Silica gel surface-imprinted solid-phase extraction of Zr(IV) from aqueous solutions
. A surface imprinted amino-functionalized silica gel material was synthesized by combining a surface molecular imprinting technology for the solid-phase extraction of Zr(IV) in aqueous solutions prior to the measurement by inductively coupled plasma atomic emission spectrometry. The ion-imprinted s...
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| Veröffentlicht in: | Mikrochimica acta (1966) 2008-07, Vol.162 (1-2), p.113-119 |
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| container_title | Mikrochimica acta (1966) |
| container_volume | 162 |
| creator | Chang, Xijun Wang, Xiaoyan Jiang, Na He, Qun Zhai, Yunhui Zhu, Xiangbing Hu, Zheng |
| description | .
A surface imprinted amino-functionalized silica gel material was synthesized by combining a surface molecular imprinting technology for the solid-phase extraction of Zr(IV) in aqueous solutions prior to the measurement by inductively coupled plasma atomic emission spectrometry. The ion-imprinted sorbent had higher selectivity and adsorption capacity for Zr(IV). The maximum static adsorption capacity of the ion-imprinted and non-imprinted sorbent for Zr(IV) was 11 mg g
−1
and 0.3 mg g
−1
, respectively. The relatively selective factor values of Zr(IV)/Ti(IV), Zr(IV)/Y(III) and Zr(IV)/Nb(V) were 32, 34 and 50, which were greater than 1. The distribution ratio values of Zr(IV)-imprinted polymers for Zr(IV) were greatly larger than that for Ti(IV), Y(III) and Nb(V). The detection limit was 0.14 ng mL
−1
. The relative standard deviation of the method was 1.49% for eight replicate determinations. The method was successfully applied to the determination of trace zirconium in some alloys and in tape and waste water samples. |
| doi_str_mv | 10.1007/s00604-007-0870-4 |
| format | Article |
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A surface imprinted amino-functionalized silica gel material was synthesized by combining a surface molecular imprinting technology for the solid-phase extraction of Zr(IV) in aqueous solutions prior to the measurement by inductively coupled plasma atomic emission spectrometry. The ion-imprinted sorbent had higher selectivity and adsorption capacity for Zr(IV). The maximum static adsorption capacity of the ion-imprinted and non-imprinted sorbent for Zr(IV) was 11 mg g
−1
and 0.3 mg g
−1
, respectively. The relatively selective factor values of Zr(IV)/Ti(IV), Zr(IV)/Y(III) and Zr(IV)/Nb(V) were 32, 34 and 50, which were greater than 1. The distribution ratio values of Zr(IV)-imprinted polymers for Zr(IV) were greatly larger than that for Ti(IV), Y(III) and Nb(V). The detection limit was 0.14 ng mL
−1
. The relative standard deviation of the method was 1.49% for eight replicate determinations. The method was successfully applied to the determination of trace zirconium in some alloys and in tape and waste water samples.</description><identifier>ISSN: 0026-3672</identifier><identifier>EISSN: 1436-5073</identifier><identifier>DOI: 10.1007/s00604-007-0870-4</identifier><identifier>CODEN: MIACAQ</identifier><language>eng</language><publisher>Vienna: Springer-Verlag</publisher><subject>Analysis methods ; Analytical Chemistry ; Applied sciences ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Exact sciences and technology ; Global environmental pollution ; Microengineering ; Nanochemistry ; Nanotechnology ; Natural water pollution ; Original Paper ; Pollution ; Spectrometric and optical methods ; Water treatment and pollution</subject><ispartof>Mikrochimica acta (1966), 2008-07, Vol.162 (1-2), p.113-119</ispartof><rights>Springer-Verlag 2007</rights><rights>2009 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c349t-6ddd8c0794f1cabc1a17e5c3fe144100383bcac3dce4d91314b474b69f6d12dc3</citedby><cites>FETCH-LOGICAL-c349t-6ddd8c0794f1cabc1a17e5c3fe144100383bcac3dce4d91314b474b69f6d12dc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00604-007-0870-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00604-007-0870-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20897581$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Chang, Xijun</creatorcontrib><creatorcontrib>Wang, Xiaoyan</creatorcontrib><creatorcontrib>Jiang, Na</creatorcontrib><creatorcontrib>He, Qun</creatorcontrib><creatorcontrib>Zhai, Yunhui</creatorcontrib><creatorcontrib>Zhu, Xiangbing</creatorcontrib><creatorcontrib>Hu, Zheng</creatorcontrib><title>Silica gel surface-imprinted solid-phase extraction of Zr(IV) from aqueous solutions</title><title>Mikrochimica acta (1966)</title><addtitle>Microchim Acta</addtitle><description>.
