Experimental and theoretical studies on nitrate removal using epichlorohydrin-modified cross-linked chitosan derived from shrimp waste
Nitrates level in water is a worldwide problem that represents a risk to the environment and people’s health; efforts are currently devoted to the development and implementation of new biomaterials for their removal. In this study, chitosan (Ch) from shrimp waste and the related epichlorohydrin-modi...
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| Veröffentlicht in: | Environmental science and pollution research international 2023-10, Vol.30 (49), p.107772-107789 |
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| creator | EL Kaim Billah, Rachid Lgaz, Hassane Jiménez, Daniel Goma Pal, Preeti Trujillo-Navarrete, Balter Ahrouch, Mohammadi Algethami, Jari S. Abdellaoui, Youness Majdoubi, Hicham Alrashdi, Awad A. Agunaou, Mahfoud Soufiane, Abdessadik López-Maldonado, Eduardo Alberto |
| description | Nitrates level in water is a worldwide problem that represents a risk to the environment and people’s health; efforts are currently devoted to the development and implementation of new biomaterials for their removal. In this study, chitosan (Ch) from shrimp waste and the related epichlorohydrin-modified crossover chitosan (Ch-EPI) were used to remove nitrates from aqueous solutions. The mechanism of selective nitrate removal was elucidated and validated by theoretical calculations. The physicochemical performance of Ch and Ch-EPI was investigated through the main parameters pH, adsorption capacity, contact time, initial nitrate concentration, coexisting anions, and temperature. The experimental data were fitted to widely used adsorption kinetic models and adsorption isotherms. The maximum percentage of nitrate adsorption was reached at an equilibrium pH of 4.0 at an adsorbent dose of 2.0 g/L after a contact time of 50 min. Competing anion experiments show that chloride and sulfate ions have minimal and maximal effects on nitrate adsorption by Ch-EPI. Experimental adsorption data are best fitted to pseudo-second-order kinetic and isothermal Langmuir models. The maximum adsorption capacities of Ch and Ch-EPI for nitrate removal were 12.0 mg/g and 38 mg/g, respectively. |
| doi_str_mv | 10.1007/s11356-023-29896-6 |
| format | Article |
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In this study, chitosan (Ch) from shrimp waste and the related epichlorohydrin-modified crossover chitosan (Ch-EPI) were used to remove nitrates from aqueous solutions. The mechanism of selective nitrate removal was elucidated and validated by theoretical calculations. The physicochemical performance of Ch and Ch-EPI was investigated through the main parameters pH, adsorption capacity, contact time, initial nitrate concentration, coexisting anions, and temperature. The experimental data were fitted to widely used adsorption kinetic models and adsorption isotherms. The maximum percentage of nitrate adsorption was reached at an equilibrium pH of 4.0 at an adsorbent dose of 2.0 g/L after a contact time of 50 min. Competing anion experiments show that chloride and sulfate ions have minimal and maximal effects on nitrate adsorption by Ch-EPI. Experimental adsorption data are best fitted to pseudo-second-order kinetic and isothermal Langmuir models. The maximum adsorption capacities of Ch and Ch-EPI for nitrate removal were 12.0 mg/g and 38 mg/g, respectively.</description><identifier>ISSN: 1614-7499</identifier><identifier>ISSN: 0944-1344</identifier><identifier>EISSN: 1614-7499</identifier><identifier>DOI: 10.1007/s11356-023-29896-6</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>adsorbents ; Adsorption ; Anions ; Aquatic Pollution ; Aqueous solutions ; Atmospheric Protection/Air Quality Control/Air Pollution ; biocompatible materials ; Biomaterials ; Biomedical materials ; Chitosan ; chlorides ; crosslinking ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Epichlorohydrin ; Nitrate removal ; Nitrates ; Nitrogen removal ; Nutrient removal ; Research Article ; risk ; shrimp ; Shrimps ; sulfates ; temperature ; Waste Water Technology ; wastes ; Water Management ; Water Pollution Control</subject><ispartof>Environmental science and pollution research international, 