Effect of Calcination on Crystallinity for Nanostructured Development of Wormhole-Like Mesoporous Tungsten Oxide

The effects of calcination on the crystallinity and grain growth model for microstructure development of wormhole‐like mesoporous tungsten oxide are investigated in this study. We found that residual mesopores of wormhole‐like tungsten oxide can be seen calcined above 500°C, as evidenced by retentio...

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Veröffentlicht in:Journal of the American Ceramic Society 2007-12, Vol.90 (12), p.4073-4075
Hauptverfasser: Lai, Wei Hao, Teoh, Lay Gaik, Su, Yen Hsun, Shieh, Jiann, Hon, Min Hsiung
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container_end_page 4075
container_issue 12
container_start_page 4073
container_title Journal of the American Ceramic Society
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creator Lai, Wei Hao
Teoh, Lay Gaik
Su, Yen Hsun
Shieh, Jiann
Hon, Min Hsiung
description The effects of calcination on the crystallinity and grain growth model for microstructure development of wormhole‐like mesoporous tungsten oxide are investigated in this study. We found that residual mesopores of wormhole‐like tungsten oxide can be seen calcined above 500°C, as evidenced by retention of a wormhole‐like mesostructure of tungsten oxide. A model was proposed to combine grain growth with wormhole‐like mesoporous behavior and to investigate whether the formation of wormhole‐like mesoporous tungsten oxide can retard the collapse rate of mesopores during the calcination process.
doi_str_mv 10.1111/j.1551-2916.2007.02078.x
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subjects Chemical synthesis methods
Cross-disciplinary physics: materials science
rheology
Crystal structure
Exact sciences and technology
Materials science
Metals
Methods of nanofabrication
Microstructure
Nanostructured ceramics
Oxidation
Physics
title Effect of Calcination on Crystallinity for Nanostructured Development of Wormhole-Like Mesoporous Tungsten Oxide
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