The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films

The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100 g/l NaOH + 20 g/l Na 2B 4O 7·10H 2O + 50 g/l C 6H 5Na 3O 7·2H 2O + 60g/l Na 2SiO 3·9H 2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and p...

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Veröffentlicht in:Applied surface science 2007-10, Vol.253 (24), p.9387-9394
Hauptverfasser: Wu, Hai-lan, Cheng, Ying-liang, Li, Ling-ling, Chen, Zhen-hua, Wang, Hui-min, Zhang, Zhao
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container_end_page 9394
container_issue 24
container_start_page 9387
container_title Applied surface science
container_volume 253
creator Wu, Hai-lan
Cheng, Ying-liang
Li, Ling-ling
Chen, Zhen-hua
Wang, Hui-min
Zhang, Zhao
description The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100 g/l NaOH + 20 g/l Na 2B 4O 7·10H 2O + 50 g/l C 6H 5Na 3O 7·2H 2O + 60g/l Na 2SiO 3·9H 2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60 min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20 mA/cm 2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg 2SiO 4.
doi_str_mv 10.1016/j.apsusc.2007.05.085
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The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60 min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20 mA/cm 2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg 2SiO 4.</description><identifier>ISSN: 0169-4332</identifier><identifier>EISSN: 1873-5584</identifier><identifier>DOI: 10.1016/j.apsusc.2007.05.085</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Alkaline solution ; Anodized film ; Applied sciences ; Condensed matter: structure, mechanical and thermal properties ; Corrosion ; Corrosion mechanisms ; Cross-disciplinary physics: materials science; rheology ; EIS ; Exact sciences and technology ; Materials science ; Metals. 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The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60 min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20 mA/cm 2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg 2SiO 4.</description><subject>Alkaline solution</subject><subject>Anodized film</subject><subject>Applied sciences</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Corrosion</subject><subject>Corrosion mechanisms</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>EIS</subject><subject>Exact sciences and technology</subject><subject>Materials science</subject><subject>Metals. Metallurgy</subject><subject>Physics</subject><subject>Structure and morphology; thickness</subject><subject>Surface treatments</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><subject>Thin film structure and morphology</subject><subject>ZK60</subject><issn>0169-4332</issn><issn>1873-5584</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNp9kLGO1DAQhiMEEsvBG1C4gS7BjuNs0iChEweIk2iOhsaatcfHLI692A7S0fLiOOwJOqqxNN984_mb5rngneBifHXs4JTXbLqe833HVccn9aDZiWkvW6Wm4WGzq9jcDlL2j5snOR85F33t7ppfN1-RQYiWfkKhGFh07MvHkbMFbgNmWhcG3sc7RqE-voGngCxHv_6BTQwFKFC4ZZk8GSibzLJSpSamFPNGnVI8YSqEebOXvwvRMkd-yU-bRw58xmf39aL5fPX25vJ9e_3p3YfLN9etkeO-tGbCebYgpHDTKK2yB1AH5DhI6JWDad6DAynHgzMSjZrFKIQ9zCgkilG6QV40L8_e-qHvK-aiF8oGvYeAcc1aciGlGvsKDmfQ1AtyQqdPiRZId1pwvSWuj_qcuN4S11zpmngde3Hvh2zAuwTBUP43O_N5GJSs3Oszh_XYH4RJZ0MYDFpKaIq2kf6_6Dd81Zwv</recordid><startdate>20071015</startdate><enddate>20071015</enddate><creator>Wu, Hai-lan</creator><creator>Cheng, Ying-liang</creator><creator>Li, Ling-ling</creator><creator>Chen, Zhen-hua</creator><creator>Wang, Hui-min</creator><creator>Zhang, Zhao</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20071015</creationdate><title>The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films</title><author>Wu, Hai-lan ; Cheng, Ying-liang ; Li, Ling-ling ; Chen, Zhen-hua ; Wang, Hui-min ; Zhang, Zhao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c367t-c8e99da131f863d5dba5be0e43a25fa897afa336bfc3ec591611db9e13e163f43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Alkaline solution</topic><topic>Anodized film</topic><topic>Applied sciences</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Corrosion</topic><topic>Corrosion mechanisms</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>EIS</topic><topic>Exact sciences and technology</topic><topic>Materials science</topic><topic>Metals. Metallurgy</topic><topic>Physics</topic><topic>Structure and morphology; thickness</topic><topic>Surface treatments</topic><topic>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</topic><topic>Thin film structure and morphology</topic><topic>ZK60</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Hai-lan</creatorcontrib><creatorcontrib>Cheng, Ying-liang</creatorcontrib><creatorcontrib>Li, Ling-ling</creatorcontrib><creatorcontrib>Chen, Zhen-hua</creatorcontrib><creatorcontrib>Wang, Hui-min</creatorcontrib><creatorcontrib>Zhang, Zhao</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Applied surface science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Hai-lan</au><au>Cheng, Ying-liang</au><au>Li, Ling-ling</au><au>Chen, Zhen-hua</au><au>Wang, Hui-min</au><au>Zhang, Zhao</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films</atitle><jtitle>Applied surface science</jtitle><date>2007-10-15</date><risdate>2007</risdate><volume>253</volume><issue>24</issue><spage>9387</spage><epage>9394</epage><pages>9387-9394</pages><issn>0169-4332</issn><eissn>1873-5584</eissn><abstract>The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100 g/l NaOH + 20 g/l Na 2B 4O 7·10H 2O + 50 g/l C 6H 5Na 3O 7·2H 2O + 60g/l Na 2SiO 3·9H 2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60 min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20 mA/cm 2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg 2SiO 4.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.apsusc.2007.05.085</doi><tpages>8</tpages></addata></record>
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subjects Alkaline solution
Anodized film
Applied sciences
Condensed matter: structure, mechanical and thermal properties
Corrosion
Corrosion mechanisms
Cross-disciplinary physics: materials science
rheology
EIS
Exact sciences and technology
Materials science
Metals. Metallurgy
Physics
Structure and morphology
thickness
Surface treatments
Surfaces and interfaces
thin films and whiskers (structure and nonelectronic properties)
Thin film structure and morphology
ZK60
title The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films
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