Molten salt synthesis of lead lanthanum zirconate titanate ceramic powders
Lead lanthanum zirconate titanate (Pb 0.95La 0.03)(Zr 0.52Ti 0.48)O 3 (PLZT) was synthesized by one step molten salt method with the starting materials of PbC 2O 4, La 2O 3, ZrO(NO 3) 2·2H 2O and TiO 2 in the NaCl–KCl eutectic mixtures in the temperature range of 700–1000 °C. The single phase of (Pb...
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| Veröffentlicht in: | Journal of alloys and compounds 2008-04, Vol.454 (1), p.466-470 |
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| container_title | Journal of alloys and compounds |
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| creator | Cai, Zongying Xing, Xianran Li, Lu Xu, Yeming |
| description | Lead lanthanum zirconate titanate (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 (PLZT) was synthesized by one step molten salt method with the starting materials of PbC
2O
4, La
2O
3, ZrO(NO
3)
2·2H
2O and TiO
2 in the NaCl–KCl eutectic mixtures in the temperature range of 700–1000
°C. The single phase of (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 powders was prepared at a temperature as low as 850
°C for 5
h. The effects of process parameters, such as soaking temperature and time, salt species, and the amount of flux with respect to the starting materials were investigated. The growth process of the PLZT particles in the molten salt undergoes a transition from a diffusion controlled mechanism to an interfacial reaction controlled mechanism at 900
°C. |
| doi_str_mv | 10.1016/j.jallcom.2006.12.128 |
| format | Article |
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0.95La
0.03)(Zr
0.52Ti
0.48)O
3 (PLZT) was synthesized by one step molten salt method with the starting materials of PbC
2O
4, La
2O
3, ZrO(NO
3)
2·2H
2O and TiO
2 in the NaCl–KCl eutectic mixtures in the temperature range of 700–1000
°C. The single phase of (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 powders was prepared at a temperature as low as 850
°C for 5
h. The effects of process parameters, such as soaking temperature and time, salt species, and the amount of flux with respect to the starting materials were investigated. The growth process of the PLZT particles in the molten salt undergoes a transition from a diffusion controlled mechanism to an interfacial reaction controlled mechanism at 900
°C.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2006.12.128</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>(Pb 0.95La 0.03)(Zr 0.52Ti 0.48)O 3 (PLZT) ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Growth process ; Materials science ; Materials synthesis; materials processing ; Molten salt synthesis (MSS) ; Physics</subject><ispartof>Journal of alloys and compounds, 2008-04, Vol.454 (1), p.466-470</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c370t-9a86d42fdb1a44b5c7297cc8bd4b6ea92959a613252573e9aeeca583483567953</citedby><cites>FETCH-LOGICAL-c370t-9a86d42fdb1a44b5c7297cc8bd4b6ea92959a613252573e9aeeca583483567953</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0925838807000217$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20232121$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Cai, Zongying</creatorcontrib><creatorcontrib>Xing, Xianran</creatorcontrib><creatorcontrib>Li, Lu</creatorcontrib><creatorcontrib>Xu, Yeming</creatorcontrib><title>Molten salt synthesis of lead lanthanum zirconate titanate ceramic powders</title><title>Journal of alloys and compounds</title><description>Lead lanthanum zirconate titanate (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 (PLZT) was synthesized by one step molten salt method with the starting materials of PbC
2O
4, La
2O
3, ZrO(NO
3)
2·2H
2O and TiO
2 in the NaCl–KCl eutectic mixtures in the temperature range of 700–1000
°C. The single phase of (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 powders was prepared at a temperature as low as 850
°C for 5
