Sintering Properties of ZrO2 - 3 Mol % Y2O3 Obtained from Mixture of Nano and Microcrystalline Powders
The polymeric precursor route based on the Pechini process was used to prepare a mixture of nano and microcrystalline powders. The zirconia powder was stabilized with 3 mol% of yttria. Powder characteristics were evaluated by the BET technique determined the specific area and the BJH method supplied...
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| Veröffentlicht in: | Materials science forum 2006-01, Vol.530-531, p.456-460 |
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| creator | Mineiro, Sergio Luiz Kuranaga, Carlos Nono, Maria do Carmo de Andrade |
| description | The polymeric precursor route based on the Pechini process was used to prepare a
mixture of nano and microcrystalline powders. The zirconia powder was stabilized with 3
mol% of yttria. Powder characteristics were evaluated by the BET technique determined the
specific area and the BJH method supplied the pore size distribution. The X-ray diffraction
results and SEM observations were carried out to characterize both the powder mixture and
the microstructures of the ceramic bodies. The sintering behavior shown in this work was
studied by dilatometric experiment, being considered the shrinkage rate and densification of
the microstructure. |
| doi_str_mv | 10.4028/www.scientific.net/MSF.530-531.456 |
| format | Article |
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mol% of yttria. Powder characteristics were evaluated by the BET technique determined the
specific area and the BJH method supplied the pore size distribution. The X-ray diffraction
results and SEM observations were carried out to characterize both the powder mixture and
the microstructures of the ceramic bodies. The sintering behavior shown in this work was
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mol% of yttria. Powder characteristics were evaluated by the BET technique determined the
specific area and the BJH method supplied the pore size distribution. The X-ray diffraction
results and SEM observations were carried out to characterize both the powder mixture and
the microstructures of the ceramic bodies. The sintering behavior shown in this work was
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mixture of nano and microcrystalline powders. The zirconia powder was stabilized with 3
mol% of yttria. Powder characteristics were evaluated by the BET technique determined the
specific area and the BJH method supplied the pore size distribution. The X-ray diffraction
results and SEM observations were carried out to characterize both the powder mixture and
the microstructures of the ceramic bodies. The sintering behavior shown in this work was
studied by dilatometric experiment, being considered the shrinkage rate and densification of
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| title | Sintering Properties of ZrO2 - 3 Mol % Y2O3 Obtained from Mixture of Nano and Microcrystalline Powders |
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