Piezoelectric signal suppression by a composite-pulse sequence in NMR
Numerous NMR techniques are available for the study of nuclei with spin I > =1. These nuclei interact with their surrounding electric field gradient, which depends on the symmetry of the crystallographic site. Spurious (or piezoelectric) signals, due to the piezoelectric and ferroelectric propert...
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| Veröffentlicht in: | Comptes rendus. Chimie 2004-03, Vol.7 (3-4), p.425-430 |
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| creator | MIGNON, Claude MILLOT, Yannick MAN, Pascal P |
| description | Numerous NMR techniques are available for the study of nuclei with spin I > =1. These nuclei interact with their surrounding electric field gradient, which depends on the symmetry of the crystallographic site. Spurious (or piezoelectric) signals, due to the piezoelectric and ferroelectric properties of a LiNbO3 crystal and generated by the vibration of the macroscopic electric dipole of the crystal, have been observed with the one-pulse sequence and cancelled using a composite-pulse sequence. The suppression of these piezoelectric signals by this sequence is illustrated by lithium-7 (I=3/2) nuclei. Java applets available in our web site www.pascal-man.com for the determination of quadrupole parameters from one-dimensional nutation method are also presented. |
| doi_str_mv | 10.1016/j.crci.2003.12.013 |
| format | Article |
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| source | Elsevier ScienceDirect Journals Complete; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals |
| subjects | Condensed matter: electronic structure, electrical, magnetic, and optical properties Exact sciences and technology Infrared, submillimeter wave, microwave and radiowave instruments, equipment and techniques Instruments, apparatus, components and techniques common to several branches of physics and astronomy Magnetic resonances and relaxations in condensed matter, mössbauer effect Nuclear magnetic resonance and relaxation Physics Submillimeter wave, microwave and radiowave spectrometers magnetic resonance spectrometers, auxiliary equipment, and techniques Submillimeter wave, microwave and radiowave spectrometers magnetic resonance spectrometers, auxiliary equipments and techniques |
| title | Piezoelectric signal suppression by a composite-pulse sequence in NMR |
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