Rice husk coated with copper oxide nanoparticles for 17α-ethinylestradiol removal from an aqueous solution: adsorption mechanisms and kinetics
The 17 α-ethinylestradiol (EE2) adsorption from aqueous solution was examined using a novel adsorbent made from rice husk powder coated with CuO nanoparticles (CRH). Advanced analyses of FTIR, XRD, SEM, and EDSwere used to identify the classification parameters of a CRH-like surface morphology, conf...
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| Veröffentlicht in: | Environmental monitoring and assessment 2023-09, Vol.195 (9), p.1078-1078, Article 1078 |
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| creator | Alhares, Hasanain Saad Ali, Qahtan Adnan Shaban, Mohammed Ali A. M-Ridha, Mohanad J. Bohan, Hawraa R. Mohammed, Sabah J. Abed, Khalid M. Hasan, Hassimi Abu |
| description | The 17 α-ethinylestradiol (EE2) adsorption from aqueous solution was examined using a novel adsorbent made from rice husk powder coated with CuO nanoparticles (CRH). Advanced analyses of FTIR, XRD, SEM, and EDSwere used to identify the classification parameters of a CRH-like surface morphology, configuration, and functional groups. The rice husk was coated with CuO nanoparticles, allowing it to create large surface area materials with significantly improved textural qualities with regard to functional use and adsorption performance, according to a detailed characterization of the synthesized materials. The adsorption process was applied successfully with elimination effectiveness of 100% which can be kept up to 61.3%. The parameters of adsorption were affecting the adsorption process significantly. Thermodynamic data stated that the process of adsorption was endothermic, spontaneous, chemisorption and the molecules of EE2 show affinity with the CRH. It was discovered that the adsorption process controlled by a pseudo-second–order kinetic model demonstrates that the chemisorption process was controlling EE2 removal. The Sips model is regarded as optimal for representing this practice, exhibiting a significantly high determination coefficient of 0.948. This coefficient implies that the adsorption mechanism indicates the occurrence of both heterogeneous and homogeneous adsorption. According to the findings, biomass can serve as a cheap, operative sorbent to remove estrogen from liquified solutions. |
| doi_str_mv | 10.1007/s10661-023-11689-6 |
| format | Article |
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Advanced analyses of FTIR, XRD, SEM, and EDSwere used to identify the classification parameters of a CRH-like surface morphology, configuration, and functional groups. The rice husk was coated with CuO nanoparticles, allowing it to create large surface area materials with significantly improved textural qualities with regard to functional use and adsorption performance, according to a detailed characterization of the synthesized materials. The adsorption process was applied successfully with elimination effectiveness of 100% which can be kept up to 61.3%. The parameters of adsorption were affecting the adsorption process significantly. Thermodynamic data stated that the process of adsorption was endothermic, spontaneous, chemisorption and the molecules of EE2 show affinity with the CRH. It was discovered that the adsorption process controlled by a pseudo-second–order kinetic model demonstrates that the chemisorption process was controlling EE2 removal. The Sips model is regarded as optimal for representing this practice, exhibiting a significantly high determination coefficient of 0.948. This coefficient implies that the adsorption mechanism indicates the occurrence of both heterogeneous and homogeneous adsorption. According to the findings, biomass can serve as a cheap, operative sorbent to remove estrogen from liquified solutions.</description><identifier>ISSN: 0167-6369</identifier><identifier>EISSN: 1573-2959</identifier><identifier>DOI: 10.1007/s10661-023-11689-6</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>adsorbents ; Adsorption ; Aqueous solutions ; Atmospheric Protection/Air Quality Control/Air Pollution ; biomass ; Chemisorption ; Coatings ; Copper ; Copper oxides ; cupric oxide ; Earth and Environmental Science ; Ecology ; Ecotoxicology ; Endothermic reactions ; endothermy ; Environment ; Environmental Management ; Environmental monitoring ; Environmental science ; Estrogens ; Ethinylestradiol ; Functional groups ; Kinetics ; Mathematical models ; Monitoring/Environmental Analysis ; Nanoparticles ; Oestrogens ; Parameter identification ; Parameters ; Removal ; Rice ; rice hulls ; Sex hormones ; Sorbents ; surface area ; Surface chemistry ; thermodynamics</subject><ispartof>Environmental monitoring and assessment, 2023-09, Vol.195 (9), p.1078-1078, Article 1078</ispartof><rights>The Author(s), under exclusive licence to Springer Nature Switzerland AG 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3006-ba980f4a0abfc6f02232b2c3b0e8fad1eb5a9451bc277ace49850b33f981908b3</citedby><cites>FETCH-LOGICAL-c3006-ba980f4a0abfc6f02232b2c3b0e8fad1eb5a9451bc277ace49850b33f981908b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10661-023-11689-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10661-023-11689-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,778,782,27911,27912,41475,42544,51306</link.rule.ids></links><search><creatorcontrib>Alhares, Hasanain Saad</creatorcontrib><creatorcontrib>Ali, Qahtan Adnan</creatorcontrib><creatorcontrib>Shaban, Mohammed Ali A.</creatorcontrib><creatorcontrib>M-Ridha, Mohanad J.</creatorcontrib><creatorcontrib>Bohan, Hawraa R.</creatorcontrib><creatorcontrib>Mohammed, Sabah J.</creatorcontrib><creatorcontrib>Abed, Khalid M.