h. The effects of process parameters, such as soaking temperature and time, salt species, and the amount of flux with respect to the starting materials were investigated. The growth process of the PLZT particles in the molten salt undergoes a transition from a diffusion controlled mechanism to an interfacial reaction controlled mechanism at 900
°C.</description><subject>(Pb 0.95La 0.03)(Zr 0.52Ti 0.48)O 3 (PLZT)</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Growth process</subject><subject>Materials science</subject><subject>Materials synthesis; materials processing</subject><subject>Molten salt synthesis (MSS)</subject><subject>Physics</subject><issn>0925-8388</issn><issn>1873-4669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNqFUE1LJDEQDbKCs-pPEPqye-sxH510cpJlcP1A8aLnUJOuxgzpzmySUcZfvz3O4FV4UEXxXr2qR8gFo3NGmbpczVcQgovDnFOq5oxP0EdkxnQr6kYp84PMqOGy1kLrE_Iz5xWllBnBZuT-MYaCY5UhlCpvx_KK2ecq9lVA6KoA0wTGzVB9-OTiCAWr4gt8Ng4TDN5V6_jeYcpn5LiHkPH8UE_Jy9_r58Vt_fB0c7f481A70dJSG9Cqa3jfLRk0zVK6lpvWOb3smqVCMNxIA4oJLrlsBRpAdCC1aLSQqjVSnJLf-73rFP9tMBc7-OwwTLdi3GQreCMMVzui3BNdijkn7O06-QHS1jJqd8nZlT0kZ3fJWcYn6En362AA2UHoE4zO5y8xp1xwxtnEu9rzcPr2zWOy2XkcHXY-oSu2i_4bp__orYdJ</recordid><startdate>20080424</startdate><enddate>20080424</enddate><creator>Cai, Zongying</creator><creator>Xing, Xianran</creator><creator>Li, Lu</creator><creator>Xu, Yeming</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20080424</creationdate><title>Molten salt synthesis of lead lanthanum zirconate titanate ceramic powders</title><author>Cai, Zongying ; Xing, Xianran ; Li, Lu ; Xu, Yeming</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c370t-9a86d42fdb1a44b5c7297cc8bd4b6ea92959a613252573e9aeeca583483567953</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>(Pb 0.95La 0.03)(Zr 0.52Ti 0.48)O 3 (PLZT)</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Growth process</topic><topic>Materials science</topic><topic>Materials synthesis; materials processing</topic><topic>Molten salt synthesis (MSS)</topic><topic>Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cai, Zongying</creatorcontrib><creatorcontrib>Xing, Xianran</creatorcontrib><creatorcontrib>Li, Lu</creatorcontrib><creatorcontrib>Xu, Yeming</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cai, Zongying</au><au>Xing, Xianran</au><au>Li, Lu</au><au>Xu, Yeming</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Molten salt synthesis of lead lanthanum zirconate titanate ceramic powders</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2008-04-24</date><risdate>2008</risdate><volume>454</volume><issue>1</issue><spage>466</spage><epage>470</epage><pages>466-470</pages><issn>0925-8388</issn><eissn>1873-4669</eissn><abstract>Lead lanthanum zirconate titanate (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 (PLZT) was synthesized by one step molten salt method with the starting materials of PbC
2O
4, La
2O
3, ZrO(NO
3)
2·2H
2O and TiO
2 in the NaCl–KCl eutectic mixtures in the temperature range of 700–1000
°C. The single phase of (Pb
0.95La
0.03)(Zr
0.52Ti
0.48)O
3 powders was prepared at a temperature as low as 850
°C for 5
h. The effects of process parameters, such as soaking temperature and time, salt species, and the amount of flux with respect to the starting materials were investigated. The growth process of the PLZT particles in the molten salt undergoes a transition from a diffusion controlled mechanism to an interfacial reaction controlled mechanism at 900
°C.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2006.12.128</doi><tpages>5</tpages></addata></record> |
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| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | (Pb 0.95La 0.03)(Zr 0.52Ti 0.48)O 3 (PLZT) Cross-disciplinary physics: materials science rheology Exact sciences and technology Growth process Materials science Materials synthesis materials processing Molten salt synthesis (MSS) Physics |
| title | Molten salt synthesis of lead lanthanum zirconate titanate ceramic powders |
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