Thermal expansion properties of A2(MO4)3(A = Ho and Tm; M = W and Mo)
Compounds Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 have been prepared by conventional solid-state reaction. Their crystal structures and thermal expansion properties were investigated by room temperature and high temperature X-ray diffractions. It is found that, in certain temperature ranges (200...
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| Veröffentlicht in: | Solid state sciences 2008-03, Vol.10 (3), p.321-325 |
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| creator | XIAO, X. L CHENG, Y. Z PENG, J WU, M. M CHEN, D. F HU, Z. B KIYANAGI, R FIERAMOSCA, J. S SHORT, S JORGENSEN, J |
| description | Compounds Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 have been prepared by conventional solid-state reaction. Their crystal structures and thermal expansion properties were investigated by room temperature and high temperature X-ray diffractions. It is found that, in certain temperature ranges (200-700 deg C for Ho sample and 200-800 deg C for the others), Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 all adopt orthorhombic structure and show negative thermal expansion whereas Ho2W3O12 adopts monoclinic structure and shows positive thermal expansion. The volume thermal expansion coefficients obtained for Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 from high temperature XRD are 29.46 X 10-6 deg C-1, -34.50 X 10-6 deg C-1, -11.85 X 10-6 deg C-1 and -12.09 X 10-6 deg C-1, respectively. Thermogravimetry was used to study their hygroscopicity in air. |
| doi_str_mv | 10.1016/j.solidstatesciences.2007.09.001 |
| format | Article |
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L ; CHENG, Y. Z ; PENG, J ; WU, M. M ; CHEN, D. F ; HU, Z. B ; KIYANAGI, R ; FIERAMOSCA, J. S ; SHORT, S ; JORGENSEN, J</creator><creatorcontrib>XIAO, X. L ; CHENG, Y. Z ; PENG, J ; WU, M. M ; CHEN, D. F ; HU, Z. B ; KIYANAGI, R ; FIERAMOSCA, J. S ; SHORT, S ; JORGENSEN, J</creatorcontrib><description>Compounds Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 have been prepared by conventional solid-state reaction. Their crystal structures and thermal expansion properties were investigated by room temperature and high temperature X-ray diffractions. It is found that, in certain temperature ranges (200-700 deg C for Ho sample and 200-800 deg C for the others), Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 all adopt orthorhombic structure and show negative thermal expansion whereas Ho2W3O12 adopts monoclinic structure and shows positive thermal expansion. The volume thermal expansion coefficients obtained for Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 from high temperature XRD are 29.46 X 10-6 deg C-1, -34.50 X 10-6 deg C-1, -11.85 X 10-6 deg C-1 and -12.09 X 10-6 deg C-1, respectively. Thermogravimetry was used to study their hygroscopicity in air.</description><identifier>ISSN: 1293-2558</identifier><identifier>EISSN: 1873-3085</identifier><identifier>DOI: 10.1016/j.solidstatesciences.2007.09.001</identifier><language>eng</language><publisher>Paris: Elsevier</publisher><subject>Condensed matter: structure, mechanical and thermal properties ; Constant-composition solid-solid phase transformations: polymorphic, massive, and order-disorder ; Cross-disciplinary physics: materials science; rheology ; Crystalline state (including molecular motions in solids) ; Crystallographic aspects of phase transformations; pressure effects ; Exact sciences and technology ; Inorganic compounds ; Materials science ; Phase diagrams and microstructures developed by solidification and solid-solid phase transformations ; Physics ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids ; Thermal expansion; thermomechanical effects and density ; Thermal properties of condensed matter ; Thermal properties of crystalline solids</subject><ispartof>Solid state sciences, 2008-03, Vol.10 (3), p.321-325</ispartof><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c251t-58ebde43a0c287b4ba0cb979400416d608227c5a5e05aaf637821ba46256f3453</citedby><cites>FETCH-LOGICAL-c251t-58ebde43a0c287b4ba0cb979400416d608227c5a5e05aaf637821ba46256f3453</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27922,27923</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20259384$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>XIAO, X. 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It is found that, in certain temperature ranges (200-700 deg C for Ho sample and 200-800 deg C for the others), Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 all adopt orthorhombic structure and show negative thermal expansion whereas Ho2W3O12 adopts monoclinic structure and shows positive thermal expansion. The volume thermal expansion coefficients obtained for Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 from high temperature XRD are 29.46 X 10-6 deg C-1, -34.50 X 10-6 deg C-1, -11.85 X 10-6 deg C-1 and -12.09 X 10-6 deg C-1, respectively. Thermogravimetry was used to study their hygroscopicity in air.