Investigations on TiO2–NiO@In2O3 nanocomposite thin films (NCTFs) for gas sensing: synthesis, physical characterization, and detection of NO2 and H2S gas sensors
The spray pyrolysis technique is a versatile and cost-effective method for producing TiO 2 –NiO@In 2 O 3 NCTFs on glass substrates with varying molar ratios. NCTFs have been studied for gas sensing applications due to their excellent sensing properties. The films' structural, morphological, and...
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| Veröffentlicht in: | Journal of materials science 2024-02, Vol.59 (8), p.3451-3466 |
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| creator | Alborisha, Mohamed Abed Shahoodh Ibrahim, Foued Tarek Jilani, Wissal Bouzidi, Abdelfatteh Guermazi, Samir |
| description | The spray pyrolysis technique is a versatile and cost-effective method for producing TiO
2
–NiO@In
2
O
3
NCTFs on glass substrates with varying molar ratios. NCTFs have been studied for gas sensing applications due to their excellent sensing properties. The films' structural, morphological, and gas sensing characteristics were analyzed. The XRD analysis indicates that the NCTFs are polycrystalline, meaning that they are made up of many small crystals. The crystals are oriented in a random fashion, which is why the XRD pattern is broad. The anatase phase of TiO
2
is a tetragonal crystal structure. The NiO and In
2
O
3
phases are both cubic crystal structures. The presence of nanostructure cubic phases indicates that the nanoparticles in the films are small enough to significantly affect the crystal structure of the films. Scanning electron microscopy images showed surface homogeneity, with small granular grains of nanostructures without any cracks. The gas sensor created using the prepared samples showed high sensitivity to NO
2
and H
2
S gases, and its sensitivity was measured at different operation temperatures, along with response and recovery times. The optical properties of In
2
O
3
are affected by the addition of TiO
2
and NiO impurities. The transmittance of In
2
O
3
increases as the NiO ratio increases and the TiO
2
ratio decreases. |
| doi_str_mv | 10.1007/s10853-024-09376-z |
| format | Article |
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2
–NiO@In
2
O
3
NCTFs on glass substrates with varying molar ratios. NCTFs have been studied for gas sensing applications due to their excellent sensing properties. The films' structural, morphological, and gas sensing characteristics were analyzed. The XRD analysis indicates that the NCTFs are polycrystalline, meaning that they are made up of many small crystals. The crystals are oriented in a random fashion, which is why the XRD pattern is broad. The anatase phase of TiO
2
is a tetragonal crystal structure. The NiO and In
2
O
3
phases are both cubic crystal structures. The presence of nanostructure cubic phases indicates that the nanoparticles in the films are small enough to significantly affect the crystal structure of the films. Scanning electron microscopy images showed surface homogeneity, with small granular grains of nanostructures without any cracks. The gas sensor created using the prepared samples showed high sensitivity to NO
2
and H
2
S gases, and its sensitivity was measured at different operation temperatures, along with response and recovery times. The optical properties of In
2
O
3
are affected by the addition of TiO
2
and NiO impurities. The transmittance of In
2
O
3
increases as the NiO ratio increases and the TiO
2
ratio decreases.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-024-09376-z</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Anatase ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Classical Mechanics ; Composites & Nanocomposites ; cost effectiveness ; Crystal structure ; Crystallography and Scattering Methods ; electron microscopy ; Gas sensors ; Gases ; glass ; Glass substrates ; Homogeneity ; Indium oxides ; Materials Science ; Nanocomposites ; nanoparticles ; Nanostructure ; nickel oxide ; Nickel oxides ; Nitrogen dioxide ; Optical properties ; physical properties ; Polymer Sciences ; Production methods ; pyrolysis ; Sensitivity ; Solid Mechanics ; Spray pyrolysis ; Thin films ; Titanium dioxide ; transmittance ; X-ray diffraction</subject><ispartof>Journal of materials science, 2024-02, Vol.59 (8), p.3451-3466</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c303t-5dc0756ca0fcfea7bed2c0a435e362270a2a079a474a4991cf107bf35748c8a83</cites><orcidid>0000-0002-6166-1107</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10853-024-09376-z$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10853-024-09376-z$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Alborisha, Mohamed