A surface imprinted amino-functionalized silica gel material was synthesized by combining a surface molecular imprinting technology for the solid-phase extraction of Zr(IV) in aqueous solutions prior to the measurement by inductively coupled plasma atomic emission spectrometry. The ion-imprinted sorbent had higher selectivity and adsorption capacity for Zr(IV). The maximum static adsorption capacity of the ion-imprinted and non-imprinted sorbent for Zr(IV) was 11 mg g
−1
and 0.3 mg g
−1
, respectively. The relatively selective factor values of Zr(IV)/Ti(IV), Zr(IV)/Y(III) and Zr(IV)/Nb(V) were 32, 34 and 50, which were greater than 1. The distribution ratio values of Zr(IV)-imprinted polymers for Zr(IV) were greatly larger than that for Ti(IV), Y(III) and Nb(V). The detection limit was 0.14 ng mL
−1
. The relative standard deviation of the method was 1.49% for eight replicate determinations. The method was successfully applied to the determination of trace zirconium in some alloys and in tape and waste water samples.</description><subject>Analysis methods</subject><subject>Analytical Chemistry</subject><subject>Applied sciences</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Exact sciences and technology</subject><subject>Global environmental pollution</subject><subject>Microengineering</subject><subject>Nanochemistry</subject><subject>Nanotechnology</subject><subject>Natural water pollution</subject><subject>Original Paper</subject><subject>Pollution</subject><subject>Spectrometric and optical methods</subject><subject>Water treatment and pollution</subject><issn>0026-3672</issn><issn>1436-5073</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNp9kEtLxDAUhYMoOI7-AHfZKLqIJk2atEsRHwMDLhxduAlpHmOGTjMmLei_N6WDS1f3wv3O4Z4DwDnBNwRjcZsw5pihvCJcCYzYAZgRRjkqsaCHYIZxwRHlojgGJyltMCaCF2wGVq--9VrBtW1hGqJT2iK_3UXf9dbAFFpv0O5TJQvtdx-V7n3oYHDwI14t3q-hi2EL1ddgw5BGehjv6RQcOdUme7afc_D2-LC6f0bLl6fF_d0SacrqHnFjTKWxqJkjWjWaKCJsqamzhLGcila00UpToy0zNaGENUywhteOG1IYTefgcvLdxZB_SL3c-qRt26pufEhSWtZlXVQZJBOoY0gpWidzwq2KP5JgOfYnp_7kuI79SZY1F3tzlbRqXVSd9ulPWOCqFmVFMldMXBpbW9soN2GIXc79j_kvUz6Asg</recordid><startdate>20080701</startdate><enddate>20080701</enddate><creator>Chang, Xijun</creator><creator>Wang, Xiaoyan</creator><creator>Jiang, Na</creator><creator>He, Qun</creator><creator>Zhai, Yunhui</creator><creator>Zhu, Xiangbing</creator><creator>Hu, Zheng</creator><general>Springer-Verlag</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20080701</creationdate><title>Silica gel surface-imprinted solid-phase extraction of Zr(IV) from aqueous solutions</title><author>Chang, Xijun ; Wang, Xiaoyan ; Jiang, Na ; He, Qun ; Zhai, Yunhui ; Zhu, Xiangbing ; Hu, Zheng</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c349t-6ddd8c0794f1cabc1a17e5c3fe144100383bcac3dce4d91314b474b69f6d12dc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Analysis methods</topic><topic>Analytical Chemistry</topic><topic>Applied sciences</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Exact sciences and technology</topic><topic>Global environmental pollution</topic><topic>Microengineering</topic><topic>Nanochemistry</topic><topic>Nanotechnology</topic><topic>Natural water pollution</topic><topic>Original Paper</topic><topic>Pollution</topic><topic>Spectrometric and optical methods</topic><topic>Water treatment and pollution</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chang, Xijun</creatorcontrib><creatorcontrib>Wang, Xiaoyan</creatorcontrib><creatorcontrib>Jiang, Na</creatorcontrib><creatorcontrib>He, Qun</creatorcontrib><creatorcontrib>Zhai, Yunhui</creatorcontrib><creatorcontrib>Zhu, Xiangbing</creatorcontrib><creatorcontrib>Hu, Zheng</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Mikrochimica acta (1966)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chang, Xijun</au><au>Wang, Xiaoyan</au><au>Jiang, Na</au><au>He, Qun</au><au>Zhai, Yunhui</au><au>Zhu, Xiangbing</au><au>Hu, Zheng</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Silica gel surface-imprinted solid-phase extraction of Zr(IV) from aqueous solutions</atitle><jtitle>Mikrochimica acta (1966)</jtitle><stitle>Microchim Acta</stitle><date>2008-07-01</date><risdate>2008</risdate><volume>162</volume><issue>1-2</issue><spage>113</spage><epage>119</epage><pages>113-119</pages><issn>0026-3672</issn><eissn>1436-5073</eissn><coden>MIACAQ</coden><abstract>.
A surface imprinted amino-functionalized silica gel material was synthesized by combining a surface molecular imprinting technology for the solid-phase extraction of Zr(IV) in aqueous solutions prior to the measurement by inductively coupled plasma atomic emission spectrometry. The ion-imprinted sorbent had higher selectivity and adsorption capacity for Zr(IV). The maximum static adsorption capacity of the ion-imprinted and non-imprinted sorbent for Zr(IV) was 11 mg g
−1
and 0.3 mg g
−1
, respectively. The relatively selective factor values of Zr(IV)/Ti(IV), Zr(IV)/Y(III) and Zr(IV)/Nb(V) were 32, 34 and 50, which were greater than 1. The distribution ratio values of Zr(IV)-imprinted polymers for Zr(IV) were greatly larger than that for Ti(IV), Y(III) and Nb(V). The detection limit was 0.14 ng mL
−1
. The relative standard deviation of the method was 1.49% for eight replicate determinations. The method was successfully applied to the determination of trace zirconium in some alloys and in tape and waste water samples.</abstract><cop>Vienna</cop><pub>Springer-Verlag</pub><doi>10.1007/s00604-007-0870-4</doi><tpages>7</tpages></addata></record> |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Analysis methods Analytical Chemistry Applied sciences Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Exact sciences and technology Global environmental pollution Microengineering Nanochemistry Nanotechnology Natural water pollution Original Paper Pollution Spectrometric and optical methods Water treatment and pollution |
| title | Silica gel surface-imprinted solid-phase extraction of Zr(IV) from aqueous solutions |
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