Investigation of anti-corrosion properties of Ti:C gradient layers manufactured in hybrid deposition system
Excellent properties of hard carbon layers and especially, the unique combination of tribological, chemical and physical properties make them a popular coating material for use on surgical prosthesis, biomedical implants, and machine tools. However, their well-known poor adhesion and high internal s...
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| Veröffentlicht in: | Journal of materials science 2008-05, Vol.43 (10), p.3385-3391 |
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| description | Excellent properties of hard carbon layers and especially, the unique combination of tribological, chemical and physical properties make them a popular coating material for use on surgical prosthesis, biomedical implants, and machine tools. However, their well-known poor adhesion and high internal stress disqualifies them in many possibilities of industrial applications. These drawbacks were improved by deposition of Ti buffer layer. By a combination of Radio Frequency Plasma Assisted Chemical Vapor Deposition (RFPACVD) and DC magnetron sputtering methods, thick carbon films were manufactured on Rex 734 steel. Structure and chemical composition of deposited layers was determined by scanning electron microscope and energy dispersive spectrometer analysis. The main purpose of this work was to determine the corrosion properties of Rex 734 alloy in a typical 0.5 M NaCl solution and to find the influence of Ti:C gradient layers on these properties. Anti-corrosion behavior was measured by the detection of corrosion potential in open circuit and the registration of potentiodynamic characteristics according to Stern–Geary and Tafel methods. Five different types of samples were studied: for full analysis the investigation was conducted for every structural component of the layer: for pure Ti deposited on Rex 734 as well as for Ti containing carbon layer and carbon layer deposited subsequently, and finally the corrosion resistance of Rex 734 steel was measured for comparison. As a result of the investigation it was noticed that the Ti–C interlayer enables to maximize the thickness of DLC films and Ti:C gradient layers have the good influence on the corrosion features of Rex 734 alloy. |
| doi_str_mv | 10.1007/s10853-007-2393-0 |
| format | Article |
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However, their well-known poor adhesion and high internal stress disqualifies them in many possibilities of industrial applications. These drawbacks were improved by deposition of Ti buffer layer. By a combination of Radio Frequency Plasma Assisted Chemical Vapor Deposition (RFPACVD) and DC magnetron sputtering methods, thick carbon films were manufactured on Rex 734 steel. Structure and chemical composition of deposited layers was determined by scanning electron microscope and energy dispersive spectrometer analysis. The main purpose of this work was to determine the corrosion properties of Rex 734 alloy in a typical 0.5 M NaCl solution and to find the influence of Ti:C gradient layers on these properties. Anti-corrosion behavior was measured by the detection of corrosion potential in open circuit and the registration of potentiodynamic characteristics according to Stern–Geary and Tafel methods. Five different types of samples were studied: for full analysis the investigation was conducted for every structural component of the layer: for pure Ti deposited on Rex 734 as well as for Ti containing carbon layer and carbon layer deposited subsequently, and finally the corrosion resistance of Rex 734 steel was measured for comparison. As a result of the investigation it was noticed that the Ti–C interlayer enables to maximize the thickness of DLC films and Ti:C gradient layers have the good influence on the corrosion features of Rex 734 alloy.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-007-2393-0</identifier><identifier>CODEN: JMTSAS</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Applied sciences ; Biomedical materials ; Buffer layers ; Carbon ; Characterization and Evaluation of Materials ; Chemical composition ; Chemical vapor deposition ; Circuits ; Classical Mechanics ; Coatings and Nanostructured Materials ; Corrosion ; Corrosion environments ; Corrosion potential ; Corrosion prevention ; Corrosion resistance ; Corrosion resistant alloys ; Corrosion resistant steels ; Cross-disciplinary physics: materials science; rheology ; Crystallography and Scattering Methods ; Deposition ; Diamond-like carbon films ; Exact sciences and technology ; Hybrid systems ; Industrial applications ; Interlayers ; Machine tools ; Magnetron sputtering ; Materials Science ; Metals. Metallurgy ; NanoSmat 2007 - International Conference on Surfaces ; Organic chemistry ; Other topics in materials science ; Physical properties ; Physics ; Polymer Sciences ; Protective coatings ; Radio frequency plasma ; Residual stress ; Scanning electron microscopy ; Solid Mechanics ; Steel structures ; Structural steels ; Surgical implants ; Thick films ; Thickness ; Titanium base alloys ; Tribology</subject><ispartof>Journal of materials science, 2008-05, Vol.43 (10), p.3385-3391</ispartof><rights>Springer Science+Business Media, LLC 2008</rights><rights>2008 INIST-CNRS</rights><rights>Journal of Materials Science is a copyright of Springer, (2008). 