Hydrothermal synthesis, crystal structure, thermal behaviour, IR and Raman spectroscopy of Na3Y(CO3)3.6 H2O
A new sodium yttrium carbonate hydrate, Na3Y(CO3)36 H2O, is prepared by hydrothermal synthesis and characterized by single crystal X-ray diffraction, thermal analysis, IR and Raman spectroscopy. Na3Y(CO3)36 H2O crystallizes in the hexagonal system, space group P63; a=11.347(5) A, c=5.935(5) A; V=661...
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| Veröffentlicht in: | Comptes rendus. Chimie 2004-06, Vol.7 (6-7), p.661-668 |
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| container_issue | 6-7 |
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| container_title | Comptes rendus. Chimie |
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| creator | AMOR BEN ALI MOHAMED OSMAN AWALEH LEBLANC, Marc SMIRI, Leila Samia MAISONNEUVE, Vincent HOULBERT, Sylvie |
| description | A new sodium yttrium carbonate hydrate, Na3Y(CO3)36 H2O, is prepared by hydrothermal synthesis and characterized by single crystal X-ray diffraction, thermal analysis, IR and Raman spectroscopy. Na3Y(CO3)36 H2O crystallizes in the hexagonal system, space group P63; a=11.347(5) A, c=5.935(5) A; V=661.8(5) A3; Z=2. Refinements yield R(F2)=0.058and Rw(F2)=0.161for 692unique reflections. The structure is built up from [YO3+3+3] polyhedra surrounded by [NaO6] octahedra. Carbonate groups form infinite layers at z approx 0.175and z approx 0.675. Dehydration of Na3Y(CO3)36 H2O yields an amorphous carbonate. |
| doi_str_mv | 10.1016/j.crci.2004.03.007 |
| format | Article |
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Na3Y(CO3)36 H2O crystallizes in the hexagonal system, space group P63; a=11.347(5) A, c=5.935(5) A; V=661.8(5) A3; Z=2. Refinements yield R(F2)=0.058and Rw(F2)=0.161for 692unique reflections. The structure is built up from [YO3+3+3] polyhedra surrounded by [NaO6] octahedra. Carbonate groups form infinite layers at z approx 0.175and z approx 0.675. Dehydration of Na3Y(CO3)36 H2O yields an amorphous carbonate.</description><identifier>ISSN: 1631-0748</identifier><identifier>EISSN: 1878-1543</identifier><identifier>DOI: 10.1016/j.crci.2004.03.007</identifier><language>eng</language><publisher>Paris: Elsevier</publisher><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Exact sciences and technology ; Infrared and raman spectra and scattering ; Inorganic compounds ; Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ; Other nonmetallic inorganics ; Physics ; Salts ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids</subject><ispartof>Comptes rendus. 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Chimie</title><description>A new sodium yttrium carbonate hydrate, Na3Y(CO3)36 H2O, is prepared by hydrothermal synthesis and characterized by single crystal X-ray diffraction, thermal analysis, IR and Raman spectroscopy. Na3Y(CO3)36 H2O crystallizes in the hexagonal system, space group P63; a=11.347(5) A, c=5.935(5) A; V=661.8(5) A3; Z=2. Refinements yield R(F2)=0.058and Rw(F2)=0.161for 692unique reflections. The structure is built up from [YO3+3+3] polyhedra surrounded by [NaO6] octahedra. Carbonate groups form infinite layers at z approx 0.175and z approx 0.675. Dehydration of Na3Y(CO3)36 H2O yields an amorphous carbonate.