</description><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Constant-composition solid-solid phase transformations: polymorphic, massive, and order-disorder</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystalline state (including molecular motions in solids)</subject><subject>Crystallographic aspects of phase transformations; pressure effects</subject><subject>Exact sciences and technology</subject><subject>Inorganic compounds</subject><subject>Materials science</subject><subject>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</subject><subject>Physics</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Thermal expansion; thermomechanical effects and density</subject><subject>Thermal properties of condensed matter</subject><subject>Thermal properties of crystalline solids</subject><issn>1293-2558</issn><issn>1873-3085</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNplkEtLw0AUhQdRsFb_w2yUdpF455kJIlhKtUJLNxWXw2QywZS8nElB_72pLW5c3XPgcM7lQ2hCICZA5P0uDm1V5qE3vQu2dI11IaYASQxpDEDO0IiohEUMlDgfNE1ZRIVQl-gqhB0ASJnwEVpsP5yvTYXdV2eaULYN7nzbOd-XLuC2wDM6WW_4lE1m-BEvW2yaHG_rB7we7PuvW7fTa3RRmCq4m9Mdo7fnxXa-jFabl9f5bBVZKkgfCeWy3HFmwFKVZDwbRJYmKQfgROYSFKWJFUY4EMYUkiWKksxwSYUsGBdsjO6OvcOPn3sXel2XwbqqMo1r90EzRpQkCRuCT8eg9W0I3hW682Vt_LcmoA_89E7_56cP_DSkeuA3VNyetkywpiq8aWwZ_nooUJEyxdkPD_10BA</recordid><startdate>200803</startdate><enddate>200803</enddate><creator>XIAO, X. 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S ; SHORT, S ; JORGENSEN, J</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c251t-58ebde43a0c287b4ba0cb979400416d608227c5a5e05aaf637821ba46256f3453</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Constant-composition solid-solid phase transformations: polymorphic, massive, and order-disorder</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Crystalline state (including molecular motions in solids)</topic><topic>Crystallographic aspects of phase transformations; pressure effects</topic><topic>Exact sciences and technology</topic><topic>Inorganic compounds</topic><topic>Materials science</topic><topic>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</topic><topic>Physics</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><topic>Thermal expansion; thermomechanical effects and density</topic><topic>Thermal properties of condensed matter</topic><topic>Thermal properties of crystalline solids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>XIAO, X. L</creatorcontrib><creatorcontrib>CHENG, Y. Z</creatorcontrib><creatorcontrib>PENG, J</creatorcontrib><creatorcontrib>WU, M. M</creatorcontrib><creatorcontrib>CHEN, D. F</creatorcontrib><creatorcontrib>HU, Z. B</creatorcontrib><creatorcontrib>KIYANAGI, R</creatorcontrib><creatorcontrib>FIERAMOSCA, J. S</creatorcontrib><creatorcontrib>SHORT, S</creatorcontrib><creatorcontrib>JORGENSEN, J</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Solid state sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>XIAO, X. L</au><au>CHENG, Y. Z</au><au>PENG, J</au><au>WU, M. M</au><au>CHEN, D. F</au><au>HU, Z. B</au><au>KIYANAGI, R</au><au>FIERAMOSCA, J. S</au><au>SHORT, S</au><au>JORGENSEN, J</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Thermal expansion properties of A2(MO4)3(A = Ho and Tm; M = W and Mo)</atitle><jtitle>Solid state sciences</jtitle><date>2008-03</date><risdate>2008</risdate><volume>10</volume><issue>3</issue><spage>321</spage><epage>325</epage><pages>321-325</pages><issn>1293-2558</issn><eissn>1873-3085</eissn><abstract>Compounds Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 have been prepared by conventional solid-state reaction. Their crystal structures and thermal expansion properties were investigated by room temperature and high temperature X-ray diffractions. It is found that, in certain temperature ranges (200-700 deg C for Ho sample and 200-800 deg C for the others), Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 all adopt orthorhombic structure and show negative thermal expansion whereas Ho2W3O12 adopts monoclinic structure and shows positive thermal expansion. The volume thermal expansion coefficients obtained for Ho2W3O12, Ho2Mo3O12, Tm2W3O12 and Tm2Mo3O12 from high temperature XRD are 29.46 X 10-6 deg C-1, -34.50 X 10-6 deg C-1, -11.85 X 10-6 deg C-1 and -12.09 X 10-6 deg C-1, respectively. Thermogravimetry was used to study their hygroscopicity in air.</abstract><cop>Paris</cop><pub>Elsevier</pub><doi>10.1016/j.solidstatesciences.2007.09.001</doi><tpages>5</tpages></addata></record> |
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| subjects | Condensed matter: structure, mechanical and thermal properties Constant-composition solid-solid phase transformations: polymorphic, massive, and order-disorder Cross-disciplinary physics: materials science rheology Crystalline state (including molecular motions in solids) Crystallographic aspects of phase transformations pressure effects Exact sciences and technology Inorganic compounds Materials science Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics Structure of solids and liquids crystallography Structure of specific crystalline solids Thermal expansion thermomechanical effects and density Thermal properties of condensed matter Thermal properties of crystalline solids |
| title | Thermal expansion properties of A2(MO4)3(A = Ho and Tm; M = W and Mo) |
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