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However, their well-known poor adhesion and high internal stress disqualifies them in many possibilities of industrial applications. These drawbacks were improved by deposition of Ti buffer layer. By a combination of Radio Frequency Plasma Assisted Chemical Vapor Deposition (RFPACVD) and DC magnetron sputtering methods, thick carbon films were manufactured on Rex 734 steel. Structure and chemical composition of deposited layers was determined by scanning electron microscope and energy dispersive spectrometer analysis. The main purpose of this work was to determine the corrosion properties of Rex 734 alloy in a typical 0.5 M NaCl solution and to find the influence of Ti:C gradient layers on these properties. Anti-corrosion behavior was measured by the detection of corrosion potential in open circuit and the registration of potentiodynamic characteristics according to Stern–Geary and Tafel methods. Five different types of samples were studied: for full analysis the investigation was conducted for every structural component of the layer: for pure Ti deposited on Rex 734 as well as for Ti containing carbon layer and carbon layer deposited subsequently, and finally the corrosion resistance of Rex 734 steel was measured for comparison. As a result of the investigation it was noticed that the Ti–C interlayer enables to maximize the thickness of DLC films and Ti:C gradient layers have the good influence on the corrosion features of Rex 734 alloy.</description><subject>Applied sciences</subject><subject>Biomedical materials</subject><subject>Buffer layers</subject><subject>Carbon</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical composition</subject><subject>Chemical vapor deposition</subject><subject>Circuits</subject><subject>Classical Mechanics</subject><subject>Coatings and Nanostructured Materials</subject><subject>Corrosion</subject><subject>Corrosion environments</subject><subject>Corrosion potential</subject><subject>Corrosion prevention</subject><subject>Corrosion resistance</subject><subject>Corrosion resistant alloys</subject><subject>Corrosion resistant steels</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystallography and Scattering Methods</subject><subject>Deposition</subject><subject>Diamond-like carbon films</subject><subject>Exact sciences and technology</subject><subject>Hybrid systems</subject><subject>Industrial applications</subject><subject>Interlayers</subject><subject>Machine tools</subject><subject>Magnetron sputtering</subject><subject>Materials Science</subject><subject>Metals. Metallurgy</subject><subject>NanoSmat 2007 - International Conference on Surfaces</subject><subject>Organic chemistry</subject><subject>Other topics in materials science</subject><subject>Physical properties</subject><subject>Physics</subject><subject>Polymer Sciences</subject><subject>Protective coatings</subject><subject>Radio frequency plasma</subject><subject>Residual stress</subject><subject>Scanning electron microscopy</subject><subject>Solid Mechanics</subject><subject>Steel structures</subject><subject>Structural steels</subject><subject>Surgical implants</subject><subject>Thick films</subject><subject>Thickness</subject><subject>Titanium base alloys</subject><subject>Tribology</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kU1LxDAQhoMouK7-AG8FUbxUJ19N600Wv0DwoucymyZrtJuuSSvsvzd1RUHQU14y7zy8M0PIIYUzCqDOI4VS8jzJnPEqiS0yoVLxXJTAt8kEgLGciYLukr0YXwBAKkYn5PXOv5vYuwX2rvNZZzP0vct1F0IXx59V6FYm9M7EsfjoLmbZImDjjO-zFtcmxGyJfrCo-yGYJnM-e17Pg2uyxqwS4hMb17E3y32yY7GN5uDrnZKn66vH2W1-_3BzN7u8z7Wg0OeYJsGCIxOW2kaWqpJWzFmjSyULBrxgdl5yXileSosCFQjTVA2g5oaCAT4lJxtuyv42pOnqpYvatC160w2x5hxUlUDJePqvMe2U0UqqtMcpOfplfemG4NMYNWOyKoQUTCYX3bh02l4Mxtar4JYY1glVj3eqN3eqRzneqR7THn-RMWpsbUCvXfxuTDlZWdIxLNv4Yir5hQk_Cf6GfwDSNaKQ</recordid><startdate>20080501</startdate><enddate>20080501</enddate><creator>Batory, D.</creator><creator>Blaszczyk, T.</creator><creator>Clapa, M.</creator><creator>Mitura, S.</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>7SE</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20080501</creationdate><title>Investigation of anti-corrosion properties of Ti:C gradient layers manufactured in hybrid deposition system</title><author>Batory, D. ; Blaszczyk, T. ; Clapa, M. ; Mitura, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c410t-a085a63a24f1fd58795f4b2dc875620362fb83397385fa4a704ed9d0ac3e10e03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Applied sciences</topic><topic>Biomedical materials</topic><topic>Buffer layers</topic><topic>Carbon</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical composition</topic><topic>Chemical vapor deposition</topic><topic>Circuits</topic><topic>Classical Mechanics</topic><topic>Coatings and Nanostructured Materials</topic><topic>Corrosion</topic><topic>Corrosion