The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films
The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100 g/l NaOH + 20 g/l Na 2B 4O 7·10H 2O + 50 g/l C 6H 5Na 3O 7·2H 2O + 60g/l Na 2SiO 3·9H 2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and p...
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Veröffentlicht in: | Applied surface science 2007-10, Vol.253 (24), p.9387-9394 |
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creator | Wu, Hai-lan Cheng, Ying-liang Li, Ling-ling Chen, Zhen-hua Wang, Hui-min Zhang, Zhao |
description | The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100
g/l NaOH
+
20
g/l Na
2B
4O
7·10H
2O
+
50
g/l C
6H
5Na
3O
7·2H
2O
+
60g/l Na
2SiO
3·9H
2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60
min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20
mA/cm
2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg
2SiO
4. |
doi_str_mv | 10.1016/j.apsusc.2007.05.085 |
format | Article |
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g/l NaOH
+
20
g/l Na
2B
4O
7·10H
2O
+
50
g/l C
6H
5Na
3O
7·2H
2O
+
60g/l Na
2SiO
3·9H
2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60
min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20
mA/cm
2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg
2SiO
4.</description><identifier>ISSN: 0169-4332</identifier><identifier>EISSN: 1873-5584</identifier><identifier>DOI: 10.1016/j.apsusc.2007.05.085</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Alkaline solution ; Anodized film ; Applied sciences ; Condensed matter: structure, mechanical and thermal properties ; Corrosion ; Corrosion mechanisms ; Cross-disciplinary physics: materials science; rheology ; EIS ; Exact sciences and technology ; Materials science ; Metals. Metallurgy ; Physics ; Structure and morphology; thickness ; Surface treatments ; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) ; Thin film structure and morphology ; ZK60</subject><ispartof>Applied surface science, 2007-10, Vol.253 (24), p.9387-9394</ispartof><rights>2007 Elsevier B.V.</rights><rights>2008 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c367t-c8e99da131f863d5dba5be0e43a25fa897afa336bfc3ec591611db9e13e163f43</citedby><cites>FETCH-LOGICAL-c367t-c8e99da131f863d5dba5be0e43a25fa897afa336bfc3ec591611db9e13e163f43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.apsusc.2007.05.085$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,781,785,3551,27929,27930,46000</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=19094453$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Wu, Hai-lan</creatorcontrib><creatorcontrib>Cheng, Ying-liang</creatorcontrib><creatorcontrib>Li, Ling-ling</creatorcontrib><creatorcontrib>Chen, Zhen-hua</creatorcontrib><creatorcontrib>Wang, Hui-min</creatorcontrib><creatorcontrib>Zhang, Zhao</creatorcontrib><title>The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films</title><title>Applied surface science</title><description>The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100
g/l NaOH
+
20
g/l Na
2B
4O
7·10H
2O
+
50
g/l C
6H
5Na
3O
7·2H
2O
+
60g/l Na
2SiO
3·9H
2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60
min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20
mA/cm
2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg
2SiO
4.</description><subject>Alkaline solution</subject><subject>Anodized film</subject><subject>Applied sciences</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Corrosion</subject><subject>Corrosion mechanisms</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>EIS</subject><subject>Exact sciences and technology</subject><subject>Materials science</subject><subject>Metals. Metallurgy</subject><subject>Physics</subject><subject>Structure and morphology; thickness</subject><subject>Surface treatments</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><subject>Thin film structure and