</description><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Exact sciences and technology</subject><subject>Infrared and raman spectra and scattering</subject><subject>Inorganic compounds</subject><subject>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</subject><subject>Other nonmetallic inorganics</subject><subject>Physics</subject><subject>Salts</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><issn>1631-0748</issn><issn>1878-1543</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2004</creationdate><recordtype>article</recordtype><recordid>eNpFkEtLw0AUhYMoWKt_wNVsFIUm3nnlsZSitlAsFF24GiYzE5qalzOJkH_vhCqu7uFyzuHwBcE1hggDjh8OkbKqjAgAi4BGAMlJMMNpkoaYM3rqdUxxCAlLz4ML5w7gQxmPZ8HnatS27ffG1rJCbmy8dKVbIGVH10-v3g6qH6xZoD9Xbvbyu2wHu0DrHZKNRjtZywa5zqjetk613YjaAr1K-nG33NJ7GsVoRbaXwVkhK2eufu88eH9-eluuws32Zb183IQKc78S5wnGKeSMUpZoTVTKleJ5kuSE4ExJrQsgNNaMG8hjnjCmqYQ40wp0wbWk8-D22NvZ9mswrhd16ZSpKtmYdnCCEppSzrA3kqNR-dXOmkJ0tqylHQUGMXEVBzFxFRNXAVR4rj5089sunZJVYWWjSvef5JlHDkB_AGfheO0</recordid><startdate>20040601</startdate><enddate>20040601</enddate><creator>AMOR BEN ALI</creator><creator>MOHAMED OSMAN AWALEH</creator><creator>LEBLANC, Marc</creator><creator>SMIRI, Leila Samia</creator><creator>MAISONNEUVE, Vincent</creator><creator>HOULBERT, Sylvie</creator><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20040601</creationdate><title>Hydrothermal synthesis, crystal structure, thermal behaviour, IR and Raman spectroscopy of Na3Y(CO3)3.6 H2O</title><author>AMOR BEN ALI ; MOHAMED OSMAN AWALEH ; LEBLANC, Marc ; SMIRI, Leila Samia ; MAISONNEUVE, Vincent ; HOULBERT, Sylvie</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1531-1b71180b43347dd2c85cc5b77b2219caddf0236d45e0b65744d3a069dc0df5da3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2004</creationdate><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Exact sciences and technology</topic><topic>Infrared and raman spectra and scattering</topic><topic>Inorganic compounds</topic><topic>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</topic><topic>Other nonmetallic inorganics</topic><topic>Physics</topic><topic>Salts</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>AMOR BEN ALI</creatorcontrib><creatorcontrib>MOHAMED OSMAN AWALEH</creatorcontrib><creatorcontrib>LEBLANC, Marc</creatorcontrib><creatorcontrib>SMIRI, Leila Samia</creatorcontrib><creatorcontrib>MAISONNEUVE, Vincent</creatorcontrib><creatorcontrib>HOULBERT, Sylvie</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Comptes rendus. Chimie</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>AMOR BEN ALI</au><au>MOHAMED OSMAN AWALEH</au><au>LEBLANC, Marc</au><au>SMIRI, Leila Samia</au><au>MAISONNEUVE, Vincent</au><au>HOULBERT, Sylvie</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hydrothermal synthesis, crystal structure, thermal behaviour, IR and Raman spectroscopy of Na3Y(CO3)3.6 H2O</atitle><jtitle>Comptes rendus. Chimie</jtitle><date>2004-06-01</date><risdate>2004</risdate><volume>7</volume><issue>6-7</issue><spage>661</spage><epage>668</epage><pages>661-668</pages><issn>1631-0748</issn><eissn>1878-1543</eissn><abstract>A new sodium yttrium carbonate hydrate, Na3Y(CO3)36 H2O, is prepared by hydrothermal synthesis and characterized by single crystal X-ray diffraction, thermal analysis, IR and Raman spectroscopy. Na3Y(CO3)36 H2O crystallizes in the hexagonal system, space group P63; a=11.347(5) A, c=5.935(5) A; V=661.8(5) A3; Z=2. Refinements yield R(F2)=0.058and Rw(F2)=0.161for 692unique reflections. The structure is built up from [YO3+3+3] polyhedra surrounded by [NaO6] octahedra. Carbonate groups form infinite layers at z approx 0.175and z approx 0.675. Dehydration of Na3Y(CO3)36 H2O yields an amorphous carbonate.</abstract><cop>Paris</cop><pub>Elsevier</pub><doi>10.1016/j.crci.2004.03.007</doi><tpages>8</tpages></addata></record> |
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| subjects | Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Infrared and raman spectra and scattering Inorganic compounds Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Other nonmetallic inorganics Physics Salts Structure of solids and liquids crystallography Structure of specific crystalline solids |
| title | Hydrothermal synthesis, crystal structure, thermal behaviour, IR and Raman spectroscopy of Na3Y(CO3)3.6 H2O |
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