Gas chromatography mass spectrometer determination of dimethylamine impurity in N,N‐dimethylformamide solvent by derivatization of N,N‐dimethylbenzamide with benzoyl chloride agent

This study describes the development of a reliable and linear analytical method for precisely determining dimethylamine impurity in N,N‐dimethylformamide solvent utilizing a benzoyl chloride derivatization reagent and a gas chromatography mass spectrometer. Benzoyl chloride was used to derivatize di...

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Veröffentlicht in:	Biomedical chromatography 2024-08, Vol.38 (8), p.e5920-n/a
Hauptverfasser:	Kousrali, Sayyad, Kowtharapu, Leela Prasad, Mondal, Tanmoy
Format:	Artikel
Sprache:	eng
Schlagworte:	benzoyl chloride derivatization reagent gas chromatography mass spectrometer method validation N,N‐dimethylbenzamide N,N‐dimethylformamide
Online-Zugang:	Volltext
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