Abed Shahoodh</creatorcontrib><creatorcontrib>Ibrahim, Foued Tarek</creatorcontrib><creatorcontrib>Jilani, Wissal</creatorcontrib><creatorcontrib>Bouzidi, Abdelfatteh</creatorcontrib><creatorcontrib>Guermazi, Samir</creatorcontrib><title>Investigations on TiO2–NiO@In2O3 nanocomposite thin films (NCTFs) for gas sensing: synthesis, physical characterization, and detection of NO2 and H2S gas sensors</title><title>Journal of materials science</title><addtitle>J Mater Sci</addtitle><description>The spray pyrolysis technique is a versatile and cost-effective method for producing TiO
2
–NiO@In
2
O
3
NCTFs on glass substrates with varying molar ratios. NCTFs have been studied for gas sensing applications due to their excellent sensing properties. The films' structural, morphological, and gas sensing characteristics were analyzed. The XRD analysis indicates that the NCTFs are polycrystalline, meaning that they are made up of many small crystals. The crystals are oriented in a random fashion, which is why the XRD pattern is broad. The anatase phase of TiO
2
is a tetragonal crystal structure. The NiO and In
2
O
3
phases are both cubic crystal structures. The presence of nanostructure cubic phases indicates that the nanoparticles in the films are small enough to significantly affect the crystal structure of the films. Scanning electron microscopy images showed surface homogeneity, with small granular grains of nanostructures without any cracks. The gas sensor created using the prepared samples showed high sensitivity to NO
2
and H
2
S gases, and its sensitivity was measured at different operation temperatures, along with response and recovery times. The optical properties of In
2
O
3
are affected by the addition of TiO
2
and NiO impurities. The transmittance of In
2
O
3
increases as the NiO ratio increases and the TiO
2
ratio decreases.</description><subject>Anatase</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Composites & Nanocomposites</subject><subject>cost effectiveness</subject><subject>Crystal structure</subject><subject>Crystallography and Scattering Methods</subject><subject>electron microscopy</subject><subject>Gas sensors</subject><subject>Gases</subject><subject>glass</subject><subject>Glass substrates</subject><subject>Homogeneity</subject><subject>Indium oxides</subject><subject>Materials Science</subject><subject>Nanocomposites</subject><subject>nanoparticles</subject><subject>Nanostructure</subject><subject>nickel oxide</subject><subject>Nickel oxides</subject><subject>Nitrogen dioxide</subject><subject>Optical properties</subject><subject>physical properties</subject><subject>Polymer Sciences</subject><subject>Production methods</subject><subject>pyrolysis</subject><subject>Sensitivity</subject><subject>Solid Mechanics</subject><subject>Spray pyrolysis</subject><subject>Thin films</subject><subject>Titanium dioxide</subject><subject>transmittance</subject><subject>X-ray diffraction</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9kcFuEzEQhi0EEqHwApwscSlSF8b2er3LiSqiNFKVPRDOluvYiauNHTwbpOTEO_AIfbM-CW6CQOLAaTSj7_9nND8hrxm8YwDqPTJopaiA1xV0QjXV4QmZMKlEVbcgnpIJAOcVrxv2nLxAvAMAqTibkPtZ_O5wDCszhhSRpkgXoecPP37OQ_9xFnkvaDQx2bTZJgyjo-M6ROrDsEF6Pp8urvAt9SnTlUGKLmKIqw8U93FcOwx4QbfrPQZrBmrXJhs7uhwOx10X1MQlXbrR2ceWJk_nPT8Or_mXP34p40vyzJsB3avf9Yx8vfq0mF5XN_3n2fTyprICxFjJpQUlG2vAW--MunVLbsHUQjrRcK7AcAOqM7WqTd11zHoG6tYLqerWtqYVZ-T85LvN6duufEVvAlo3DCa6tEMtmBSykx00BX3zD3qXdjmW6zQv_y_20IpC8RNlc0LMzuttDhuT95qBfsxNn3LTJTd9zE0fikicRFjguHL5r_V_VL8A3p6dLQ</recordid><startdate>20240201</startdate><enddate>20240201</enddate><creator>Alborisha, Mohamed Abed Shahoodh</creator><creator>Ibrahim, Foued Tarek</creator><creator>Jilani, Wissal</creator><creator>Bouzidi, Abdelfatteh</creator><creator>Guermazi, Samir</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>7S9</scope><scope>L.6</scope><orcidid>https://orcid.org/0000-0002-6166-1107</orcidid></search><sort><creationdate>20240201</creationdate><title>Investigations on TiO2–NiO@In2O3 nanocomposite thin films (NCTFs) for gas sensing: synthesis, physical characterization, and detection of NO2 and H2S gas sensors</title><author>Alborisha, Mohamed Abed Shahoodh ; Ibrahim, Foued Tarek ; Jilani, Wissal ; Bouzidi, Abdelfatteh ; Guermazi, Samir</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c303t-5dc0756ca0fcfea7bed2c0a435e362270a2a079a474a4991cf107bf35748c8a83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Anatase</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Composites & Nanocomposites</topic><topic>cost effectiveness</topic><topic>Crystal structure</topic><topic>Crystallography and Scattering Methods</topic><topic>electron microscopy</topic><topic>Gas sensors</topic><topic>Gases</topic><topic>glass</topic><topic>Glass substrates</topic><topic>Homogeneity</topic><topic>Indium oxides</topic><topic>Materials Science</topic><topic>Nanocomposites</topic><topic>nanoparticles</topic><topic>Nanostructure</topic><topic>nickel oxide</topic><topic>Nickel oxides</topic><topic>Nitrogen dioxide</topic><topic>Optical properties</topic><topic>physical properties</topic><topic>Polymer Sciences</topic><topic>Production methods</topic><topic>pyrolysis</topic><topic>Sensitivity</topic><topic>Solid Mechanics</topic><topic>Spray pyrolysis</topic><topic>Thin films</topic><topic>Titanium dioxide</topic><topic>transmittance</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Alborisha, Mohamed Abed Shahoodh</creatorcontrib><creatorcontrib>Ibrahim, Foued Tarek</creatorcontrib><creatorcontrib>Jilani, Wissal</creatorcontrib><creatorcontrib>Bouzidi, Abdelfatteh</creatorcontrib><creatorcontrib>Guermazi, Samir</creatorcontrib><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>AGRICOLA</collection><collection>AGRICOLA - Academic</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Alborisha, Mohamed Abed Shahoodh</au><au>Ibrahim, Foued Tarek</au><au>Jilani, Wissal</au><au>Bouzidi, Abdelfatteh</au><au>Guermazi, Samir</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigations on TiO2–NiO@In2O3 nanocomposite thin films (NCTFs) for gas sensing: synthesis, physical characterization, and detection of NO2 and H2S gas sensors</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2024-02-01</date><risdate>2024</risdate><volume>59</volume><issue>8</issue><spage>3451</spage><epage>3466</epage><pages>3451-3466</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>The spray pyrolysis technique is a versatile and cost-effective method for producing TiO
2
–NiO@In
2
O
3
NCTFs on glass substrates with varying molar ratios. NCTFs have been studied for gas sensing applications due to their excellent sensing properties. The films' structural, morphological, and gas sensing characteristics were analyzed. The XRD analysis indicates that the NCTFs are polycrystalline, meaning that they are made up of many small crystals. The crystals are oriented in a random fashion, which is why the XRD pattern is broad. The anatase phase of TiO
2
is a tetragonal crystal structure. The NiO and In
2
O
3
phases are both cubic crystal structures. The presence of nanostructure cubic phases indicates that the nanoparticles in the films are small enough to significantly affect the crystal structure of the films. Scanning electron microscopy images showed surface homogeneity, with small granular grains of nanostructures without any cracks. The gas sensor created using the prepared samples showed high sensitivity to NO
2
and H
2
S gases, and its sensitivity was measured at different operation temperatures, along with response and recovery times. The optical properties of In
2
O
3
are affected by the addition of TiO
2
and NiO impurities. The transmittance of In
2
O
3
increases as the NiO ratio increases and the TiO
2
ratio decreases.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-024-09376-z</doi><tpages>16</tpages><orcidid>https://orcid.org/0000-0002-6166-1107</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0022-2461 |
| ispartof | Journal of materials science, 2024-02, Vol.59 (8), p.3451-3466 |
| issn | 0022-2461 1573-4803 |
| language | eng |
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| source | SpringerLink Journals |
| subjects | Anatase Characterization and Evaluation of Materials Chemistry and Materials Science Classical Mechanics Composites & Nanocomposites cost effectiveness Crystal structure Crystallography and Scattering Methods electron microscopy Gas sensors Gases glass Glass substrates Homogeneity Indium oxides Materials Science Nanocomposites nanoparticles Nanostructure nickel oxide Nickel oxides Nitrogen dioxide Optical properties physical properties Polymer Sciences Production methods pyrolysis Sensitivity Solid Mechanics Spray pyrolysis Thin films Titanium dioxide transmittance X-ray diffraction |
| title | Investigations on TiO2–NiO@In2O3 nanocomposite thin films (NCTFs) for gas sensing: synthesis, physical characterization, and detection of NO2 and H2S gas sensors |
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