Fabrication and Characterization of Biomedical Ti-Mg Composites via Spark Plasma Sintering
The fabrication of Ti-Mg composite biomaterials was investigated using spark plasma sintering (SPS) with varying Mg contents and sintering pressures. The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were syst...
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| Veröffentlicht in: | Materials 2024-07, Vol.17 (14), p.3470 |
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| creator | Masuda, Taisei Oh, Minho Kobayashi, Equo |
| description | The fabrication of Ti-Mg composite biomaterials was investigated using spark plasma sintering (SPS) with varying Mg contents and sintering pressures. The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were systematically analyzed. Uniform dispersion of Mg within the Ti matrix was achieved, confirming the efficacy of ethanol-assisted ball milling for consistent mixing. The Young's modulus of the composite materials exhibited a linear decrease with increasing Mg content, with Ti-30vol%Mg and Ti-50vol%Mg demonstrating reduced modulus values compared to pure Ti. Based on density measurements, compression tests, and Young's modulus results, it was determined that the sinterability of Ti-30vol%Mg saturates at a sintering pressure of approximately 50 MPa. Moreover, our immersion tests in physiological saline underscore the profound significance of our findings. Ti-30vol%Mg maintained compressive strength above that of cortical bone for 6-to-10 days, with mechanical integrity improving under higher sintering pressures. These findings mark a significant leap towards the development of Ti-Mg composite biomaterials with tailored mechanical properties, thereby enhancing biocompatibility and osseointegration for a wide range of biomedical applications. |
| doi_str_mv | 10.3390/ma17143470 |
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The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were systematically analyzed. Uniform dispersion of Mg within the Ti matrix was achieved, confirming the efficacy of ethanol-assisted ball milling for consistent mixing. The Young's modulus of the composite materials exhibited a linear decrease with increasing Mg content, with Ti-30vol%Mg and Ti-50vol%Mg demonstrating reduced modulus values compared to pure Ti. Based on density measurements, compression tests, and Young's modulus results, it was determined that the sinterability of Ti-30vol%Mg saturates at a sintering pressure of approximately 50 MPa. Moreover, our immersion tests in physiological saline underscore the profound significance of our findings. Ti-30vol%Mg maintained compressive strength above that of cortical bone for 6-to-10 days, with mechanical integrity improving under higher sintering pressures. These findings mark a significant leap towards the development of Ti-Mg composite biomaterials with tailored mechanical properties, thereby enhancing biocompatibility and osseointegration for a wide range of biomedical applications.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma17143470</identifier><identifier>PMID: 39063762</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Analysis ; Ball milling ; Biocompatibility ; Biological products ; Biomedical materials ; Composite materials ; Compression tests ; Compressive strength ; Ethanol ; Fractures ; Magnesium ; Mechanical properties ; Modulus of elasticity ; Particle size ; Physiological aspects ; Plasma sintering ; Porous materials ; Powder metallurgy ; Powders ; Pressure effects ; Sinterability ; Sintering ; Sintering (powder metallurgy) ; Spark plasma sintering ; Stainless steel ; Stress concentration ; Titanium alloys ; Transplants & implants</subject><ispartof>Materials, 2024-07, Vol.17 (14), p.3470</ispartof><rights>COPYRIGHT 2024 MDPI AG</rights><rights>2024 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). 