morphology</subject><subject>ZK60</subject><issn>0169-4332</issn><issn>1873-5584</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNp9kLGO1DAQhiMEEsvBG1C4gS7BjuNs0iChEweIk2iOhsaatcfHLI692A7S0fLiOOwJOqqxNN984_mb5rngneBifHXs4JTXbLqe833HVccn9aDZiWkvW6Wm4WGzq9jcDlL2j5snOR85F33t7ppfN1-RQYiWfkKhGFh07MvHkbMFbgNmWhcG3sc7RqE-voGngCxHv_6BTQwFKFC4ZZk8GSibzLJSpSamFPNGnVI8YSqEebOXvwvRMkd-yU-bRw58xmf39aL5fPX25vJ9e_3p3YfLN9etkeO-tGbCebYgpHDTKK2yB1AH5DhI6JWDad6DAynHgzMSjZrFKIQ9zCgkilG6QV40L8_e-qHvK-aiF8oGvYeAcc1aciGlGvsKDmfQ1AtyQqdPiRZId1pwvSWuj_qcuN4S11zpmngde3Hvh2zAuwTBUP43O_N5GJSs3Oszh_XYH4RJZ0MYDFpKaIq2kf6_6Dd81Zwv</recordid><startdate>20071015</startdate><enddate>20071015</enddate><creator>Wu, Hai-lan</creator><creator>Cheng, Ying-liang</creator><creator>Li, Ling-ling</creator><creator>Chen, Zhen-hua</creator><creator>Wang, Hui-min</creator><creator>Zhang, Zhao</creator><general>Elsevier B.V</general><general>Elsevier Science</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20071015</creationdate><title>The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films</title><author>Wu, Hai-lan ; Cheng, Ying-liang ; Li, Ling-ling ; Chen, Zhen-hua ; Wang, Hui-min ; Zhang, Zhao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c367t-c8e99da131f863d5dba5be0e43a25fa897afa336bfc3ec591611db9e13e163f43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Alkaline solution</topic><topic>Anodized film</topic><topic>Applied sciences</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Corrosion</topic><topic>Corrosion mechanisms</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>EIS</topic><topic>Exact sciences and technology</topic><topic>Materials science</topic><topic>Metals. Metallurgy</topic><topic>Physics</topic><topic>Structure and morphology; thickness</topic><topic>Surface treatments</topic><topic>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</topic><topic>Thin film structure and morphology</topic><topic>ZK60</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Hai-lan</creatorcontrib><creatorcontrib>Cheng, Ying-liang</creatorcontrib><creatorcontrib>Li, Ling-ling</creatorcontrib><creatorcontrib>Chen, Zhen-hua</creatorcontrib><creatorcontrib>Wang, Hui-min</creatorcontrib><creatorcontrib>Zhang, Zhao</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Applied surface science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Hai-lan</au><au>Cheng, Ying-liang</au><au>Li, Ling-ling</au><au>Chen, Zhen-hua</au><au>Wang, Hui-min</au><au>Zhang, Zhao</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films</atitle><jtitle>Applied surface science</jtitle><date>2007-10-15</date><risdate>2007</risdate><volume>253</volume><issue>24</issue><spage>9387</spage><epage>9394</epage><pages>9387-9394</pages><issn>0169-4332</issn><eissn>1873-5584</eissn><abstract>The anodization of ZK60 magnesium alloy in an alkaline electrolyte of 100
g/l NaOH
+
20
g/l Na
2B
4O
7·10H
2O
+
50
g/l C
6H
5Na
3O
7·2H
2O
+
60g/l Na
2SiO
3·9H
2O was studied in this paper. The corrosion resistance of the anodic films was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques and the microstructure and composition of films were examined by SEM and XRD. The influence of anodizing time was studied and the results show that the anodizing time of 60
min is suitable for acquiring films with good corrosion resistance. The influence of current density on the corrosion resistance of anodizing films was also studied and the results show that the film anodized at 20
mA/cm
2 has the optimum corrosion resistance. The film formed by anodizing in the alkaline solution with optimized parameters show superior corrosion resistance than that formed by the traditional HAE process. The XRD pattern shows that the components of the anodized film consist of MgO and Mg
2SiO
4.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.apsusc.2007.05.085</doi><tpages>8</tpages></addata></record> |
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source | Access via ScienceDirect (Elsevier) |
subjects | Alkaline solution Anodized film Applied sciences Condensed matter: structure, mechanical and thermal properties Corrosion Corrosion mechanisms Cross-disciplinary physics: materials science rheology EIS Exact sciences and technology Materials science Metals. Metallurgy Physics Structure and morphology thickness Surface treatments Surfaces and interfaces thin films and whiskers (structure and nonelectronic properties) Thin film structure and morphology ZK60 |
title | The anodization of ZK60 magnesium alloy in alkaline solution containing silicate and the corrosion properties of the anodized films |
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