Synthesis and characterization of CuO flower-nanostructure processing by a domestic hydrothermal microwave

The synthesis and characterization of CuO flower-nanostructure processed in domestic hydrothermal microwave oven was presented. Phase analysis was carried out using X-ray diffraction (XRD) and micro-Raman scattering (MRS) and the results confirmed the CuO flower-nanostructure as a single-phase. The...

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Veröffentlicht in:Journal of alloys and compounds 2008-07, Vol.459 (1-2), p.537-542
Hauptverfasser: VOLANTI, D. P, KEYSON, D, CAVALCANTE, L. S, SIMOES, A. Z, JOYA, M. R, LONGO, E, VARELA, J. A, PIZANI, P. S, SOUZA, A. G
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Sprache:eng
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Zusammenfassung:The synthesis and characterization of CuO flower-nanostructure processed in domestic hydrothermal microwave oven was presented. Phase analysis was carried out using X-ray diffraction (XRD) and micro-Raman scattering (MRS) and the results confirmed the CuO flower-nanostructure as a single-phase. The field-emission scanning electron microscopy (FEG-SEM) was used to estimate the average spheres diameter while transmission electron microscope (TEM) to observe the thorn of the flower-nanostructures. The mechanism of CuO flower-nanostructures formation is proposed and explained.
ISSN:0925-8388
1873-4669
DOI:10.1016/j.jallcom.2007.05.023