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The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were systematically analyzed. Uniform dispersion of Mg within the Ti matrix was achieved, confirming the efficacy of ethanol-assisted ball milling for consistent mixing. The Young's modulus of the composite materials exhibited a linear decrease with increasing Mg content, with Ti-30vol%Mg and Ti-50vol%Mg demonstrating reduced modulus values compared to pure Ti. Based on density measurements, compression tests, and Young's modulus results, it was determined that the sinterability of Ti-30vol%Mg saturates at a sintering pressure of approximately 50 MPa. Moreover, our immersion tests in physiological saline underscore the profound significance of our findings. Ti-30vol%Mg maintained compressive strength above that of cortical bone for 6-to-10 days, with mechanical integrity improving under higher sintering pressures. These findings mark a significant leap towards the development of Ti-Mg composite biomaterials with tailored mechanical properties, thereby enhancing biocompatibility and osseointegration for a wide range of biomedical applications.</description><subject>Analysis</subject><subject>Ball milling</subject><subject>Biocompatibility</subject><subject>Biological products</subject><subject>Biomedical materials</subject><subject>Composite materials</subject><subject>Compression tests</subject><subject>Compressive strength</subject><subject>Ethanol</subject><subject>Fractures</subject><subject>Magnesium</subject><subject>Mechanical properties</subject><subject>Modulus of elasticity</subject><subject>Particle size</subject><subject>Physiological aspects</subject><subject>Plasma sintering</subject><subject>Porous materials</subject><subject>Powder metallurgy</subject><subject>Powders</subject><subject>Pressure effects</subject><subject>Sinterability</subject><subject>Sintering</subject><subject>Sintering (powder metallurgy)</subject><subject>Spark plasma sintering</subject><subject>Stainless steel</subject><subject>Stress concentration</subject><subject>Titanium alloys</subject><subject>Transplants & implants</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkV1LwzAUhoMobszd-AOk4I0Inflq2lzO4VSYKDhvvCmnbTIz22YmnaC_3sz5hTkXyTk8bzi8L0KHBI8Yk_isAZISzniKd1CfSCliIjnf_fPuoaH3SxwOYySjch_1glCwVNA-epxC4UwJnbFtBG0VTZ7AQdkpZ963Q6ujc2MbVQWqjuYmvllEE9usrDed8tGrgeh-Be45uqvBN6Ex7UbdLg7Qnobaq-HXPUAP04v55Cqe3V5eT8azuKSp7GIFVGSFykSRpTRhILkEirXWItOp5qmAilaiUoWGJNNSMw5cYE4kBV6WirIBOtn-u3L2Za18lzfGl6quoVV27XOGs4QEnOCAHv9Dl3bt2rDdJ4UxT3ASqNGWWkCtctNq2wVLQlWqMaVtlTZhPs4w45IGU4PgdCsonfXeKZ2vnGnAveUE55uU8t-UAnz0tcO6CK7-oN-ZsA-Z_ItM</recordid><startdate>20240713</startdate><enddate>20240713</enddate><creator>Masuda, Taisei</creator><creator>Oh, Minho</creator><creator>Kobayashi, Equo</creator><general>MDPI AG</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><orcidid>https://orcid.org/0000-0003-0635-163X</orcidid><orcidid>https://orcid.org/0000-0001-8043-5044</orcidid></search><sort><creationdate>20240713</creationdate><title>Fabrication and Characterization of Biomedical Ti-Mg Composites via Spark Plasma Sintering</title><author>Masuda, Taisei ; 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The effects of powder mixing, Mg addition, and sintering pressure on the microstructure and mechanical properties of the composite materials were systematically analyzed. Uniform dispersion of Mg within the Ti matrix was achieved, confirming the efficacy of ethanol-assisted ball milling for consistent mixing. The Young's modulus of the composite materials exhibited a linear decrease with increasing Mg content, with Ti-30vol%Mg and Ti-50vol%Mg demonstrating reduced modulus values compared to pure Ti. Based on density measurements, compression tests, and Young's modulus results, it was determined that the sinterability of Ti-30vol%Mg saturates at a sintering pressure of approximately 50 MPa. Moreover, our immersion tests in physiological saline underscore the profound significance of our findings. Ti-30vol%Mg maintained compressive strength above that of cortical bone for 6-to-10 days, with mechanical integrity improving under higher sintering pressures. 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| subjects | Analysis Ball milling Biocompatibility Biological products Biomedical materials Composite materials Compression tests Compressive strength Ethanol Fractures Magnesium Mechanical properties Modulus of elasticity Particle size Physiological aspects Plasma sintering Porous materials Powder metallurgy Powders Pressure effects Sinterability Sintering Sintering (powder metallurgy) Spark plasma sintering Stainless steel Stress concentration Titanium alloys Transplants & implants |
| title | Fabrication and Characterization of Biomedical Ti-Mg Composites via Spark Plasma Sintering |
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