Thermal and structural investigation of SnO2/Sb2O3 obtained by the polymeric precursor method
SnO2-based materials are used as sensors, catalysts and in electro-optical devices. This work aims to synthesize and characterize the SnO2/Sb2O3-based inorganic pigments, obtained by the polymeric precursor method, also known as Pechini method (based on the metallic citrate polymerization by means o...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2007-03, Vol.87 (3), p.697-701 |
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| container_end_page | 701 |
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| container_issue | 3 |
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| container_title | Journal of thermal analysis and calorimetry |
| container_volume | 87 |
| creator | DE MELO, Danniely S SANTOS, M. R. C SANTOS, Ieda M. G SOLEDADE, L. E. B BERNARDI, M. I. B LONGO, E SOUZA, A. G |
| description | SnO2-based materials are used as sensors, catalysts and in electro-optical devices. This work aims to synthesize and characterize the SnO2/Sb2O3-based inorganic pigments, obtained by the polymeric precursor method, also known as Pechini method (based on the metallic citrate polymerization by means of ethylene glycol). The precursors were characterized by thermogravimetry (TG) and differential thermal analysis (DTA). After characterization, the precursors were heat-treated at different temperatures and characterized by X-ray diffraction. According to the TG/DTA curves basically two-step mass loss process was observed: the first one is related to the dehydration of the system; and the second one is representative to the combustion of the organic matter. Increase of the heat treatment temperature from 500 to 600 deg C and 700 deg C resulted higher crystallinity of the formed product. |
| doi_str_mv | 10.1007/s10973-006-7778-9 |
| format | Article |
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According to the TG/DTA curves basically two-step mass loss process was observed: the first one is related to the dehydration of the system; and the second one is representative to the combustion of the organic matter. 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According to the TG/DTA curves basically two-step mass loss process was observed: the first one is related to the dehydration of the system; and the second one is representative to the combustion of the organic matter. 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| ispartof | Journal of thermal analysis and calorimetry, 2007-03, Vol.87 (3), p.697-701 |
| issn | 1388-6150 1588-2926 1572-8943 |
| language | eng |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Applied sciences Chemical industry and chemicals Dyes, pigments Exact sciences and technology Industrial chemicals |
| title | Thermal and structural investigation of SnO2/Sb2O3 obtained by the polymeric precursor method |
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