2023-10, Vol.30 (49), p.107772-107789</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c336t-8f1c33dd486e5d181a89a493bb639035a7b4e1a83fda7000eb41903a0557bdf63</cites><orcidid>0000-0002-1884-4821</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11356-023-29896-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11356-023-29896-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>EL Kaim Billah, Rachid</creatorcontrib><creatorcontrib>Lgaz, Hassane</creatorcontrib><creatorcontrib>Jiménez, Daniel Goma</creatorcontrib><creatorcontrib>Pal, Preeti</creatorcontrib><creatorcontrib>Trujillo-Navarrete, Balter</creatorcontrib><creatorcontrib>Ahrouch, Mohammadi</creatorcontrib><creatorcontrib>Algethami, Jari S.</creatorcontrib><creatorcontrib>Abdellaoui, Youness</creatorcontrib><creatorcontrib>Majdoubi, Hicham</creatorcontrib><creatorcontrib>Alrashdi, Awad A.</creatorcontrib><creatorcontrib>Agunaou, Mahfoud</creatorcontrib><creatorcontrib>Soufiane, Abdessadik</creatorcontrib><creatorcontrib>López-Maldonado, Eduardo Alberto</creatorcontrib><title>Experimental and theoretical studies on nitrate removal using epichlorohydrin-modified cross-linked chitosan derived from shrimp waste</title><title>Environmental science and pollution research international</title><addtitle>Environ Sci Pollut Res</addtitle><description>Nitrates level in water is a worldwide problem that represents a risk to the environment and people’s health; efforts are currently devoted to the development and implementation of new biomaterials for their removal. In this study, chitosan (Ch) from shrimp waste and the related epichlorohydrin-modified crossover chitosan (Ch-EPI) were used to remove nitrates from aqueous solutions. The mechanism of selective nitrate removal was elucidated and validated by theoretical calculations. The physicochemical performance of Ch and Ch-EPI was investigated through the main parameters pH, adsorption capacity, contact time, initial nitrate concentration, coexisting anions, and temperature. The experimental data were fitted to widely used adsorption kinetic models and adsorption isotherms. The maximum percentage of nitrate adsorption was reached at an equilibrium pH of 4.0 at an adsorbent dose of 2.0 g/L after a contact time of 50 min. Competing anion experiments show that chloride and sulfate ions have minimal and maximal effects on nitrate adsorption by Ch-EPI. Experimental adsorption data are best fitted to pseudo-second-order kinetic and isothermal Langmuir models. 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In this study, chitosan (Ch) from shrimp waste and the related epichlorohydrin-modified crossover chitosan (Ch-EPI) were used to remove nitrates from aqueous solutions. The mechanism of selective nitrate removal was elucidated and validated by theoretical calculations. The physicochemical performance of Ch and Ch-EPI was investigated through the main parameters pH, adsorption capacity, contact time, initial nitrate concentration, coexisting anions, and temperature. The experimental data were fitted to widely used adsorption kinetic models and adsorption isotherms. The maximum percentage of nitrate adsorption was reached at an equilibrium pH of 4.0 at an adsorbent dose of 2.0 g/L after a contact time of 50 min. Competing anion experiments show that chloride and sulfate ions have minimal and maximal effects on nitrate adsorption by Ch-EPI. Experimental adsorption data are best fitted to pseudo-second-order kinetic and isothermal Langmuir models. 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| subjects | adsorbents Adsorption Anions Aquatic Pollution Aqueous solutions Atmospheric Protection/Air Quality Control/Air Pollution biocompatible materials Biomaterials Biomedical materials Chitosan chlorides crosslinking Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Epichlorohydrin Nitrate removal Nitrates Nitrogen removal Nutrient removal Research Article risk shrimp Shrimps sulfates temperature Waste Water Technology wastes Water Management Water Pollution Control |
| title | Experimental and theoretical studies on nitrate removal using epichlorohydrin-modified cross-linked chitosan derived from shrimp waste |
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