environments</topic><topic>Corrosion potential</topic><topic>Corrosion prevention</topic><topic>Corrosion resistance</topic><topic>Corrosion resistant alloys</topic><topic>Corrosion resistant steels</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Crystallography and Scattering Methods</topic><topic>Deposition</topic><topic>Diamond-like carbon films</topic><topic>Exact sciences and technology</topic><topic>Hybrid systems</topic><topic>Industrial applications</topic><topic>Interlayers</topic><topic>Machine tools</topic><topic>Magnetron sputtering</topic><topic>Materials Science</topic><topic>Metals. Metallurgy</topic><topic>NanoSmat 2007 - International Conference on Surfaces</topic><topic>Organic chemistry</topic><topic>Other topics in materials science</topic><topic>Physical properties</topic><topic>Physics</topic><topic>Polymer Sciences</topic><topic>Protective coatings</topic><topic>Radio frequency plasma</topic><topic>Residual stress</topic><topic>Scanning electron microscopy</topic><topic>Solid Mechanics</topic><topic>Steel structures</topic><topic>Structural steels</topic><topic>Surgical implants</topic><topic>Thick films</topic><topic>Thickness</topic><topic>Titanium base alloys</topic><topic>Tribology</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Batory, D.</creatorcontrib><creatorcontrib>Blaszczyk, T.</creatorcontrib><creatorcontrib>Clapa, M.</creatorcontrib><creatorcontrib>Mitura, S.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection (ProQuest)</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Batory, D.</au><au>Blaszczyk, T.</au><au>Clapa, M.</au><au>Mitura, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigation of anti-corrosion properties of Ti:C gradient layers manufactured in hybrid deposition system</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2008-05-01</date><risdate>2008</risdate><volume>43</volume><issue>10</issue><spage>3385</spage><epage>3391</epage><pages>3385-3391</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><coden>JMTSAS</coden><abstract>Excellent properties of hard carbon layers and especially, the unique combination of tribological, chemical and physical properties make them a popular coating material for use on surgical prosthesis, biomedical implants, and machine tools. However, their well-known poor adhesion and high internal stress disqualifies them in many possibilities of industrial applications. These drawbacks were improved by deposition of Ti buffer layer. By a combination of Radio Frequency Plasma Assisted Chemical Vapor Deposition (RFPACVD) and DC magnetron sputtering methods, thick carbon films were manufactured on Rex 734 steel. Structure and chemical composition of deposited layers was determined by scanning electron microscope and energy dispersive spectrometer analysis. The main purpose of this work was to determine the corrosion properties of Rex 734 alloy in a typical 0.5 M NaCl solution and to find the influence of Ti:C gradient layers on these properties. Anti-corrosion behavior was measured by the detection of corrosion potential in open circuit and the registration of potentiodynamic characteristics according to Stern–Geary and Tafel methods. Five different types of samples were studied: for full analysis the investigation was conducted for every structural component of the layer: for pure Ti deposited on Rex 734 as well as for Ti containing carbon layer and carbon layer deposited subsequently, and finally the corrosion resistance of Rex 734 steel was measured for comparison. As a result of the investigation it was noticed that the Ti–C interlayer enables to maximize the thickness of DLC films and Ti:C gradient layers have the good influence on the corrosion features of Rex 734 alloy.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-007-2393-0</doi><tpages>7</tpages></addata></record> |
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| subjects | Applied sciences Biomedical materials Buffer layers Carbon Characterization and Evaluation of Materials Chemical composition Chemical vapor deposition Circuits Classical Mechanics Coatings and Nanostructured Materials Corrosion Corrosion environments Corrosion potential Corrosion prevention Corrosion resistance Corrosion resistant alloys Corrosion resistant steels Cross-disciplinary physics: materials science rheology Crystallography and Scattering Methods Deposition Diamond-like carbon films Exact sciences and technology Hybrid systems Industrial applications Interlayers Machine tools Magnetron sputtering Materials Science Metals. Metallurgy NanoSmat 2007 - International Conference on Surfaces Organic chemistry Other topics in materials science Physical properties Physics Polymer Sciences Protective coatings Radio frequency plasma Residual stress Scanning electron microscopy Solid Mechanics Steel structures Structural steels Surgical implants Thick films Thickness Titanium base alloys Tribology |
| title | Investigation of anti-corrosion properties of Ti:C gradient layers manufactured in hybrid deposition system |
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