</creatorcontrib><creatorcontrib>Hasan, Hassimi Abu</creatorcontrib><title>Rice husk coated with copper oxide nanoparticles for 17α-ethinylestradiol removal from an aqueous solution: adsorption mechanisms and kinetics</title><title>Environmental monitoring and assessment</title><addtitle>Environ Monit Assess</addtitle><description>The 17 α-ethinylestradiol (EE2) adsorption from aqueous solution was examined using a novel adsorbent made from rice husk powder coated with CuO nanoparticles (CRH). Advanced analyses of FTIR, XRD, SEM, and EDSwere used to identify the classification parameters of a CRH-like surface morphology, configuration, and functional groups. The rice husk was coated with CuO nanoparticles, allowing it to create large surface area materials with significantly improved textural qualities with regard to functional use and adsorption performance, according to a detailed characterization of the synthesized materials. The adsorption process was applied successfully with elimination effectiveness of 100% which can be kept up to 61.3%. The parameters of adsorption were affecting the adsorption process significantly. Thermodynamic data stated that the process of adsorption was endothermic, spontaneous, chemisorption and the molecules of EE2 show affinity with the CRH. It was discovered that the adsorption process controlled by a pseudo-second–order kinetic model demonstrates that the chemisorption process was controlling EE2 removal. The Sips model is regarded as optimal for representing this practice, exhibiting a significantly high determination coefficient of 0.948. This coefficient implies that the adsorption mechanism indicates the occurrence of both heterogeneous and homogeneous adsorption. According to the findings, biomass can serve as a cheap, operative sorbent to remove estrogen from liquified solutions.</description><subject>adsorbents</subject><subject>Adsorption</subject><subject>Aqueous solutions</subject><subject>Atmospheric Protection/Air Quality Control/Air Pollution</subject><subject>biomass</subject><subject>Chemisorption</subject><subject>Coatings</subject><subject>Copper</subject><subject>Copper oxides</subject><subject>cupric oxide</subject><subject>Earth and Environmental Science</subject><subject>Ecology</subject><subject>Ecotoxicology</subject><subject>Endothermic reactions</subject><subject>endothermy</subject><subject>Environment</subject><subject>Environmental Management</subject><subject>Environmental monitoring</subject><subject>Environmental science</subject><subject>Estrogens</subject><subject>Ethinylestradiol</subject><subject>Functional groups</subject><subject>Kinetics</subject><subject>Mathematical models</subject><subject>Monitoring/Environmental Analysis</subject><subject>Nanoparticles</subject><subject>Oestrogens</subject><subject>Parameter identification</subject><subject>Parameters</subject><subject>Removal</subject><subject>Rice</subject><subject>rice hulls</subject><subject>Sex hormones</subject><subject>Sorbents</subject><subject>surface area</subject><subject>Surface 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Assess</stitle><date>2023-09-01</date><risdate>2023</risdate><volume>195</volume><issue>9</issue><spage>1078</spage><epage>1078</epage><pages>1078-1078</pages><artnum>1078</artnum><issn>0167-6369</issn><eissn>1573-2959</eissn><abstract>The 17 α-ethinylestradiol (EE2) adsorption from aqueous solution was examined using a novel adsorbent made from rice husk powder coated with CuO nanoparticles (CRH). Advanced analyses of FTIR, XRD, SEM, and EDSwere used to identify the classification parameters of a CRH-like surface morphology, configuration, and functional groups. The rice husk was coated with CuO nanoparticles, allowing it to create large surface area materials with significantly improved textural qualities with regard to functional use and adsorption performance, according to a detailed characterization of the synthesized materials. The adsorption process was applied successfully with elimination effectiveness of 100% which can be kept up to 61.3%. The parameters of adsorption were affecting the adsorption process significantly. Thermodynamic data stated that the process of adsorption was endothermic, spontaneous, chemisorption and the molecules of EE2 show affinity with the CRH. It was discovered that the adsorption process controlled by a pseudo-second–order kinetic model demonstrates that the chemisorption process was controlling EE2 removal. The Sips model is regarded as optimal for representing this practice, exhibiting a significantly high determination coefficient of 0.948. This coefficient implies that the adsorption mechanism indicates the occurrence of both heterogeneous and homogeneous adsorption. According to the findings, biomass can serve as a cheap, operative sorbent to remove estrogen from liquified solutions.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s10661-023-11689-6</doi><tpages>1</tpages></addata></record> |
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| subjects | adsorbents Adsorption Aqueous solutions Atmospheric Protection/Air Quality Control/Air Pollution biomass Chemisorption Coatings Copper Copper oxides cupric oxide Earth and Environmental Science Ecology Ecotoxicology Endothermic reactions endothermy Environment Environmental Management Environmental monitoring Environmental science Estrogens Ethinylestradiol Functional groups Kinetics Mathematical models Monitoring/Environmental Analysis Nanoparticles Oestrogens Parameter identification Parameters Removal Rice rice hulls Sex hormones Sorbents surface area Surface chemistry thermodynamics |
| title | Rice husk coated with copper oxide nanoparticles for 17α-ethinylestradiol removal from an aqueous solution: adsorption mechanisms and kinetics |
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