorcontrib>Principi, G.</creatorcontrib><creatorcontrib>Schinteie, G.</creatorcontrib><title>An anelastic spectroscopy, differential scanning calorimetry and X-ray diffraction study of the crystallization process of Mg–Ni–Fe alloys</title><title>Journal of alloys and compounds</title><description>The effects of heating-induced crystallization on the structural and mechanical properties of Mg–Ni–Fe amorphous ribbons were studied by anelastic spectroscopy, differential scanning calorimetry (DSC) and X-ray diffraction. DSC results show that the crystallization occurs through several non-reversible steps, which correspond to significant changes in the Young's modulus and concomitant irreversible elastic energy loss peaks. Moreover, an anelastic peak is found at 215
K, which for the first time indicates the presence of some dynamical process related to the simultaneous presence of different phases. The formation of a metastable Mg
6Ni phase is detected, which transforms into Mg and Mg
2Ni stable phases. 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Moreover, an anelastic peak is found at 215
K, which for the first time indicates the presence of some dynamical process related to the simultaneous presence of different phases. The formation of a metastable Mg
6Ni phase is detected, which transforms into Mg and Mg
2Ni stable phases. A quantitative analysis of the different phases present at the different steps was also carried out.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2007.08.081</doi><tpages>5</tpages></addata></record> |
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subjects | Cross-disciplinary physics: materials science rheology Crystal structure and symmetry Exact sciences and technology Growth from solid phases (including multiphase diffusion and recrystallization) Materials science Methods of crystal growth physics of crystal growth Physics Thermal analysis X-ray diffraction |
title | An anelastic spectroscopy, differential scanning calorimetry and X-ray diffraction study of the crystallization process of Mg–Ni–Fe alloys |
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