Synthesis and characterisation of carbon nanotubes and zinc oxide composites: sub-millisecond UV response
In this study, various morphological configurations of zinc oxide (ZnO) were fabricated onto the carbon nanotube (CNT) network by influencing the pH levels of the growth solution (specifically, pH values of 5, 7, and 9). The CNT network was fabricated using the thermal chemical vapour deposition met...
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| Veröffentlicht in: | Journal of materials science 2023-11, Vol.58 (44), p.17019-17033 |
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| creator | Majumder, Rahul Kundu, Soumalya Mukherjee, Suchandra Banerjee, Aritra Gayen, Rabindranath Pal Chowdhury, Manish |
| description | In this study, various morphological configurations of zinc oxide (ZnO) were fabricated onto the carbon nanotube (CNT) network by influencing the pH levels of the growth solution (specifically, pH values of 5, 7, and 9). The CNT network was fabricated using the thermal chemical vapour deposition method, while the ZnO nanostructure was synthesised using the chemical bath deposition technique. The growth of the multi-walled CNT network was confirmed by utilising field emission gun transmission electron microscopy and Raman spectroscopy. On the other hand, the investigation of the distinct morphology of pH-dependent ZnO on the CNT network was confirmed by employing field emission scanning electron microscopy. Three specific types of UV photo-sensing devices were manufactured utilising the synthesised samples, and a comprehensive investigation was conducted to analyse their UV-responsive characteristics. The analysis of the UV-responsive behaviour involved subjecting the devices to an array of UV LEDs. The intensity of the 365 nm UV LED array varied between 18.7 and 95.22 μW/cm
2
. For a device fabricated with ZnO grown at pH 5, the maximum photocurrent was recorded to be 40.7 ± 0.26 μA, and the external quantum efficiency was 5359 ± 73%. The device also showed remarkable responsivity to UV radiation with a pulsing frequency of 500 Hz. Exceptional response time and recovery time of 316 μs and 364 μs have been measured for the device. |
| doi_str_mv | 10.1007/s10853-023-09058-2 |
| format | Article |
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2
. For a device fabricated with ZnO grown at pH 5, the maximum photocurrent was recorded to be 40.7 ± 0.26 μA, and the external quantum efficiency was 5359 ± 73%. The device also showed remarkable responsivity to UV radiation with a pulsing frequency of 500 Hz. Exceptional response time and recovery time of 316 μs and 364 μs have been measured for the device.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-023-09058-2</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Analysis ; Arrays ; Carbon nanotubes ; Characterization and Evaluation of Materials ; Chemical synthesis ; Chemical vapor deposition ; Chemistry and Materials Science ; Classical Mechanics ; Crystallography and Scattering Methods ; electric current ; Electron microscopy ; Electronic Materials ; Field emission microscopy ; Light-emitting diodes ; Materials Science ; Microscopy ; Morphology ; Nanotubes ; Photoelectric effect ; Polymer Sciences ; Quantum efficiency ; Radiation ; Raman spectroscopy ; Recovery time ; Sensors ; Solid Mechanics ; transmission electron microscopy ; Ultraviolet radiation ; vapors ; Zinc oxide ; Zinc oxides</subject><ispartof>Journal of materials science, 2023-11, Vol.58 (44), p.17019-17033</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><rights>COPYRIGHT 2023 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c404t-b812e7ff2591f5f542a830785de02dfffb067b72c4155e7e9cb188cc2dc2d1803</cites><orcidid>0000-0003-4001-8048</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10853-023-09058-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10853-023-09058-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Majumder, Rahul</creatorcontrib><creatorcontrib>Kundu, Soumalya</creatorcontrib><creatorcontrib>Mukherjee, Suchandra</creatorcontrib><creatorcontrib>Banerjee, Aritra</creatorcontrib><creatorcontrib>Gayen, Rabindranath</creatorcontrib><creatorcontrib>Pal Chowdhury, Manish</creatorcontrib><title>Synthesis and characterisation of carbon nanotubes and zinc oxide composites: sub-millisecond UV response</title><title>Journal of materials science</title><addtitle>J Mater Sci</addtitle><description>In this study, various morphological configurations of zinc oxide (ZnO) were fabricated onto the carbon nanotube (CNT) network by influencing the pH levels of the growth solution (specifically, pH values of 5, 7, and 9). The CNT network was fabricated using the thermal chemical vapour deposition method, while the ZnO nanostructure was synthesised using the chemical bath deposition technique. The growth of the multi-walled CNT network was confirmed by utilising field emission gun transmission electron microscopy and Raman spectroscopy. On the other hand, the investigation of the distinct morphology of pH-dependent ZnO on the CNT network was confirmed by employing field emission scanning electron microscopy. Three specific types of UV photo-sensing devices were manufactured utilising the synthesised samples, and a comprehensive investigation was conducted to analyse their UV-responsive characteristics. The analysis of the UV-responsive behaviour involved subjecting the devices to an array of UV LEDs. The intensity of the 365 nm UV LED array varied between 18.7 and 95.22 μW/cm
2
. For a device fabricated with ZnO grown at pH 5, the maximum photocurrent was recorded to be 40.7 ± 0.26 μA, and the external quantum efficiency was 5359 ± 73%. The device also showed remarkable responsivity to UV radiation with a pulsing frequency of 500 Hz. Exceptional response time and recovery time of 316 μs and 364 μs have been measured for the device.</description><subject>Analysis</subject><subject>Arrays</subject><subject>Carbon nanotubes</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemical vapor deposition</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Crystallography and Scattering Methods</subject><subject>electric current</subject><subject>Electron microscopy</subject><subject>Electronic Materials</subject><subject>Field emission microscopy</subject><subject>Light-emitting diodes</subject><subject>Materials Science</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>Nanotubes</subject><subject>Photoelectric effect</subject><subject>Polymer Sciences</subject><subject>Quantum efficiency</subject><subject>Radiation</subject><subject>Raman spectroscopy</subject><subject>Recovery time</subject><subject>Sensors</subject><subject>Solid Mechanics</subject><subject>transmission electron microscopy</subject><subject>Ultraviolet radiation</subject><subject>vapors</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9ktFKHTEQhkOx4NH2Bbxa6E29WJtkNybbOxHbCoJQa29DNjs5RnaTYyYL2qdvTrcgR0QyIWH4_mFm-Ak5YvSEUSq_IKNKNDXl5XZUqJq_IysmZFO3ijZ7ZEUp5zVvT9k-OUC8p5QKydmK-JunkO8APVYmDJW9M8nYDMmjyT6GKrrKmtSXXzAh5rmHBfzjg63iox-gsnHaRPQZ8GuFc19Pfhw9go0Fu_1dJcBNDAgfyHtnRoSP_99Dcvvt4tf5j_rq-vvl-dlVbVva5rpXjIN0jouOOeFEy41qqFRiAMoH51xPT2UvuW2ZECChsz1Tylo-lGBl2EPyeam7SfFhBsx68mhhHE2AOKNumGiEZB1nBf30Ar2PcwqlO81V13CpOsafqbUZQfvgYi472hbVZ1K2rJUFLNTJK1Q5A0y-7AKcL_kdwfGOoDAZHvPazIj68ubnLssX1qaImMDpTfKTSU-aUb01gF4MoIsB9D8D6G3fzSLCAoc1pOfp3lD9BaYcsdQ</recordid><startdate>20231101</startdate><enddate>20231101</enddate><creator>Majumder, Rahul</creator><creator>Kundu, Soumalya</creator><creator>Mukherjee, Suchandra</creator><creator>Banerjee, Aritra</creator><creator>Gayen, Rabindranath</creator><creator>Pal Chowdhury, Manish</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>7S9</scope><scope>L.6</scope><orcidid>https://orcid.org/0000-0003-4001-8048</orcidid></search><sort><creationdate>20231101</creationdate><title>Synthesis and characterisation of carbon nanotubes and zinc oxide composites: sub-millisecond UV response</title><author>Majumder, Rahul ; Kundu, Soumalya ; Mukherjee, Suchandra ; Banerjee, Aritra ; Gayen, Rabindranath ; Pal Chowdhury, Manish</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c404t-b812e7ff2591f5f542a830785de02dfffb067b72c4155e7e9cb188cc2dc2d1803</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Analysis</topic><topic>Arrays</topic><topic>Carbon nanotubes</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical synthesis</topic><topic>Chemical vapor deposition</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Crystallography and Scattering Methods</topic><topic>electric current</topic><topic>Electron microscopy</topic><topic>Electronic Materials</topic><topic>Field emission microscopy</topic><topic>Light-emitting diodes</topic><topic>Materials Science</topic><topic>Microscopy</topic><topic>Morphology</topic><topic>Nanotubes</topic><topic>Photoelectric effect</topic><topic>Polymer Sciences</topic><topic>Quantum efficiency</topic><topic>Radiation</topic><topic>Raman spectroscopy</topic><topic>Recovery time</topic><topic>Sensors</topic><topic>Solid Mechanics</topic><topic>transmission electron microscopy</topic><topic>Ultraviolet radiation</topic><topic>vapors</topic><topic>Zinc oxide</topic><topic>Zinc oxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Majumder, Rahul</creatorcontrib><creatorcontrib>Kundu, Soumalya</creatorcontrib><creatorcontrib>Mukherjee, Suchandra</creatorcontrib><creatorcontrib>Banerjee, Aritra</creatorcontrib><creatorcontrib>Gayen, Rabindranath</creatorcontrib><creatorcontrib>Pal Chowdhury, Manish</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection (ProQuest)</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>AGRICOLA</collection><collection>AGRICOLA - Academic</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Majumder, Rahul</au><au>Kundu, Soumalya</au><au>Mukherjee, Suchandra</au><au>Banerjee, Aritra</au><au>Gayen, Rabindranath</au><au>Pal Chowdhury, Manish</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterisation of carbon nanotubes and zinc oxide composites: sub-millisecond UV response</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2023-11-01</date><risdate>2023</risdate><volume>58</volume><issue>44</issue><spage>17019</spage><epage>17033</epage><pages>17019-17033</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>In this study, various morphological configurations of zinc oxide (ZnO) were fabricated onto the carbon nanotube (CNT) network by influencing the pH levels of the growth solution (specifically, pH values of 5, 7, and 9). 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2
. For a device fabricated with ZnO grown at pH 5, the maximum photocurrent was recorded to be 40.7 ± 0.26 μA, and the external quantum efficiency was 5359 ± 73%. The device also showed remarkable responsivity to UV radiation with a pulsing frequency of 500 Hz. Exceptional response time and recovery time of 316 μs and 364 μs have been measured for the device.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-023-09058-2</doi><tpages>15</tpages><orcidid>https://orcid.org/0000-0003-4001-8048</orcidid></addata></record> |
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| subjects | Analysis Arrays Carbon nanotubes Characterization and Evaluation of Materials Chemical synthesis Chemical vapor deposition Chemistry and Materials Science Classical Mechanics Crystallography and Scattering Methods electric current Electron microscopy Electronic Materials Field emission microscopy Light-emitting diodes Materials Science Microscopy Morphology Nanotubes Photoelectric effect Polymer Sciences Quantum efficiency Radiation Raman spectroscopy Recovery time Sensors Solid Mechanics transmission electron microscopy Ultraviolet radiation vapors Zinc oxide Zinc oxides |
| title | Synthesis and characterisation of carbon nanotubes and zinc oxide composites: sub-millisecond UV response |
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